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Fabrication and Tribological

R. Caslaru
Department of Mechanical Engineering,
The University of Alabama,
Functions of Microdent Arrays
Tuscaloosa, AL 35487
on Ti6Al4V Surface by Laser
M. P. Sealy
Department of Mechanical Engineering,
The University of Alabama,
Shock Peening
Tuscaloosa, AL 35487
Surface patterning has become a valuable technique for fabricating microdents, which
Y. B. Guo1 may act as lubricant reservoirs to reduce friction and wear in sliding and rolling contact
applications. In this paper, the use of laser shock peening (LSP) along with an automatic
Department of Mechanical Engineering,
XY table proves to be an attractive and reliable method for producing microdent arrays
The University of Alabama,
with enhanced surface integrity. Surface topography and profiles of the fabricated micro-
Tuscaloosa, AL 35487
dent arrays on polished Ti6Al4V have been characterized. The effect of dent arrays
e-mail: yguo@eng.ua.edu
with different density on friction reduction at low and high viscosity lubrication was
investigated. An acoustic emission (AE) sensor was used to online monitor friction and
X. T. Wei wear processes. It was found that a surface with 10% dent density provides better effect
School of Mechanical Engineering,
in reducing coefficient of friction (CoF) than those of smooth surface and a surface with
Shandong University of Technology,
20% dent density. It was shown that there is a strong correlation between AE energy
Zibo 255049, China
signals and wear rate. [DOI: 10.1115/1.4027918]

Keywords: surface patterning, tribology, laser shock peening, acoustic emission

Introduction loading. Treating critical fatigue areas that have high stress con-
centrations can prevent cracking and subsequent spalling [1012].
Dent Arrays Fabrication Techniques and Functions. Con- Usually, LSP is applied to metals to strengthen the surface and
trolled patterning of solid surfaces improves wear, friction, and is not traditionally considered a patterning process. However,
lubrication [1]. Controlled surface patterning involves the altering when the desired outcome is to improve tribological performance,
of surface topography by mechanical, lithographic, laser, or coat- LSP becomes an attractive alternative method because it can pat-
ing techniques [2]. Microdents serve as fluid reservoirs that effec- tern while simultaneously imparting a strengthened surface integ-
tively retain lubricant and function as traps for wear debris, which rity free of thermal damage associated with many other processes.
can minimize any potential plowing effect caused by entrapped Other processes require choosing between strengthening and
particles. The long term benefit of surface patterning is to extend patterning. This study focused on feasibility of the patterning
the life of contacting surfaces. Microdents on the surface can capability of LSP. The objective of this study is to introduce
improve the surface lifetime by a factor of 10 [3]. Experimental micro-LSP as a surface patterning process to produce microdent
studies on the effect of dent patterns on microgrooved sapphire arrays on sliding interfaces with direct impact on tribological
disks lead to the conclusion that fabricated microdent arrays on performance.
metallic surfaces are a useful method to reduce friction in sliding Various experimental setups have been used to evaluate the
contact [4]. Manufacturing techniques to fabricate microdents effect of different surface topographies on wear, friction, and
arrays on component surfaces include micro-indentation [4], lubrication behavior of patterned surfaces. The experimental set-
microdrilling [5], and laser ablation/machining [6]. These proc- ups include: (1) pin-on-disk tests on microgrooved sapphire disks
esses often induce surface damage such as cracks, phase transfor- by Blatter et al. [13], (2) block-on-ring tests on ceramic plates by
mation, or a heat affected zone (HAZ), which may shorten a Geiger et al. [14], (3) three-pins-on-disks tests with dents achieved
components life. A new process to create dents while avoiding by abrasive jet machining and laser beam machining by Wakuda
material damage is highly needed. et al. [15], (4) oscillating tests on coated silicon disks by Petters-
LSP is a mechanical process where pressure waves caused by son and Jacobson [16], (5) customized test rig, which simulates
expanding plasma plastically deform a materials surface. The ring-cylinder interaction in piston-cylinder applications, by Ryk
plastic deformation from LSP induces beneficial deep compres- et al. [17], and (6) fixed-ball-on-disk tests on steel laser textured
sive residual stresses well below the surface. The residual stresses disks by Andersson et al. [1]. All authors have concluded the ben-
can penetrate as deep as 1 mm [7]. In addition to producing com- eficial effect of patterning on reducing friction and improving the
pressive residual stress and refining grain size to increase material tribological behavior.
strength, LSP also eliminates thermally induced damage, such as Ti6Al4V is the most commonly used titanium alloy. Over
a HAZ, which is often associated with laser machining processes. 70% of all alloy grades melted are a subgrade of Ti6Al4V.
Instead, dents are formed by purely mechanical means. Applications include aerospace, marine, and power generation
Furthermore, the compressive residual stresses greatly improve components. However, surface contact applications of Ti6Al4V
against fatigue crack formation and propagation induced by cyclic are limited due to a pronounced galling tendency.
loading [8,9]. LSP is well suited for localized regions under cyclic
Acoustic Monitoring of Tribology. One objective of this
1
Corresponding author. research is to evaluate the effect of micro-LSP produced dent
Contributed by the Manufacturing Engineering Division of ASME for publication
in the JOURNAL OF MANUFACTURING SCIENCE AND ENGINEERING. Manuscript received
arrays on tribology and to establish a correlation between AE fea-
March 12, 2014; final manuscript received June 20, 2014; published online August ture signals and the investigated tribological parameters of CoF,
12, 2014. Editor: Y. Lawrence Yao. wear, and lubrication. AE monitoring is one of the most effective

