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This standard has been approved for use by agencies of the Department of Defense.
Columbium-Alloy (UNS N06625), Nickel-Chromium- E 101 Test Method for Spectrographic Analysis of Alumi-
Molybdenum-Silicon Alloy (UNS N06219), and Nickel- num and Aluminum Alloys by the Point-to-Plane Tech-
Chromium-Molybdenum-Tungsten Alloy (UNS N06650) nique12
Rod and Bar5 E 120 Test Methods for Chemical Analysis of Titanium and
B 565 Test Method for Shear Testing of Aluminum and Titanium Alloys9
Aluminum-Alloy Rivets and Cold-Heading Wire and E 165 Practice for Liquid Penetrant Examination13
Rods4 E 227 Test Method for Optical Emission Spectrometric
D 3951 Practice for Commercial Packaging6 Analysis of Aluminum and Aluminum Alloys by the
E 8 Test Methods for Tension Testing of Metallic Materials7 Point-to-Plane Technique11
E 354 Test Methods for Chemical Analysis of High-
Temperature, Electrical, Magnetic, and Other Similar Iron,
1
Nickel, and Cobalt Alloys9
This specification is under the jurisdiction of ASTM Committee F16 on
Fasteners and is the direct responsibility of Subcommittee F16.04 on Nonferrous E 478 Test Methods for Chemical Analysis of Copper
Fasteners. Alloys9
Current edition approved Oct. 1, 2003. Published October 2003. Originally
approved in 1976. Last previous edition approved in 2003 as F 468 03.
2 8
Annual Book of ASTM Standards, Vol 02.01. Annual Book of ASTM Standards, Vol 14.02.
3 9
Annual Book of ASTM Standards, Vol 02.03. Annual Book of ASTM Standards, Vol 03.05.
4 10
Annual Book of ASTM Standards, Vol 02.02. Discontinued; see 1988 Annual Book of ASTM Standards, Vol 03.05.
5 11
Annual Book of ASTM Standards, Vol 02.04. Discontinued; see 2001 Annual Book of ASTM Standards, Vol 03.05.
6 12
Annual Book of ASTM Standards, Vol 15.09. Discontinued; see 1995 Annual Book of ASTM Standards, Vol 03.05.
7 13
Annual Book of ASTM Standards, Vol 03.01. Annual Book of ASTM Standards, Vol 03.03.
Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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3.1.7 Source inspection, if required (see Section 14); 5.1 Chemical CompositionThe fasteners shall conform to
3.1.8 Certificate of compliance or test report, if required the requirements as to chemical composition prescribed in
(see Section 16); Table 1 for the specified alloy.
3.1.9 Additional requirements, if any, to be specified on the 5.2 Manufacturers Analysis:
purchase order (see 4.2.1, 4.2.4, 7.3.1, 8.2, 11.1, and 12.1); 5.2.1 When test reports are required on the inquiry or
3.1.10 Supplementary Requirements, if any; and purchase order (see 3.1.8), the manufacturer shall make indi-
3.1.11 ASTM designation and date of issue. vidual analyses of randomly selected finished fasteners from
NOTE 2 Example the product to be shipped and report the results to the
10 000 pieces, Hex Cap Screw, 0.250 in.-20 3 3.00 in., Alloy 270. purchaser, except as provided in 5.2.2. Alternatively, if heat
Furnish Certificate of Compliance, Supplementary Requirement S1, and lot identities have been maintained, the analysis of the raw
ASTM F 468-XX. material from which the fasteners have been manufactured may
be reported instead of product analysis.
4. Materials and Manufacture 5.2.2 For aluminum fasteners, the manufacturer may furnish
4.1 Materials: instead a certificate of conformance certifying compliance with
4.1.1 The bolts, cap screws, and studs shall be manufactured the chemical composition specified in Table 1.
from material having a chemical composition conforming to 5.3 Product Analysis:
the requirements in Table 1 and capable of developing the 5.3.1 Product analyses may be made by the purchaser from
required mechanical properties for the specified alloy in the finished products representing each lot. The chemical compo-
finished fastener. sition thus determined shall conform to the requirements in
Table 1.
