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International Journal of Impact Engineering 45 (2012) 28e38

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International Journal of Impact Engineering


journal homepage: www.elsevier.com/locate/ijimpeng

Tensile behaviour of high performance bre-reinforced cementitious composites


at high strain rates
Alessio Caverzan a, *, Ezio Cadoni b, Marco di Prisco a
a
Department of Structural Engineering (DIS), Politecnico di Milano, Milan, Italy
b
Department of Environment, Constructions and Design, University of Applied Sciences of Southern Switzerland, Lugano, Switzerland

a r t i c l e i n f o a b s t r a c t

Article history: The promise of bre-reinforced cementitious composites for dynamic loading application stems from
Received 25 October 2010 their observed good response under static loading. An experimental research aimed at contributing to
Received in revised form the understanding of the behaviour of advanced bre-reinforced cementitious composites subjected to
29 November 2011
low and high strain rates was carried out. The material behaviour was investigated at four strain rates
Accepted 18 January 2012
Available online 2 February 2012
(0.1, 1, 150 and 300 s1) and the tests results were compared with their static behaviour. Tests at
intermediate strain rates (0.1e1 s1) were carried out by means of a hydro-pneumatic machine (HPM).
High strain rates (150e300 s1) were investigated by exploiting a Modied Hopkinson bar (MHB).
Keywords:
High performance bre-reinforced
Comparison between static and dynamic tests highlighted several relevant aspects. First, with the change
cementitious composites in the strain rate, the Dynamic Increase Factor (DIF) of the material appears well predicted by some
HPFRCC models proposed in the literature up to a value of 0.1 s1, while at higher strain rates it increases less than
High strain rates expected from models. Moreover, the post-peak behaviour showed a stress plateau inuenced by the
Dynamic behaviour bres and dependent on the strain rate.
Hopkinson bar 2012 Elsevier Ltd. All rights reserved.

1. Introduction Banthia [2], Banthia et al. [3], Bentur et al. [4] and Ross [5] reported
a reduced value of the ratio between dynamic and static strength
The mechanical behaviour of bre-reinforced cementitious with a growing of static strength of concrete, while in the results
composites when subjected to impact or blast still has many reported by Bischoff and Perry [6] that ratio is independent of static
aspects open to investigation [1], with specic reference to large strength.
and socially-sensitive structures, as sheltering structures, high-rise High performance bre cementitious composites are charac-
buildings, bridges, off-shore platforms, pipelines, gasication terised by high toughness and a hardening behaviour in bending.
reactors, secondary containment shells for nuclear power plants, Fibres enhance the ductility of brittle materials like concrete, and
and tunnels. For such reasons, the mechanical response of concrete this improvement is strictly related to the process by which the load
structures exposed to blast and impact loading can only be is transferred from the matrix to the bres and the bridging effect of
predicteddand controlleddby formulating proper materials bres across the cracks. Fibre pull-out is the principal mechanism
models for cementitious composites, including strain rate effects. contributing to the high toughness of the material and it is the
As a matter of fact, the scanty information provided so far by spe- preferred failure mode, rather than the fracture failure mechanism,
cialised equipment such as the Hopkinson bar for very high strain because of its ability to redistribute stresses. Gokoz and Naaman [7]
rates shows a signicant increase in mechanical properties, but this carried out tests under static condition (with a velocity n equal to
increase still needs to be related to the main engineering parame- 4.2  105 m/s) and high displacement rate (n 3 m/s) for three
ters. The current understanding of the dynamic response and types of bres (smooth steel, glass and polypropylene). They
impact resistance of cementitious composites, and especially of concluded that, while polypropylene bres were very sensitive to
high strength concrete, is very limited. There are also contradictory the imposed displacement rate, smooth steel bres were insensitive
results in the literature. With reference to compressive behaviour, to it. They also reported that the post-peak behaviour of steel
smooth bres, whose pull-out behaviour is essentially based on
friction, was almost insensitive to displacement rate. Banthia and
* Corresponding author. Dept. of Structural Eng. (DIS), Politecnico di Milano, P.zza Trottier [8] investigated the pull-out resistance of deformed bres
Leonardo da Vinci, 32, 20133 Milano, Italy. Tel.: 39 02 2399 4251. (hooked end, crimped and I-shaped bres) embedded in a cement-
E-mail address: caverzan@stru.polimi.it (A. Caverzan).