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noninvasive methods for process monitoring used in surface qual- While there is explicit experimental support that tribological
ity control. AE signals may be defined as transient elastic stress phenomena are correlated to AE signals, the assignment of a spe-
waves generated at the interaction zone by the rapid release of cific wear mechanism to specific AE signal characteristics is still
strain energy within the material. A detected AE signal is directly a complicated task. Two important issues need to be addressed.
proportional to the mechanical energy released between the con- One problem is that theoretical models of how AEs are generated
tacting surfaces and can be related to different phenomena within by various possible mechanisms are not developed to allow a clear
the contact zone, such as asperity contact, dislocation movements, definition of AE signal details as resulting from all of the possible
microcrack initiation and growth, plastic deformation, and flow. mechanical processes. The second issue is that the AE signal trav-
Since any combination of these mechanisms involved in the wear els through different physical bodies and interfaces from its gener-
process could be active at any time, signal processing becomes a ation point to the sensor. These interfaces may act as wave
very complicated task. An important advantage for using AE sig- modulators and filters for transmitted wave characteristics. So, the
nal processing is presented by the software capabilities to elimi- interpretation of AE signals in terms of specific causes is a very
nate noise signal and extract feature signal that could be difficult task. There are two general experimental strategies imple-
distinctively correlated to process parameters. AE signals could be mented as a response to these difficulties. The first approach
divided into two categories: transient pulses characterized by requires entire signal analysis from a particular process while gen-
burst-type AE signals and continuous AE signals [18]. Two types eration mechanisms are assigned on the basis of material behavior
of AE signal analysis are typically used: frequency analysis and knowledge. For the second approach, experimental plans are
time domain analysis [19]. Another key aspect of using AE signals developed in which only certain mechanisms are known to be
to monitor different processes is that frequency range of the AE active and generate AE signals.
signal is much higher than that of machine vibrations and environ-
mental noise. Different methods based on burst-type AE signal
using frequency analysis have been developed for monitoring tool Surface Texturing by LSP
wear in face milling [2022], surface integrity during hard turning Sample Preparation and Dent Array Fabrication.
process [23], stamping process [24], and drilling [25]. Ti6Al4V samples were sectioned 1=4 in. thick from a 3 in. diam-
AE monitoring offers a useful approach in investigating wear eter round bar. Ti6Al4V is a widely used a b Ti alloy due to
mechanisms. Since wear during sliding is a quasi-continuous pro- its combination of high strength, light weight, good formability,
cess, AE monitoring was expected to offer a good measure of the corrosion resistance, and creep properties at room and elevated
wear process. In past research, real time analysis for parameters temperatures. In order to improve surface finish, each sample was
such as AE counts, count rate, rms, peak amplitude, and AE turned and then polished to a mirror finish. To remove the effects
energy were successfully used to evaluate wear mechanisms. Mat- of turning, the samples went through a lapping process. Two hours
suoka et al. [26] conducted a study aimed at determining the use- of continuously lapping, using lapping oil and powder, were esti-
fulness of AE techniques for investigation of tribological mated to remove an approximate 0.1 mm surface layer. In the next
phenomena in hard disk drive slider and disk applications. The step, titanium samples underwent two stages TM of polishing using
study correlates rms signal with wear coefficient and with wear various polishing pads: 1200 grit and Lecloth . In order to pre-
