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Minerals Engineering 41 (2013) 916

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Minerals Engineering
journal homepage: www.elsevier.com/locate/mineng

Assessing the stirred mill design space


Peter Radziszewski
Department of Mechanical Engineering, Comminution Dynamics Lab, McGill University, 817 Sherbrooke Str. West, Montreal, Quebec, Canada H3A 0C3

a r t i c l e i n f o a b s t r a c t

Article history: In the context of the mining industry, smaller grain size and other mineralogical characteristics have
Received 19 April 2012 motivated the need to grind ner. In order to address this need, the interest in ne grinding technologies
Accepted 2 October 2012 has grown over the last 20 years as is illustrated by a growing body of knowledge on stirred milling.
Available online 4 December 2012
Emphasis in recent years has been on the use of computationally intensive modeling and simulation
methods such as the discrete element method (DEM) and computational uid dynamics (CFDs). However,
Keywords: due to the computational requirements of these two methods, initiating a study that spans the stirred
Stirred mills
mill design space would take a lot of computational effort and time. Therefore the goal of this paper is
Shear
Design
to propose and apply a simplied stirred mill model that will then be used to assess congurations in
Power the stirred mill design space.
To this end, a stirred mill model was proposed based on the assumption that the main if not only mech-
anism of ore breakage is shear. As the basis of this model is the uid mechanics denition of shear stress,
the stirred mill power model became a function of viscosity, mill speed and a new parameter called shear
volume. An initial validation using published data indicated the shear based power model correlated well
with measured power.
Establishing a morphological chart to delimit the stirred mill design space indicated that 24 design and
operating conditions can be assess using the established shear volume measure. The results indicated for
the mill congurations tested that a change in stirred mill liner design can potentially increase shear vol-
ume and power from 14% to 290% as compared to smooth chamber liners.
2012 Elsevier Ltd. All rights reserved.

1. Introduction 1998), particle motion (Barley et al., 2004; Blecher and Schwedes,
1996; Conway-Baker et al., 2002; Theuerkauf and Schwedes, 1999;
Stirred mill technology dates back to 1928 (Stehr, 1988) Thyn and Pokorny, 1980) and energy/mass point-of-view (Becker
where the idea to use an agitator and spherical grinding media and Schwedes, 1999; Becker et al., 2001; Bel Fadhel and Frances,
was presented. The year 1948 saw the successful application of 2001; Blecher et al., 1996; Gao and Forssberg, 1993, 1995; Janko-
Du Ponts sand mill for pigment grinding. Subsequent years vic, 2001, 2003; Kapur et al., 1996; Keuhen et al., 1988; Kheifets
have led to the development of different types of stirred mills and Lin, 1998; Kwade and Schwedes, 2002; Kwades, 1999a,b;
spanning a number of industries that require ne and ultrane Kwades et al., 1996; Mankosa et al., 1986, 1989; Mende et al.
grinding. 2003; Neese et al., 2004; Nesset et al., 2006; Sadler et al., 1997; Tu-
In the context of the mining industry, smaller grain size and zun et al., 1995; Wang and Forssberg, 2000; Weller, 1996; Zheng
other mineralogical characteristics have motivated the need to et al., 1996) with only one paper covering the interactive subjects
grind ner. In order to address this need, the interest in ne grind- of power consumption, ore grinding and media wear (Becker and
ing technologies has grown over the last 20 years as can be illus- Schwedes, 1999). Focusing on the works treating mill performance,
trated by the large body of literature published over this same these papers can be paired down to those where energy in grinding
period of time. These studies address the stirred mill characteriza- was either calculated from typically a volume based procedure
tion from a mass balance (Baudet et al., 1999; Bel Fadhel et al., leading to stress intensity (Becker and Schwedes, 1999; Blecher
1999; Bernhardt et al., 1999; Berthiaux et al., 1996a,b; Berthiaux, et al., 1996; Kheifets and Lin, 1998; Kwades, 1999a,b; Kwades
2000; Cho et al., 1996; Frances et al., 2001; Muller et al., 1999; Siv- et al., 1996; Kwade and Schwedes, 2002) or measured directly
amohan and Vachot, 1990; Stehr, 1984; Varinot et al., 1997, 1999; (Becker et al., 2001; Bel Fadhel and Frances, 2001; Gao and Forss-
Weller et al., 2000; Yue and Klein, 2004, 2005a,b; Zhenhua et al., berg, 1993; Jankovic, 2003; Keuhen et al., 1988; Mankosa et al.,
1986; Mende et al., 2003; Nesset et al., 2006; Sadler et al., 1997;
Tel.: +1 514 398 6282; fax: +1 514 398 7365. Tuzun et al., 1995; Wang and Forssberg, 2000; Weller, 1996; Zheng
E-mail address: peter.radziszewski@mcgill.ca et al., 1996).