14 5.3.2 In the event of disagreement, a referee chemical
Annual Book of ASTM Standards, Vol 01.08.
15
Available from Global Engineering Documents, 15 Inverness Way, East analysis of samples from each lot shall be made in accordance
Englewood, CO 80112 with 11.1 and 12.1.
3
C61400 614 aluminum bronze 6.08.0 88.0D 1.53.5 1.0
C63000 630 aluminum bronze 9.011.0 78.0D 2.04.0 1.5 4.05.5 0.25 max 0.20 max
C64200 642 aluminum silicon bronze 6.37.6 88.65D 0.30 0.10 0.25 1.52.2E 0.50 0.05 0.20 max 0.15
C65100 651 silicon bronze 96.0D 0.8 0.7 0.82.0 1.5 0.05
C65500 655 silicon bronze 94.8D 0.8 1.5 0.6 2.83.8 1.5 0.05
F 468 03a
C66100 661 silicon bronze 0.25 max 94.0D 0.25 1.5 2.83.5 1.5 0.200.8
C67500 675 manganese bronze 57.060.0 0.82.0 0.050.5 balance 0.20 0.51.5
C71000 710 cupro-nickel 74.0D 0.60 1.00 19.023.0C 1.00 0.05
C71500 715 cupro-nickel 65.0D 0.400.7 1.00 29.033.0C 1.00 0.05
A
Elements shown as balance shall be arithmetically computed by deducting the sum of the other named elements from 100.
B
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Copper plus specified elements = 99.8 min; copper plus silver = 88.591.5.
C
Cobalt is to be counted as nickel.
D
Minimum content of copper plus all other elements with specified limits shall be 99.5 %.
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TABLE 1 Continued
Nickel and Nickel-Base Alloys
UNS
Man- Phos-
Designa- Car- Sili- Co
Al- General Alumi- Chro- A Iron, ga- A pho- Tita- Molyb- Sulfur, Vana- Tung-
tion bon, Copper Nickel con, balt,
loy Name num mium max nese, rus, nium denum max dium sten
Num- max max max
max max
ber
N10001 335 Ni-Mo 0.05 1.0 max 4.06.0 1.0 balance 0.025 1.00 2.50 26.030.0 0.030 0.20.4
N10276 276 Ni-Mo-Cr 0.02 14.516.5 4.07.0 1.00 balance 0.040 0.08 2.50 15.017.0 0.030 0.35 max 3.04.5
B
4
N04400 400 Ni-Cu Class A 0.3 balance 2.5 2.0 63.070.0 0.5 0.024
B
N04405 405 Ni-Cu Class B 0.3 balance 2.5 2.0 63.070.0 0.5 0.0250.060
B
N05500 500 Ni-Cu-Al 2.303.15 0.25 balance 2.0 1.5 63.070.0 0.5 0.350.85 0.01
N06625 625C Ni-Cr-Mo-Cb 0.40 0.010 20.023.0 5.0 0.50 58.0 min 0.015 0.50 0.40 max 1.00 8.010.0 0.015 3.24.2
max max max max
F 468 03a
N06686 686 Ni-Cr-Mo-W 0.010 19.023.0 5.0 0.75 balance 0.04 0.08 0.020.25 15.017.0 0.02 max 3.04.4
max max max max max
A
Elements shown as balance shall be arithmetically computed by deducting the sum of the other named elements from 100.
B
Cobalt is to be counted as nickel.
C
Alloy 625 material shall be refined using the electroslag remelting process (ESR), or the vacuum arc remelting process (VAR).