volume through Archards equation [26]. Accurate correlation vent and remove any micron sized pits and scratches induced by
between CoF and AE rms voltage for dry ball-on-cylinder tests polishing, aluminum powder in conjunction with lapping oil and/
and proportionality between the theoretically determined grease or de-ionized water was used at low polishing speeds to achieve a
film thickness and rms were reported [27]. mirror finish. The surface roughness (Ra) was measured along
AE signal energy could be very useful in the characterization of 10 mm spans at random locations across the surface. The average
wear mechanisms since AE energy measurements can be directly surface roughness measured less than 10 nm.
related to important physical parameters. Intensification of wear Dent arrays were created with a Q-switched neodymium-doped
mechanisms through generation of bigger wear particles was pro- yttrium aluminum garnet (Nd:YAG) laser with a wavelength of
portionally reflected in higher levels of AE energy recorded dur- 1064 nm and a frequency of 30 Hz. The laser emitted a 57 ns
ing the tests [28]. Gaussian distributed pulse. The laser beam was focused to a diam-
AE counts and cumulative counts for wear characterization eter of 43.3 lm using a 100 mm focal length lens. The energy was
were used for dry rubbing of pin on rotating disk tests [28]. The measured using an Ophir 30 A-HE power meter and ranged from
AE cumulative counts are connected to the number of wear par- 33 to 133 mJ. The calculated laser intensity was 323 GW/cm2 cor-
ticles. AE method could detect tribological phenomena such as responding to a power of 1 W. Figure 1 shows the experimental
the removal or transfer particles that could not be detected by setup. Each experiment was performed in a water confined regime
CoF. The wear mode and wear scale could be judged from magni- at a depth of 2.53 mm. The ablative material was polyester black
tude of AE count rate and variations in count rate amplitude [28]. tape with a thickness of 0.07 mm. Key parameters for experiment
Lingard et al. have concluded that emissions frequencies in the repeatability are focal length and depth of focus (DOF). DOF is
range of 50 kHz2 MHz are useful to characterize the stress waves defined as the distance over which the focused beam has constant
generated by the rubbing surfaces. These frequency ranges are intensity. Positioning within DOF was controlled by attaching the
distinct from lower frequency produced in large scale mechanical focal lens to a translation stage.
vibrations and the environment noise. In their study, severe wear To ensure uniform dent density and repeatability, a VXM XY
for metal specimens was investigated in pure sliding motion using table was used. The XY table presents the advantage of moving in
a two disk-machine. They proposed a correlation between AE micron incremented steps with high precision. The XY table was
total counts and frictional work as well as between AE count rate programmed and synchronized with the laser to obtain two differ-
and lubrication conditions. Count rate dropped at lubricated con- ent dent patterns in a radial orientation on the sample as presented
ditions when compared to count rate at dry conditions [29]. A in Fig. 2.
strong correlation between AE signal and wear rates was reported Geometrical pattern characteristics for 10% and 20% dent den-
for tests using a steel ball sliding against a sapphire and steel disks sities are presented in Table 1. The zigzag pattern was chosen to
under lubricated conditions. Lower AE count rates were reported provide a higher dent density along the wear track during tribolog-
for mild wear and high AE count rates for severe wear. In fre- ical tests. Repeatability becomes an issue for higher dent densities
quency domain, the AE signal variation is low for low wear rate due of the ablative material limitations.
and high for severe wear rate. It was also found that AE peak am-
plitude and rms levels are decreasing with the increase of the
applied load. It indicates the unreliability of a correlation between LSP Process Concept. LSP is a mechanical process where
these parameters with the wear rate [30]. pressure waves caused by expanding plasma plastically deform