0892-6875/$ - see front matter 2012 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.mineng.2012.10.012
10 P. Radziszewski / Minerals Engineering 41 (2013) 916

This body of knowledge indicates that there are a number of de-


sign and operating parameters that affect stirred mill performance.
These include but are not limited to impellor type, tip speed, media
size, impellor tip to mill wall gap size, lling, slurry rheology, med-
ia and slurry density, solid concentration and slurry ow.
Emphasis in recent years has been on the use of computation-
ally intensive modeling and simulation methods such as the dis-
crete element method (DEM) (Martins et al., 2011; Mishra and
Rajamani, 1990, 1992, 1993a,b; Sinnot et al., 2006, 2011; Clear Fig. 1. Shear between two parallel plates sliding past one another.
et al., 2006); Jayasundara et al., 2006, (Jayasundara et al., 2008,
2009, 2010, 2011) and computational uid dynamics (CFDs) (Eskin
et al., 2005; Gers et al., 2010; Lane, 1999; Vuthaluru et al., 2006). sliding or shear stress (s) is a function of a parameter known as vis-
However, due to the computational requirements of these two cosity (l) and the velocity (u) over the uid thickness (y):
methods, initiating a study that spans the stirred mill design space
u
would take a lot of computational effort and time. Therefore the sl 3
goal of this paper is to propose and apply a simplied stirred mill
y
model that will then be used to assess congurations in the stirred In a rotating system, such as a rotating concentric viscometer
mill design space. (Streeter and Wylie, 1979), the same description can be made as
illustrated in Fig 2. In this particular case, the sliding velocity (u)
2. Dening a performance metric is a product of the angular rotation speed (x) and the radius of
the surface (r) resulting in the shear stress expression being mod-
In a thorough analysis, Kwade et al. (Blecher et al., 1996; Kwade ied to:
et al., 1996; Kwade, 1999a,b; Kwade and Schwedes, 2002) devel- xr
oped a stress intensity relationship by using dimensional analysis. sl 4
y
This relationship has been used extensively to evaluate grinding
performance in operating stirred mills (Jankovic, 2001). As pre- If the surface over which the shear stress is applied to is known,
sented, the stress intensity relationship produces a value, SIr, has it becomes possible to determine the force acting on that surface.
the units of energy (Nm). Typically, multiplying such a value with In the case of a rotating system, the resulting force would dene
the angular rotation speed of the impellor, x, would produce a va- the torque acting on the system as:
lue having the units of power (W) which should relate to measured xr 2
power through the use of a correlation factor, fr, giving the follow- T sAr lA Nm 5
y
ing relationship:
Assuming that all shear surfaces are in contact with the shear-
Pr fr SIr x W 1 ing uid, the power needed to turn that cylinder can be determined
where: as follows:
x2 r 2
SIr D3b qm  qsl m2 2 P s T x lA W 6
y
Db is the media diameter m It will be assumed that Eq. (6) is applicable to dening the
power being consumed in a stirred mill. Grouping the area over
qm is the media density kg=m3 which shear is acting, A, the radius at which the shear is acting,
r, and the gap over which shear is acting, y, produces a value that
qsl is the slurry density kg=m3 has cubic meters for its units and will therefore be known as the
shear volume. It is dened as follows:
m is the stirrer tip speed m=s r2
Vs A m3 7
In examining the resulting power relationship (Eq. (1)), it be- y
comes evident that it would be of limited use in the assessment This allows the redenition of mill power (Eq. (6)) as a function
and comparison of different stirred mill design congurations be- of shear volume as:
cause only operating parameters are used in this denition of mill
power. Ideally, a design performance metric would include ele- Ps lx2 V s W 8
ments of the physical dimensions of the mill being assessed. As a
result, an effort to re-examine the development of a stirred mill
model is motivated.
As such and for the purposes of simplicity, it will be assumed
that the only mechanism of ore breakage in a stirred mill is
through two media particles sliding past one another, nipping
some ore and, depending on the speed and applied force, breaking
that nipped ore. This sliding mechanism also applies to layers of
media particles sliding past one another grinding any ore found be-
tween these layers. Whether it is limited to single particles or slid-
ing layers of particles, the predominant ore breakage mechanism is
shear.
From a uid mechanics point of view, shear typically is de-
scribed by two parallel plates sliding past one another and sepa-
rated by a uid of a given thickness (see Fig. 1). The resistance to Fig. 2. Shear between concentric cylinders.
P. Radziszewski / Minerals Engineering 41 (2013) 916 11

