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Titration Start (mL) End (mL) V (mL) MW of Sodium Oxal

1 24.50 31.10 6.60 MW of CaC2O4


2 3.10 10.50 7.40 MW of Ca
3 10.50 17.30 6.80 MW of CaCO3
4 17.30 24.50 7.20

Sodium Stoichiome
Mass of Sodium Oxalate tric mol of
Trial # Oxalate (g) (mol) KMnO4 Mpermanganate
1 0.2565 0.00183 0.00073 0.1110
2 0.2582 0.00184 0.00074 0.0997 Mean Molarity of the permanganate so
3 0.2546 0.00182 0.00073 0.1070 STDEV of Molarity of the permanganat
4 0.2582 0.00184 0.00074 0.1025 90 %Confidence Interval
Mean Molarity of the permanganate so

Eggs:

Mass of ammonium oxalate 25.082 g

Student
Name/Egg # White (g) Brown(g)
Us/6,5 0.2706 0.2542
Group1/1,2 0.2748 0.2621
Group2/3,4 0.2733 0.2669

Gravimetric Results

Weight
After clean with After dry in Mass of Mass of Percent
Crucible # filter and dry oven CaC2O4 (g) Ca (g) of Ca (%)
1 19.2432 19.6229 0.3797 0.1188 43.2 Average of Ca weight percen
2 18.0132 18.3674 0.3542 0.1108 42.3 STDEV of Ca in white
3 17.4435 17.814 0.3705 0.1159 42.4 Average of Ca weight percen
4 16.5418 16.9117 0.3699 0.1157 43.4 STDEV of Ca in brown
5 17.4882 17.8337 0.3455 0.1081 42.5 90% Confidence Interval
6 17.5746 17.944 0.3694 0.1156 42.7 Mean of Ca in white
Mean of Ca in brown
Titrimetric Results
Titration

Mass of CaCO3 Mole of Moles of Mass of


Crucible # (g) Start (mL) End (mL) V (mL) KMnO4 Ca Ca (g)
1 0.2967 31.1 40.5 9.4 0.00099 0.00247 0.0989
2 0.2767 12.7 21.7 9 0.00095 0.00236 0.0947
3 0.2895 21.7 30.9 9.2 0.00097 0.00242 0.0968
4 0.2890
5 0.2700
6 0.2886

Average of Ca weight percent in 35.72 %


STDEV of Ca in white 0.40 %
Average of Ca weight percent in 36.14 %
STDEV of Ca in brown 0.00 %
90% Confidence Interval
Mean of Ca in white 35.72 0.68 %
Mean of Ca in brown 36.14 0.00 %
139.999 g/mol
128.097 g/mol
40.078 g/mol
100.087 g/mol

Molarity of the permanganate solution 0.1050 M


of Molarity of the permanganate solution 0.0050 M
nfidence Interval
Molarity of the permanganate solution 0.1050 0.0059 M

Average of Ca weight percent in White 42.79 %


STDEV of Ca in white 0.41 %
Average of Ca weight percent in brown 42.72 %
STDEV of Ca in brown 0.57 %
90% Confidence Interval
Mean of Ca in white 42.79 0.70 %
Mean of Ca in brown 42.72 0.96 %
Weight Percent of Ca (%)
36.0
36.1
35.4

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