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Fig. 3 Dent profiles at different peening power

Fig. 1 LSP experimental setup

Fig. 4 Fabricated dent array and 3D topography at 1 W laser


power (20% density)

wave is the mechanical process that plastically deforms the sur-


face. Once the peak pressure exceeds the dynamic yield stress
(Hugoniot elastic limit), plastic deformation occurs and forms a
Fig. 2 Sliding contact tracks at different dent density dent. After the shock wave disperses, the deformed region
presents a state of compressive residual stress due to constraints
from the surrounding material [10].
Table 1 Calculated geometrical pattern for dent density
Geometrical Characterization of Dent Arrays. For two
Dent Theoretical dent Vertical Horizontal dimensional dent profile characterization, experiments were car-
density diameter (lm) spacing (lm) spacing (lm) ried out on three rows. Each row corresponds to a different power
10% 120 350 120
setting. For repeatability, ten dents were produced at each power
20% 120 120 120 level and then measured to determine average dent properties.
The dent geometry was measured using a Dektak II profiler.
Figure 3 presents the dent profiles for three laser powers. Increas-
ing the power causes the radial stress to increase and wider dents
the surface. LSP uses a thin layer of ablative material that is opa- are produced. The dent depth is also increased with increasing
que to the laser. The opaque ablative material, typically black power.
spray paint or tape, is a sacrificial layer [31]. The sacrificial layer To comprehensively characterize the dent geometry, the outer
also eliminates undesirable thermal effects on the surface caused edge of the dent should be examined. As expected when doing
by the laser beam during direct ablation. The laser partially vapor- LSP, a pile-up region is formed on the outer edge of the dent. It is
izes the ablative layer to form high pressure plasma. The plasma, theorized that tensile stress develops in these pile-up regions, neg-
confined by a thin layer of water film, expands rapidly resulting in atively influencing the tribological properties. To characterize the
a recoiling pressure wave on the order of GPa [32]. The pressure pile-up region, a dent array was generated at 1 W power with a

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Table 2 Characterizations of dent depth Table 3 Linear sliding test plan

Parameter Value Surface Lubricant No. of Sliding Normal Testing


treatment type tests speed load time
Mean depth 0.507 lm
Range 1.231 lm Smooth SAE 85W-140 2 1 mm/s 5N 30 min.
Standard deviation 0.2217 lm SAE 15W-40 2
Total number of measured dents 1604 10% dent density SAE 85W-140 2
SAE 15W-40 2
20% dent density SAE 85W-140 2
SAE 15W-40 2

Table 4 Typical lubricant properties

Kinematic viscosity (cSt)

Lubricant type @ 40  C @ 100  C Density (kg/m3)