Applying these relationships to a stirred mill would require not In the general case where there are several different parallel
only the knowledge of the physical dimensions of the impellor and shear surface pairs, the shear surface calculation would take the
chamber, but also a determination of all parallel shear surfaces that form of a summation:
are in contact with the uid media.
Xn
r2
In any given stirred mill there are number of parallel or near Vs Ai i 10
parallel surfaces. However, only the parallel surfaces moving past i0
yi
one another would be admissible as parallel shear surfaces. This
criterion means that parallel surfaces on the impellor, such as where n is the number of parallel shear surface pairs in a stirred
the surfaces of two adjacent disks, would not be admissible as mill.
these two surfaces are moving at the same rotation speed. How-
ever, the circumferential surface on the disk is parallel to the mill 3. Calibrating the performance metric
chamber wall and is denitely moving past the stationary mill
chamber wall. Therefore these parallel surfaces are a parallel shear In the proposed model, one performance metric was presented
surface pair. Further, the surface of a disk found at the bottom or which is shear volume. However, the effect of shear volume can
end of an impellor shaft would be parallel to the bottom of the mill only be evaluated in relationship to mill power consumption which
and would also constitute a parallel shear surface pair. requires the use of mill power consumption data.
As a general guideline, if one parallel surface is found on the In 1996, Gao et al. (1996) presented a paper on the development
rotating impellor and the other is parallel surface is found on or at- of an empirical power model for a horizontal stirred mill from a de-
tached to the chamber, then these two surfaces would be consti- sign of experiments involving 27 different operating points. As the
tute a parallel shear surface pair. proposed power model is not a function of gravity and that it is ex-
This can be illustrated using the following example of a single pected that the mill charge is centrifuged during operation of the
disk impellor in a 1 m diameter  1 m media height chamber mill, it is assumed that this data set is a good data set for initial
(see Fig. 3) where there are three parallel shearing surfaces to be model validation.
considered. The shear volume, Vs, is calculated using Eq. (10) with a note
The rst one is the disk circumference side (a), the second is the that the shaft is assumed not to be in contact with the shearing
shaft surface (b) and the third is the circular end (c) (see Fig. 3). uid. The result is a shear volume of 0.006407 m3.
Therefore, the shear volume calculation needs to include the shear Assuming that the shear based power, Ps, is equal to the actual
volume contribution of all three of these parallel shear surfaces as mill power, Pmill, it should be possible to back calculate the viscos-
follows: ity of the mill media/slurry mix as follows:
r 2disk r2shaft r2 Pmill
V s Adisk Ashaft Aend end 9 lbc Ns=m2 11
ydisk yshaft yend x2 V s
where r end r disk  21= 2. The average of the viscosity, l
 , over the 27 data points leads to a
Note that the radius, rend, is determined from integrating shear rst correlation between shear based power and measured mill
stress over the disk end area leading to the rend result as a function power as illustrated in Fig. 4. Although the graph in Fig. 4 indicates
of the disk radius. that there is a correlation between measured and estimated power,
It should be noted that all parallel shearing surfaces should be the correlation is rather weak. However, this correlation clearly
in contact with the shearing uid in order to be considered. In underlines the inuence of rotation speed on the mills power
Fig. 3, the shear volume is presented for both the case where the consumption.
shaft surface is considered in contact with the uid and where it This correlation can be improved by observing that the viscosity
is not considered in contact. It is interesting to note that the shaft is also a function of the rotational speed of the mill as shown in
contribution to shear volume is small for this case. Fig. 5.

