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SKL 1033
Separation
Techniques in
Chemistry
INSTRUCTIONAL PLAN
Department of Chemistry
Faculty of Science and Mathematics
Sultan Idris Education University
Date:
INSTRUCTIONAL PLAN
LECTURERS INFORMATION:
COURSE SYNOPSIS :
This course introduces the principles and theory of separation techniques includes
distillation, filtration, evaporation, chromatography, solvent extraction, centrifugation,
fractional distillation, crystallization and solid phase extraction.
(Kursus ini memperkenalkan prinsip dan teori teknik pemisahan termasuk penyulingan,
penapisan, penyejatan, kromatografi, pengekstrakan pelarut, emparan, penyulingan
berperingkat, penghabluran dan pengekstrakan fasa pepejal)
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RATIONALE OF THE COURSE:
This course provides principals and theories of knowledge of separation techniques such as
distillation, filtration, evaporation, chromatograph, solvent extraction, centrifugation,
fractional distillation, crystallization and solid phase extraction.
Kursus ini menyediakan pengetahuan prinsip dan teori teknik pemisahan seperti
penyulingan, penapisan, penyejatan, kromatografi, pengekstrakan pelarut, emparan,
penyulingan berperingkat, penghabluran dan pengekstrakan fasa pepejal.
LEARNING OUTCOMES:
TRANSFERABLE SKILLS:
Skills in this course are developed through individual, group assignments and practical skills.
Skills are assessed through coursework including report, presentation and group
participation.
REFERENCES:
1. Steve, T. & Richard, W. (2006). Solid/Liquid separation: Equipment selection and process
design. Oxford, UK: Elsevier Science.
2. Christian, G.D. (2004). Analytical chemistry. (6th Ed.). New York, USA: John Wiley.
3. Skoog, D.A., West, D.M., Holler, F.J., & Crouch, S.R. (2003). Fundamental of analytical
chemistry. (8th Ed.). Forth Worth, New York, USA: Brooks Cole.
4. Nigel J.K. S. (200). Solid-Phase Extraction: Principles, Techniques, and Applications,
New York: Varian Inc.
5. Ramli Ibrahim, Illyas Md Isa & Anuar Kassim. (2003). Kimia analisis, Tanjong Malim:
Penerbit UPSI.
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OF SOFT SKILLS EMBEDDED:
Abbreviation Skills
KOM Communication Skill
BKMM Critical Thinking and Problem Solving Skills
PBPM Continuous Learning and Information Management
KKBP Team Work Skills
KKU Entrepreneurial Skills
KKP Leadership Skill
EM Professional Ethics and Moral
GRADING SCALE:
3/8
B- 60 64 2.75
C+ 55 59 2.50
C 50 54 2.00
C- 45 49 1.75
D+ 40 44 1.50
D 35 39 1.00
F 0 34 0
Scale
4 Excellent
3 Good
2 Moderate
1 Weak
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WEEK TEACHING SCHEDULE:
*Optional
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3.0 Chromatography LO1, LO2,LO3 & LO4 EM Lecture &
Practical
Formative
4-5 Type of chromatography. Selection of stationary
and mobile phases. Mobile phase manipulation
and optimization strategies.
6.0 Crystallization
Theory of crystallization, crystallization as KKBP Lecture
LO1 Formative
9-11 separation techniques, procedures and
experimental set-up, application in research and
industries.
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TUTORIAL/LAB/WORKSHOP PLAN
2 Thin Layer LO2, LO3 & PBPM, KKBP, Demonstration and Formative
Chromatography (TLC) LO4 KKP & EM Practical
3 Isolation Caffeine From LO2, LO3 & PBPM, KKBP, Demonstration and Formative
Tea Leaves LO4 KKP & EM Practical (2weeks)
4 Distillation- Separation LO2, LO3 & PBPM, KKBP, Demonstration and Formative
of Mixture LO4 KKP & EM Practical
Reminder: (optional)
1. Students attendance to all lectures, tutorials and lab works is compulsory
2. Students with total of attendance of less than 80% can be barred from taking final examination
3. Any absence due to health problem must be corroborated with a medical certification from Pusat Kesihatan Pelajar UPSI, UPSIs Panel clinics
or Clinic/Government Hospital.
4. Absence due to other problems must be justified using a show cause letter.
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