SAE 85W-140 411 25 901


SAE 15W-40 117 15.2 872

Fig. 5 Tribology testing setup

20% density pattern as described in Table 1. The peened area was


approximately 3.7 mm  24.5 mm as scanned and presented in
Fig. 4.
Three dimensional mapping was performed on the top dented
surface using Zygo New View 7300 White Light Interferometer.
Statistical information with regard to the dent depth within the
investigated area is presented in Table 2. The mean depth was
evaluated to be 0.507 lm within a range of 1.231 lm. Standard
deviation for a population of 1604 dents was 0.2217 lm.
The high range could be explained as a limitation of the abla-
tive material, which suffers drastic transformation throughout the
peening process. The tensile pile-up region from data provided for
ten individual dents was evaluated to approximately 40% of the
total volume displaced from the dented region. Consequently,
60% of the material was compressed into the bulk material. As a
result of the deformation, compressive residual stresses formed in
Fig. 6 The effect of surface patterning on friction coefficient
the material subsurface and tensile stresses developed in the pile-
up region.
positioning system meant to apply the load and position on the
sample surface. The load cell measures simultaneously the normal
Tribology Tests and Results and frictional forces in the linear sliding tests. The applied load
was controlled by an active feedback system with an accuracy of
Experimental Setup of Tribology and AE Sensor. The linear 61 N. The ball used as the upper specimen was a 10 mm diameter
sliding tests were performed on a universal UMT-2 microtribome- chrome steel ball bearing with a hardness of 63 HRC (Rockwell
ter presented in Fig. 5. The microtribometer consists of a lower ta- hardness scale C). To increase the dent effect during the tribologi-
ble on which the Ti6Al4V sample is mounted and a vertical cal tests and reduce the contact pressure between ball and surface,

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Fig. 7 Wear track profiles at high viscosity lubrication conditions

a calotte of 2 mm in diameter was produced onto the ball by grind- applied load was 5 N, and the experiment time was 30 min. Before
ing against 1200 grit sandpaper. The calotte reduced the contact the test, each sample was ultrasonically cleaned in acetone. The
pressure from 655 MPa as calculated through Hertz Theory for a tracking velocity was set for 0.15 mm/s. Tracking velocity repre-
point contact, to 1.59 MPa as obtained by dividing the applied sents the upper specimens vertical reaction velocity to the surface
pressure by the calotte area. A contact pressure of 655 MPa is roughness along the wear track. Its purpose is to keep the applied
close to the materials compressive yield strength of 970 MPa and load to a constant 5 N level while allowing for instrument self-
could result in a complete cancelation of any dent effect on the corrections due to an uneven surface geometry. For repeatability
surface. The ball, fixed in the load cell in a permanent position, reasons, two tests were completed under the same conditions.
was repolished using 1 lm diamond paste for approximately The Dektak II profiler was used to characterize the wear track
20 min before every test. after tests on tribometer. Three profiles were scanned at three dis-
Table 3 presents the linear sliding test conditions for each type of tinct locations on every wear track using the lowest tracking ve-
surface treatment. The surface treatments were a smooth polished locity (50 lm/s). The cross-sectional area was obtained by
surface, 10% dent density, and 20% dent density. Linear sliding averaging the three measured values. The cross-sectional area
tests were performed under flooded lubricated conditions using two estimated the volume of material lost used in the wear rate
distinct lubricants, high viscosity lubricant (typical gear box oil calculation. The wear rate was calculated by
SAE 85 W-140) and low viscosity lubricant (typical engine oil SAE
15 W-40). The tests were performed at room temperature at a con- V
k (1)
stant sliding speed of 1 mm/s for a track length of 20 mm. The LS

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Fig. 8 Wear track profiles at low viscosity lubrication conditions

where k is the wear rate in mm3/N m, V is the volume of material analysis. Data smoothing was used to average the signal and
lost in mm3 on a wear track, L is the load applied in Newtons, and reveal the trends.
S is the sliding distance in meters.
As presented in Fig. 5, an AE sensor was attached on the ball
holder. AE signal is captured through a high frequency piezoelec- Effect of Dent Arrays on CoF at Diffident Lubrication
tric transducer. The sensor was mounted as close as possible to Conditions. Lubricant properties used in the experiments are pre-
the contact point to minimize the number of signal traveling inter- sented in Table 4. The lubricant creates a thin film between inter-
faces. The output is amplified and filtered to remove unrelated acting surfaces, thereby acting on sustaining the load and reducing
noise before being sent to the data processing unit. Vacuum grease the wear. The film created by low viscosity oil breaks much easier
was used as the coupling medium between sensor and ball holder. under the given stress conditions. Under flooded lubrication con-
The forces and the AE signals were collected in real time during dition, low viscosity oil will favorably remove wear particles from
the test for postanalysis. Sliding wear processes were monitored the wear zone. High viscosity oil presents a lower fluidity and
using the AE signal acquisition software and processing package higher cohesive forces entrapping wear particles within the
AEWin [33]. The AE sensor has a 125 kHz resonant frequency interaction zone.
and is connected to a 18 bit PCI-2 data acquisition board incorpo- Figure 6 presents the CoF variation during the tests under high
rated into a PC. The data were passed through a preamplifier that viscosity and low viscosity conditions. For both testing condi-
was set to a 40 dB gain. The threshold was set to 25 dB. tions, 10% dent density reduces the CoF and 20% dent density
Investigated AE signals include amplitude, counts, rms, and increases the CoF value. For high viscosity lubrication condition,
absolute energy. TecPlot was the main software used for signal the CoF trend reaches steady state much earlier than for low