0734-743X/$ e see front matter 2012 Elsevier Ltd. All rights reserved.
doi:10.1016/j.ijimpeng.2012.01.006
A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38 29

based matrix. They performed a series of static (n 8.46  106 m/s) 2. Mix design and manufacturing
pull-out tests using a hydraulic testing machine and a series of
dynamic (n 1.5 m/s) tests carried out by means a pendulum impact This research studies a high performance cementitious
device. The study highlighted that deformed steel bres embedded composite optimised with steel bres. The mix design of the
in cementitious matrixes generally sustain a higher load under HPFRCC material is specied in Table 1. The steel bres were high
impact than under static pull-out and that the pull-out energy is carbon straight bres, 13 mm long with a 0.16 mm diameter (aspect
also greater under impact as long as the bre pulls out and does not ratio lf/df equal to 80); their proportion in the mix was equal to
fail. Similar results were found by Kim et al. [9]. The authors studied 100 kg/m3 (volume fraction Vf equal to 1.25%), while the density of
the pull-out sensitivity to loading rates for two types of high the composite material was equal to 2380 kg/m3. The sand used in
strength steel bres (hooked and twisted) by applying four the material was sieved up to 2 mm and it can be classied as mixed
displacement rates (n was equal to 0.018, 0.18, 1.8 and 18 mm/s). quartz sand. The mix procedure was composed of several phases.
They concluded that the pull-out response of high strength steel First cement and slag were mixed in dry condition for 2 min, then
hooked bres showed no appreciable rate sensitivity, and this result water and super plasticiser were added and the cement paste was
was attributed to the fact that microcracking, from which the rate mixed for 5 min. Then the sand was introduced into the cement
effects are thought to arise, is localised in a small region in the paste and mixed for 5 min. Finally, bres were added while the
vicinity of the hooks, and therefore should not affect signicantly mortar material was mixing. Before casting, its workability was
the rate sensitivity. On the other hand, high strength steel twisted measured by means of a ow test carried out with Abrams cone.
bres showed rate sensitive pull-out behaviour and they attributed A 1.6 m  0.60 m in plane slab, 30 mm thick, was manufactured. The
this to the radial and longitudinal interface cracking that takes place slab was cast by applying a unidirectional ow as shown in Fig. 1. In
along the entire embedded bre length. Since of bre behaviour, order to guarantee a certain bre orientation, the properties of the
cement matrix and the bond between them (or the pull-out self compacting material were used, taking advantage of the ow
mechanism) are likely dependent on the strain rate, it is expected direction. Three prismatic beam samples, 40 mm wide and 600 mm
that the response of bre-reinforced cementitious composites is long, were sawed from the slab and tested in bending to perform
also rate dependent: however, the investigation of the rate depen- a proper mechanical characterisation of the material according to
dency of the pull-out mechanism cannot conclusively identify the Italian Guidelines. The high bre content and the favourable
complete rate sensitivity of the composite. orientation imposed by the casting ow control allow us to guar-
Beginning in the 1980s, various researchers [10e14] studied antee a small dispersion of the response before and after single-
strain rate effects on the tensile properties of strain-softening bre- crack localisation and a hardening behaviour in uniaxial tension
reinforced concrete. They observed a signicant increase in tensile [17e20]. From the bent specimens, several small cylinders 20 mm
strength, strain at maximum stress, and fracture energy due to high long, the object of the present work, were cored in the direction of
strain rates. Moreover, these studies have pointed out that the tensile stresses. Their diameter was nominally equal to 20 mm
mechanical properties and rate sensitivity of bre-reinforced (Fig. 2(a)). Each cylinder cored from each prismatic specimen was
cementitious composites are dependent upon the bre type, bre notched (notch depth 1.5 mm), to be tested in uniaxial tension at
volume fraction and matrix composition, which inuences the different loading rates. The specimen identication used in the
bond between the bre and the matrix. Very few studies have paper consists in two parts: the rst one identies the strain rate
investigated on the effect of the strain rate on the tensile behaviour investigated (S0 for the quasi-static tests, S1 for a strain rate equal
of strain-hardening high performance bre-reinforced cementi- to 0.1 s1, S2 for a strain rate equal to 1 s1, etc.), while the second
tious composites. Kim et al. [15], following the work presented on part is referred to the specimen number. The tests reported are part
the bre pull-out rate sensitivity [9], have investigated the tensile of a large experimental campaign investigated in Caverzans PhD
response of High Performance Fibre-Reinforced Cementitious thesis. In order to simplify the identication scheme the rst part
Composites (HPFRCC) to strain rates. The main parameters inves- (T20/U-20) was deleted; a reader interested to collect all the data
tigated were the type of high strength steel bres (hooked and coming from this experimental campaign performed on HPFRCC
twisted), the bre volume fraction (Vf 1% and Vf 2%), and the material and to have a database focused on the HPFRCC mechanical
matrix strength using a specimen with a bell-shaped ends geom- behaviour characterized by different tests type should consider the
etry. They have investigated four different strain rates from extended notation (i.e. T20/U-20-S3-1).
4 1
3_ 10 s up to 3_ 101 s1 and between these extremes, the
strain rates of 3_ 103 s1 and 3_ 102 s1. They reported that, in
3. Experimental procedures
general, the HPFRCC specimens with twisted bres are generally
sensitive to strain rate, whereas their counterparts with hooked
An experimental programme was carried out to properly iden-
bres are generally not. However, it is important to highlight that the
tify the mechanical properties of high performance steel bre-
strain rates investigated by Kim et al. [15] are considered as a seismic
reinforced cementitious composites under static and dynamic
rate, because they are usually reached during an earthquake, while
conditions. In particular, two different mechanical testing machines
blast and impact scenarios are characterised by strain rates thousand
were used: a hydro-pneumatic machine (HPM) was employed to
times greater than seismic ones. Cadoni et al. [16] studied the
investigate the strain rate range between 0.1 s1 and 1 s1, and
behaviour of HPFRCC (two different bres were studied: polyvinyl-
alcohol and steel bres) when subjected to high strain rates
(_3 50 s1 and higher) by means of a modied Hopkinson bar Table 1
(MHB). They observed, after dynamic failure, that steel bres were Mix design.
pulled-out from the matrix, while the majority of polyvinyl-alcohol Constituent Dosage [kg/m3]
bres experienced tensile failure. The difference in failure could Cement type I 52.5 600
justify the variation in terms of fracture energy as reported by the Slag 500
authors. On the other hand, the tensile strength of the steel bre Water 200
composite increases with strain rate while the tensile strength of Sand 0e2 mm 983
Fibres (lf 13 mm; df 0.16 mm) 100
PVA composites seems to be less sensitive to strain rates, even Super plasticizer 33 l/m3
though it is remarkably increased compared to the static values.
30 A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38