5
C
A92024 2024 Aluminum 2024 balance 0.10 max 3.84.9 0.50 0.300.9 0.50 0.15 0.25 1.21.8 0.05 0.15
A96061 6061 Aluminum 6061 balance 0.040.35 0.150.40 0.7 0.15 0.400.8 0.15 0.25 0.81.2 0.05 0.15
A97075 7075 Aluminum 7075 balance 0.180.35 1.22.0 0.50 0.30 0.40 0.20D 5.16.1 2.12.9 0.05 0.15
F 468 03a
A
Analysis shall regularly be made only for the elements specified in this table. If, however, the presence of other elements
is suspected or indicated in amounts greater than the specified limits, further analysis shall be made to determine that these elements are not present in excess of the specified limits.
B
Elements shown as balance shall be arithmetically computed by deducting the sum of the other named elements from 100.
C
Titanium + zirconium 0.20 %, max.
D
Titanium + zirconium 0.25 %, max.
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TABLE 1 Continued
Titanium and Titanium-Base AlloysA
UNS ResidualsB
Car- Nitro- Oxy- Molyb- Zirco- Sili Ruthe-
Des- General Alumi- Iron, Tita- Hydro- Palla- Vana- Chro- Tin, to-
Alloy bon, gen, gen, denum, nium, con, nium, each,
ignation Name num, Al Fe nium, Ti gen, H dium, Pd dium, V mium, Cr Sn tal,
C N O Mo Zr Si Ru max
Number max
R50250 1 Titanium Gr 1 0.10 0.20 balance 0.0125 0.05 0.18 0.1 0.4
R50400 2 Titanium Gr 2 0.10 0.30 balance 0.0125 0.05 0.25 0.1 0.4
R50700 4 Titanium Gr 4 0.10 0.50 balance 0.0125 0.07 0.40 0.1 0.4
R56400 5C Titanium Gr 5C 5.56.75 0.10 0.40 balance 0.0125 0.05 0.20 3.54.5 0.1 0.4
6
R56401 23 Titanium Ti-6Al-4V 5.56.5 0.08 0.25 balance 0.0125 0.05 0.13 3.54.5 0.1 0.4
ELI
R52400 7 Titanium Gr 7 0.10 0.30 balance 0.0125 0.05 0.25 0.120.25 0.1 0.4
R58640 19 Titanium Ti-38-6-44 3.04.0 0.05 0.30 balance 0.0200 0.03 0.12 0.10D 7.58.5 5.56.5 3.54.5 3.54.5 0.10D 0.15 0.4
R55111 32 Titanium Ti-5-1-1-1 4.55.5 0.08 0.25 balance 0.0125 0.03 0.11 0.61.4 0.61.2 0.61.4 0.61.40.060.14 0.1 0.4
F 468 03a
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A
All reported values are maximums, unless a range is specified.
B
A residual is an element present in a metal or an alloy in small quantities inherent to the manufacturing process but not added intentionally. Residual elements need not be reported unless a report is specifically required
by the purchaser.
C
Identical chemical requirements apply to both Class A and B as defined in Table 2 and 6.5.
D
Ruthenium and palladium, or both, may be added to Grade 19 for enhanced corrosion resistance as negotiated between purchaser and vendor. Chemical analysis is not required unless specifically required by the
purchaser.
Alloy Mechanical Nominal Thread HardnessA Full-Size TestsB Machined Specimen Tests
Property Diameter, in.