Fig. 3. Example of shear volume calculation.


12 P. Radziszewski / Minerals Engineering 41 (2013) 916

Fig. 4. First correlation between shear power and measured power.

Fig. 6. Stirred mill power correlation with Gaos data set (Gao et al., 1996).

Fig. 5. Viscosity as a function of rotation speed.

Fig. 7. Stirred mill power comparison.


Using the trend relationship in Fig. 5 along with the general
form of Gaos empirical power model (Gao et al., 1996), it becomes 4. Performance metric validation
possible to propose a generalized form for a stirred mill viscosity
model as follows: Keeping in mind that that goal of the development of this shear
based stirred mill model is to dene a metric that can be used to
evaluate the design parameters of a given mill, it becomes impor-
tant to nd an initial validation data set for a stirred mill of a dif-
ferent geometry than the one used by Gao et al. (1996). To this end,
the work of Jankovic (1998) provides a large experimental data set
for a lab scale tower and Sala (pin) mill. Most of the physical
dimensions and operating parameters were included in the work
as well as measured power consumption with the exception of
tower mill auger thickness. From the physical specications of
the mills, it was possible to determine the shear volume for each.
Assuming the auger thickness is 1 mm, the shear volume for the
tower mill is 0.0004 m3. For the pin mill, the shear volume is
12 0.0015 m3.
Using these shear volume results along with the associated
The reference values are: operating parameters, it was possible to predict mill power using
Eqs. (8) and (13) and compare these results with the measured stir-
Dbref 0:00205 m; qmref 7:8 g=cc; qslref 1 g=cc red mill power for these two mills. Plotting these results on those
found in Fig. 6 (see Fig. 7) indicate that the power predictions for
It is important to note that this model provides a baseline vis-
the tower and Sala mills generally fall into line with the previously
cosity value which is a function of rotation speed. Subsequently,
calibrated results.
this baseline value is corrected using power functions of adimen-
More importantly, this comparison indicates that the shear
sional ratios.
based power model provides an estimate of the power consump-
Applying this model to Gaos data set (Gao et al., 1996) and the
tion of the mills as a function of both the physical design and oper-
associated reference values, it is possible to determine which con-
ating parameters. This observation conrms that the shear based
stants and exponents reduce the error between the measure power
power model and its components are sufciently sensitive to
and the predicted power. These are:
changes in impellor design and therefore can be used to assess dif-
ferent stirred mill design congurations.
k 0:0199; a 566:04; b 0:571; c 3:5761; d 0:2; e
5; f 4:0188:
5. Stirred mill design space
The resulting correlation between the shear power estimate and
the measured power estimate is quite good with an R2 value of All stirred mills are composed of four components which are
0.9654 and can be found in Fig. 6. (Fig. 8) the motor/transmission, the impellor, the chamber and
P. Radziszewski / Minerals Engineering 41 (2013) 916 13

chamber wall is modied with protrusions such as pins. As such,


one can add similar protrusions to the chamber as found on an
impellor: pins and disks. Also, there is some interest in the devel-
opment of annular gap mills (Reinsch et al., 1991; Orumwense,
1992; Stender et al., 2004). The resulting morphological chart (Ta-
ble 2) delimits the stirred mill design space to be assessed.