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Fig. 9 Calculated wear rate at high viscosity lubrication
conditions
Fig. 11 AE energy at high viscosity lubrication conditions

Fig. 10 Calculated wear rate at low viscosity lubrication


conditions

viscosity lubrication condition. Under high viscosity testing con-


ditions, 10% dent density considerably reduces the CoF from a
smooth surface CoF value of 0.420.34. The 20% dent density Fig. 12 AE energy at low viscosity lubrication conditions
treatment negatively affects CoF, increasing its value to 0.49.
This behavior could be correlated with the presence of the pile-up
regions. Greater pile-up from 20% dent density results in higher the physical lubricant properties described above. High viscosity
surface roughness, more adhesive wear, and higher CoF as lubricant acts towards increasing the wear track width due to its
opposed to 10% dent density. lack of fluidity. The wear depth is reduced due to high viscosity
Figure 6(b) shows the effect of surface patterning on CoF under oil capability to sustain the load. On the other side, the low viscos-
low viscosity lubrication conditions. The small bump at the begin- ity lubricant presents lower load carrying capability resulting in
ning of each test for all investigated surfaces could be an indicator higher depths. Low viscosity oil is more active on removing wear
of the onset of adhesive wear processes. The 10% dent density particles from the interaction zone, so thinner track widths are
acts toward lowering the CoF, but the trend is increasing with the recorded. Also, a lower galling tendency for surfaces with 10%
time following the same pattern as the smooth surface. The 20% dent density was observed. Galling is characterized as a form of
dent density presents a higher CoF value but with a linear trend. surface damage arising between sliding solids and is distinguished
The CoF behavior could be correlated with the lubrication and by microscopic, highly localized roughening and the creation of
dent density effect under the experiment region. The low viscosity protrusions.
lubricant under flooded condition will act mostly on removing Figures 9 and 10 present the calculated wear rate at high and
wear particles from the interaction zone with much less effect on low viscosity conditions. Wear rate for 20% density is higher than
sustaining the load. the wear rate for the smooth surface, and the wear rate for 10%
density is lower than the wear rate for the smooth surface. A good
Effect of Dent Arrays on Wear at Diffident Lubrication correlation with the CoF trend is established and proves that wear
Conditions. Figures 7 and 8 present representative wear track rate has a strong influence on metal friction behavior.
profiles at high and low viscosity conditions. The wear track pro- A similar conclusion regarding wear rate and CoF correlation
file is shallow but wider for tracks at high viscosity conditions and under low viscosity lubrication conditions could be drawn by
deep but thinner for tracks at low viscosity conditions. For low comparing results in Fig. 10 with Fig. 6(b).
viscosity lubricant conditions, the wear track is approximately
two times deeper when compared to maximum wear track depth Effect of Dent Arrays on AE Signals. AE energy was used to
at high viscosity lubricant conditions. The wear track at high vis- characterize the dent density effect on wear processes. The real
cosity conditions is approximately 1.52.5 times wider than the time recorded data were processed to reveal the trends and are
wear track for low viscosity lubricant. This behavior is owed to presented in Figs. 11 and 12.

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