Tensile Yield Strength, Tensile Yield Strength Elongation in
Marking
Strength, ksi min, ksiC Strength, min, ksiC 4D, min, %D
min, ksi
Copper
Cu 110 F 468A all 6590 HRF 3050 10 30 10 15
Cu 270 F 468B all 5580 HRF 6090 50 55 50 35
Cu 462 F 468C all 6590 HRB 5080 25 50 25 20
Cu 464 F 468D all 5575 HRB 5080 15 50 15 25
Cu 510 F 468E all 6095 HRB 6090 35 55 30 15
Cu 613 F 468F $ 0.2500.500 7095 HRB 80110 50 80 50 30
0.6251.500 7095 HRB 75105 45 75 45 30
Cu 614 F 468G all 7095 HRB 75110 35 75 35 30
Cu 630 F 468H all 85100 HRB 100130 50 100 50 5
Cu 642 F 468J all 7595 HRB 75110 35 75 35 10
Cu 651 F 468K $ 0.250 to 0.750 7595 HRB 70100 55 70 53 8
0.8751.500 7095 HRB 5590 40 54 38 8
Cu 655 F 468L all 6080 HRB 5080 20 50 15 20
Cu 661 F 468M all 7595 HRB 70100 35 70 35 15
Cu 675 F 468N all 6090 HRB 5585 25 55 25 20
Cu 710 F 468P all 5085 HRB 4575 15 45 15 40
Cu 715 F 468R all 6095 HRB 5585 20 55 20 45
Nickel
Ni 335 F 468S all 2032 HRC 115145 45 115 45 35
Ni 276 F 468T all 2032 HRC 110140 45 110 45 25
Ni 400 F 468U $ 0.250 to 0.750 75 HRB25 HRC 80130 40 80 40 20
0.875 to 1.500 60 HRB25 HRC 70130 30 70 30 20
Ni 400 HFE F 468HF all 6095 HRB 70120 30 70 30 20
Ni 405 F 468V all 60 HRB20 HRC 70125 30 70 30 20
Ni 500 F 468W $ 0.250 to 0.875 2437 HRC 130180 90 130 90 20
1.000 to 1.500 2437 HRC 130180 85 130 85 20
Ni 625 F 468AC all 85 HRB35 HRC 120 60 120 60 30
Ni 686
Grade 1 F468BN all 2145 HRC 120165 85 120 85 20
Ni 686
Grade 2 F468CN all 2347 HRC 135185 125 135 125 20
Ni 686
Grade 3 F468DN all 2549 HRC 160200 150 160 150 15
Aluminum
Al 2024T4F F 468X all 7085 HRB 5570 36 62 40 10
Al 6061T6F F 468Y all 4050 HRB 3752 31 42 35 10
Al 7075T73F F 468Z all 8090 HRB 6176 50 68 56 10
TitaniumG
Ti 1 F 468AT all 140160 HV 3570 30 35 25 24
Ti 2 F 468BT all 160180 HV 5085 45 50 40 20
Ti 4 F 468CT all 200220 HV 80115 75 80 70 15
Ti 5 Class AH F 468DT all 3039 HRC 130165 125 130 120 10
Ti 5 Class BH F 468HT all 3039 HRC 130165 125 130 120 10
Ti 7 F 468ET all 160180 HV 5085 45 50 40 20
Ti 19 F 468FT all 2438 HRC 115150 115 120 115 15
Ti 23 F 468GT all 2536 HRC 120165 110 120 110 10
Ti-5-1-1-1 F 468HT all 2438 HRC 105150 90 100 85 10
A
Where both tension and hardness tests are performed, the tension tests shall take precedence for acceptance purposes. For aluminum and titanium alloys, hardness
tests are for information only. See 6.5.
B
The yield and tensile strength values for full-size products shall be computed by dividing the yield and maximum tensile load by the stress area for the product diameter
and thread pitch as given in table on tensile stress areas.
C
Yield strength is the stress at which an offset of 0.2 % gage length occurs.
D
Elongation is determined using a gage length of 4 diameters of test specimen in accordance with Test Methods E 8.
E
HF denotes a hot-formed product.
F
Aluminum alloy temper designations are in accordance with ANSI H35.1.
G
Full-size test mechanical properties apply to fasteners with a maximum diameter of 76 mm. Mechanical properties of larger sections shall be negotiated between the
material manufacturer and the fastener producer.
H
Ti 5 Class A requires wedge tensile testing in accordance with 6.6. Ti 5 Class B requires wedge tensile testing in accordance with 6.5.1.