6. Design space assessment

Examining the stirred mill design space as described in Table 2,


there are a couple of alternatives that will not be assessed. The rst
is the horizontal mill orientation as it is assumed that mill opera-
tion of disk or pin mills will ensure that the mill charge is well cen-
trifuged. The second is the shear uid which will be assumed to be
Fig. 8. Sketch of the main components of a stirred mill.
homogenous with equal slurry and bead densities (1000 g/cc), a
bead size equal to the reference size and no viscosity modifying
additives (x = 0). The resulting design space to assess reduces from
the mill charge. Each of these components fullls a particular func-
a possible 144 possible congurations to 36 (three speeds, four
tion. Essentially, motor/transmission converts electrical energy
impellors, three containment structures). However, only the
into mechanical energy dened by rotation speed and torque.
smooth liner containment structure will work with the screw
The mechanical energy is transferred to the charge by the impellor
and drum impellors. Therefore only 24 design combinations (eight
and the mill charge transfers that energy to the ore through com-
designs and three speeds) will be assessed.
minution. The chamber is a containment system in which all of
The containment chamber is 1 m diameter and a media depth of
these components can be found.
1 m. The three rotation speeds used for the assessment are
The components and their variations can be laid out in the mor-
100 rpm, 500 rpm and 1000 rpm.
phological chart found in Table 1. From this chart, one can easily
The eight design combinations are found in Fig. 9 with the asso-
reconstruct the different stirred mills commercially available to
ciated results for shear volume as well as power in Table 3.
the mining industry.
A number of observations can be made from the results pre-
However, with shear being assumed to be the main grinding
sented in Table 3. These are:
mechanism, there is room to propose that a stirred mill can actu-
ally be dened by seven sub-functions as follows: in any orienta-
(i) The shear volume increases from a low for the pin impellor
tion, the motor/transmission converts electrical energy into
only to a high with the drum impellor only.
mechanical energy dened by rotation speed and torque. The
(ii) Although the pin impellor mill has a lower shear volume
mechanical energy is transfer to an impellor structure which then
than the screw impellor mill for this scale of mill, it is oper-
transfer this energy through a 1st shear surface to the mill uid.
ated at a higher rotation speed resulting in higher power
The uid in turn transfers a portion of that energy through to the
consumption than the screw impellor mill as seen in litera-
2nd shear surface to the containment structure.
ture (Jankovic, 1998).
In this modied list of sub-functions, comminution is removed
(iii) The additions of protrusions such as pins and then disks to
as it is actually part of the multi-phase uid system which is com-
the chamber liners increases the shear volume by 32% and
posed of water, media and ore.
210% respectively for the pin mill shown.
Before redistributing the different stirred mill alternative com-
(iv) The additions of protrusions such as pins and then disks to
ponents in a modied morphological chart, it might be of interest
the chamber liners increases the shear volume by 29% and
to expand the possible alternatives with those indicated in the re-
55% respectively for the disk mill shown.
view of Stehr (1988). In this review of high speed stirred milling
(v) The drum impellor which represents the annular gap mill
technologies it is indicated that in some cases the containment
shows the greatest shear volume and associated mill power.

Table 1
Initial morphological chart for a stirred mill.

Function Alternative components


Energy conversion Motor-transmission (low speed) Motor-transmission (med. speed) Motor-transmission (high speed)
Energy transfer Screw impellor Pin impellor Disk impellor
Comminution Iron media Ceramic media Sand Pebbles
Containment Vertical chamber Horizontal chamber

Table 2
Modied morphological chart for stirred mill development.

Function Alternatives
Orientation Vertical Horizontal
Energy conversion Low speed Medium speed High speed
Impellor shape Disk impellor Screw (augar) impellor Pin impellor Drum impellor
1st shear surface Parallel surface
Shear uid Homogeneous Multi-phase
2nd shear surface Parallel surface
Containment structure Smooth liner Disk liner Pin liner
14 P. Radziszewski / Minerals Engineering 41 (2013) 916

Fig. 9. Stirred mill design combinations.

Table 3
Shear volumes and shear power for the stirred mills in Fig. 9.