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tensile (minimum and maximum) and yield strength properties bolts and cap screws threaded essentially to the head, the
in Table 2 for the specified alloy. wedge angle shall be 6 for sizes 0.750 in. in nominal diameter
6.3 Fasteners having a length equal to or longer than the and less and 4 for sizes over 0.750 in. in diameter.
minimum length of product requiring tension testing as 6.5.1 Ti5 Class B wedge angles shall be 6 for bolts and cap
specified in Test Methods F 606 and a breaking load exceeding screws of 0.750 in. nominal diameter and less and 4 for bolts
120 000 lbf shall preferably be tested full size and shall meet and cap screws over 0.750 in. in diameter. For bolts and cap
the full-size tensile (minimum and maximum) and yield screws threaded essentially to the head, the wedge angle shall
strength properties in Table 2. When equipment of sufficient be 4 for bolts and cap screws of 0.750 in. nominal diameter
capacity for such tests is not available, or if excessive length of and less and 2 for bolts and cap screws over 0.750 in. in
the bolts or stud makes full-size testing impractical, standard diameter.
round specimens shall be used which shall meet the machined 6.6 Where both tension and hardness tests are performed,
specimen tests tensile properties in Table 2. In the event of a the tension test results shall take precedence for acceptance
discrepancy between full-size and machined specimen tension purposes.
tests, full-size tests shall be used as the referee method to
determine acceptance. 7. Dimensions
6.4 For all alloys except aluminum and titanium, fasteners 7.1 Bolts and Hex Cap Screws:
that are too short (lengths less than that specified in Test 7.1.1 Unless otherwise specified, the dimensions of hex cap
Methods F 606 as the minimum length of product requiring screws (finished hex bolts), excluding silicon bronze alloy 651,
tension testing), that have insufficient threads for tension shall be in accordance with the requirements of ASME
testing (see 11.2), or that have drilled or undersized heads B18.2.1.
weaker than the thread section, are not subject to tension tests 7.1.2 Unless otherwise specified, the dimensions of silicon
but shall conform to the minimum and maximum hardness in bronze alloy 651 hex cap screws [finished hex bolt] shall be in
Table 2. Hardness tests are not applicable to aluminum and accordance with the requirements of ASME B18.2.1; or, the
titanium alloys. When required for aluminum alloys, a shear bolts and cap screws shall have a roll thread body diameter
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finish free of injurious burrs, seams, laps, irregular surfaces,
Copper E 53, E 54, E 62, E 75, E 478
and other imperfections affecting serviceability. Aluminum E 34, E 101, E 227
8.2 FinishUnless otherwise specified, the fasteners shall Nickel E 38, E 76, E 354
be furnished without an additive chemical or metallic finish. Titanium E 120, E 1409
12.2 Mechanical:
9. Sampling 12.2.1 When full-size tests are to be performed, determine
9.1 A lot, for the purposes of selecting test specimens, shall the yield strength, wedge tensile strength, and axial tensile
consist of not more than 100 000 pieces offered for inspection strength, as required by Section 6, on each sample in accor-
at one time having the following common characteristics: dance with the appropriate methods of Test Methods F 606.
9.1.1 One type of item (that is, bolts, hex cap screws, studs, 12.2.2 When machined specimen tests are necessary (see
and so forth), Section 7), determine the yield strength, tensile strength, and
9.1.2 Same alloy and temper, elongation on each sample in accordance with Test Methods
9.1.3 One nominal diameter and thread series, and E 8; and the shear strength (applicable to aluminum alloys
9.1.4 One nominal length. only) in accordance with Test Method B 565.
12.2.3 Determine the hardness in accordance with Test
10. Number of Tests and Retests Methods E 18 or E 92 at mid radius on the bottom of the
threaded end after suitable preparation. Make a minimum of
10.1 Number of TestsThe requirements of this specifica- two readings, each of which shall conform to the specified
tion shall be met in continuous mass production for stock. The requirements.
manufacturer shall make sample inspections as specified below
to ensure that the product conforms to the specified require- 13. Significance of Numerical Limits
ments. When tests of individual shipments are required,
13.1 For purposes of determining compliance with the
Supplementary Requirement S2 shall be specified.
specified limits for requirements of the properties listed in this
Acceptance Criteria
Number of Pieces Number Acceptance Rejection specification, an observed value or calculated value shall be
in Lot of Tests Number Number rounded in accordance with Practice E 29.
50 and under 2 0 1
51 to 500 3 0 1
14. Inspection
501 to 35 000 5 0 1 14.1 When specified on the inquiry or purchase order, the
35 001 to 100 000 8 0 1
product shall be subject to inspection by the purchaser at the
10.2 Retests: place of manufacture before shipment. The inspector represent-
10.2.1 When tested in accordance with the required sam- ing the purchaser shall have controlled entry only to those parts
pling plan, a lot shall be subject to rejection if any of the test of the manufacturers operations that concern the manufacture
specimens fails to meet the applicable test requirements. of the ordered product and only when and where work on the
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16. Certification and Test Reports or be plainly marked with the following:
17.3.1 ASTM designation,
16.1 Certificate of ComplianceWhen specified in the 17.3.2 Alloy number,
contract or purchase order, the manufacturer shall furnish 17.3.3 Alloy/mechanical property marking,
certification that the product was manufactured and tested in 17.3.4 Size,
accordance with this specification and conforms to all specified 17.3.5 Name and brand or trademark of the manufacturer,
requirements. 17.3.6 Number of pieces,
16.2 Test ReportsWhen shipment lot testing in accor- 17.3.7 Country of origin, and
dance with Supplementary Requirement S3 is specified in the 17.3.8 Purchase order number.
contract or purchase order, the manufacturer shall furnish a test
report showing the results of the mechanical tests for each lot 18. Keywords
shipped. 18.1 bolts; cap screws; general use; nonferrous; studs
SUPPLEMENTARY REQUIREMENTS
One or more of the following supplementary requirements shall apply only when specified by the
purchaser on the inquiry, contract, or order. Supplementary requirements shall in no way negate any
requirement of the specification itself.
S1. Stress Corrosion Requirements S2.2 The manufacturer shall make an analysis of a ran-
S1.1 Copper AlloysCopper alloy fasteners shall exhibit no domly selected finished fastener from each lot of product to be
evidence of cracking after immersion for 30 min in an aqueous shipped. Heat or lot control shall be maintained. The analysis
solution of mercurous nitrate when tested in accordance with of the starting material from which the fasteners have been
Test Method B 154. manufactured may be reported in place of the product analysis.
S1.1.1 WarningMercury is a definite health hazard and S2.3 The manufacturer shall perform mechanical property
equipment for the detection and removal of mercury vapor tests in accordance with this specification and Guide F 1470 on
produced in volatilization is recommended. The use of rubber the individual lots for shipment.
gloves in testing is advisable. S2.4 The manufacturer shall furnish a test report for each lot
S1.2 7075-T73 Aluminum AlloyFor aluminum alloy in the shipment showing the actual results of the chemical
7075-T73 fasteners, the resistance to stress corrosion cracking analysis and mechanical property tests performed in accor-
shall be established by testing the previously selected tension dance with Supplementary Requirement S2.
test specimens to the electrical conductivity-yield strength
S3. Dye Penetrant Inspection
criteria listed in 12.2 of Specification B 211. When the fasten-
ers are too short to permit tension testing, suitable lengths of S3.1 When dye penetrant inspection is specified on the
the stock used to produce the fasteners shall be heat treated purchase order, the fasteners shall be tested in accordance with
with the fasteners and tested to the electrical conductivity-yield Practice E 165 or other mutually acceptable procedures, and
strength criteria. The conductivity shall be determined in shall conform to acceptance criteria as mutually agreed upon
accordance with Test Method B 193. by the purchaser and manufacturer.
S2. Shipment Lot Testing S4. Heat Control (Alloys 400, 405, and 500 Only)
S2.1 When Supplementary Requirement S2 is specified on S4.1 When Supplementary Requirement S4 is specified on
the order (see 3.1.6), the manufacturer shall make sample tests the inquiry or order, the manufacturer shall control the product
on the individual lots for shipment to ensure that the product by heat analysis and identify the finished product in each
conforms to the specified requirements. shipment by the actual heat number.
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of infringement of such rights, are entirely their own responsibility.
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if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
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