Shear volume (m3) Shear power (100 rpm) (kW) Shear power (500 rpm) (kW) Shear power (1000 rpm) (kW)
3  6 Pin impellor 0.114 0.037 0.367 0.989
Pin on pin 0.150 0.048 0.483 1.301
Pin on disk 0.355 0115 1.143 3.078
Screw impellor 0.466 0.151 1.502 4.044
3 Disk impellor 1.618 0.523 5.213 14.037
Disk on pin 2.079 0.672 6.699 18.038
Disk on disk 2.503 0.809 8.066 21.720
Large diameter drum 4.021 1.299 12.957 34.888

7. Discussion Further, the ratio of shear volume to mill volume can poten-
tially be considered as a measure of shear intensity of a particu-
There are a number of points that should be underlined from lar mill design. The product of such a shear intensity ratio or
the results obtained starting with the design performance metrics factor with the square of the rotation speed and the viscosity
dened and used. of the slurry/media mix would equal the power intensity of the
Shear volume is a new parameter that is based on a uid mill.
mechanics description of shear stresses in a stirred milling. It is A point should be made on the comparison of the shear based
developed from the design parameters of a given mill. Along with power model with the empirical model developed by Gao et al.
mill rotation speed and viscosity it is possible to estimate mill (1996). The complete shear based power model which combines
power consumption. Eq. (8) with viscosity (Eq. (13)) with the exponents is presented
It is interesting to note that the shear volume of a given mill can here:
be greater than the physical volume of that mill. This is mainly due
 2 !0:2 !2  4
to the fact that the shear volume is a function of the inverse of the Db qm qsl 100  x
gap distance between the impellor and the mill chamber wall. Ps kax0:571 x2 V s
Db ref qm ref qsl ref 100
Essentially, as the gap distance decreases, the shear volume
increases. 13
P. Radziszewski / Minerals Engineering 41 (2013) 916 15

The Gao power model is reproduced here: lished data indicated that power dened as a function of shear cor-
related quite well with the measured power for the cases tested.
PGao 109:29 N1:429 q0:18 2:9 0:096
m qsl x 14 The proposed model divides the mill power calculation into
three distinct parts of physical, operating and uid parameters.
The differences between the two models are apparent. How-
The shear volume, Vs, denes the physical arrangement of the
ever, the form of these two models is very similar. The order of
impellor and mill chamber. The mill operating parameter is de-
the exponents related to media and slurry density is similar. Fur-
ned by the impellor rotation speed. The shear uid is described
ther and more importantly, the exponent on the rotation speed
by the viscosity. The form of this proposed model is relatively
in the two equations is identical. In the shear based power model
simple.
(Eq. (14)), the aggregate exponent on the rotation speed is (2
Establishing a morphological chart to delimit the stirred mill
0.571) 1.429 which is the same in Gaos model. This is indeed reas-
design space indicated that 24 design and operating conditions
suring especially that this result was arrived at from two different
can be assess using the established shear volume measure. The re-
directions.
sults indicated for the mill congurations tested that a change in
Despite this promising observation, further investigation and
stirred mill liner design can potentially increase shear volume
validation of this model using experimental data for different stir-
and power from 14% to 290% as compared to smooth chamber
red mill congurations and operating conditions is required.
liners.
It is expected that with such added investigations, viscosity as a
It is apparent that further research is required to validate the
function of rotation speed would be corrected not only with re-
power model based on the shear volume denition against indus-
spect to media diameter, media density, slurry density and viscos-
trial power data as well as computational models of stirred milling
ity thinners, but also with respect to other parameters such as
before it can be considered for use with condence to predict stir-
viscosity thickeners, slurry temperature, ore granulometry and
red mill power. Such validation will contribute to determining and
gravity effects.
conrming how viscosity is affected by the media diameter, media
With respect to ore granulometry, it has been shown to affect
density, media size distribution, slurry rheology, slurry solid con-
the power in an Nesset et al. (2006). However, it has been indicated
tent, slurry density, etc. Undoubtedly, viscosity will also be found
that in a mill such as the horizontal mill used by Gao et al. (1996),
to be a function of the granulometry which will require tying the
ore granulometry has little effect on power consumption. This
power model dened from shear stress with either and energy-size
should require tying the power model dened from shear stress
relationship or a breakage kinetics relationship.
with either an energy-size relationship or a breakage kinetics rela-
If successful, the use of this model could contribute to the
tionship to estimate the evolving ore granulometry in a given mill.
development of a better understanding of how different design
It is clear from the results presented in Table 3 that the addition
parameters work together to produce the power required in any
of protrusions to the containment chamber such as pins or disks
particular stirred milling operation.
can improve the shear volume and associated mill power in a given
mill ranging from 14% to almost 300% for the mills congurations
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