test starts when the second chamber discharges the water through
a calibrated orice that is activated by a fast electro-valve. The
piston then starts to move, expelling the water. The specimen
(S1 and S2 series) is connected on one side to the piston shaft, and
on the other side, to the end of an elastic bar which is rigidly xed
to a supporting structure. When the piston shaft moves, the spec-
imen is pulled at a xed strain rate that depends on the velocity of
expulsion of the water from the chamber. It can be demonstrated
that the movement of the piston at a constant velocity assures
a constant strain rate throughout the test. To allow for better
control of constant velocity conditions, it was chosen to perform
small decreases in the gas pressure and thus small changes in the
piston force. The elastic bar is instrumented with a strain-gauge
that provides, through the elastic properties of the bar, the force
Fig. 1. Slab cast applying a unidirectional ow.
acting on the specimen during the test. Two targets are attached at
both ends of the specimen and their movement is measured by two
a modied Hopkinson bar (MHB) [21] was exploited to investigate contact-less displacement transducers.
high strain rates 150e300 s1. Finally, the load P resisted by the specimen is measured by the
dynamometric elastic bar, whereas the specimen elongation DL is
3.1. Quasi-static tests measured by the displacement transducers, sensing the displace-
ment of the plate target xed to both specimen ends. This data
Uniaxial tensile tests on notched cylindrical specimens (S0 acquisition system allows of deducing the stress versus strain
series) were performed with an electro-mechanical testing relationship for the investigated strain rate.
machine INSTRON 5867 at the laboratory of the Politecnico di
MilanodPolo Regionale di Lecco. The machine has a maximum 3.3. Dynamic tests at high strain rates
loading capacity of 30 kN and it is characterised by a precision for
loading measures of 0.4% of the read value up to 1/100 of the The Hopkinson Pressure Bar (HPB) is an experimental device
maximum load cell capacity, and of 0.5% of the read value up to 1/ widely used for intermediate and high strain rate testing
500 of the maximum load cell capacity. The precision of the stroke (101e104 s1). Several versions of this equipment were developed
displacement measures is equal to 0.05% of the read value. The to derive the dynamic properties of a material under different stress
samples were glued to the machine platens by means of an epoxy conditions (tensile, compression, exural, etc.) [22e24].
resin. Two aluminium cylinders connected to the press by In the present research programme, a Modied Hopkinson Bar
a knuckled joint (Fig. 2(b)) were used as press platens. In both (MHB), placed in the DynaMat laboratory of the University of
cylinders, a 5 mm deep cylindrical cavity with a 22 mm diameter Applied Sciences of Southern Switzerland (SUPSI) of Lugano,
was made in order to increase the glued sample surface. Stroke was Switzerland, was used to carry out the dynamic tests at high strain
considered as feedback parameter during the tests. The displace- rates (Fig. 4). The MHB consists of two circular aluminium bars,
ment rate imposed during the tests was equal to 5  105 mm/s up called input and output bars (with a diameter of 20 mm and having
to 1.5 mm and it was progressively increased to 103 mm/s. lengths of 3 and 6 m, respectively) between which the HPFRCC
specimen (S3 and S4 series) is glued using a bi-component epoxy
3.2. Dynamic tests at medium strain rates resin. The input bar is connected to a high strength steel pretension
bar (having 6 m length and 12 mm diameter), used as pulse
The HPM functioning scheme is presented in Fig. 3. At the generator. The test with the MHB is performed as follows:
beginning of the test, a sealed piston divides the cylindrical tank
into two chambers, one being lled with gas at high pressure a) rst, a hydraulic actuator (of maximum loading capacity of
(viz., 150 bars), and the other with water. An equal pressure is 600 kN) pulls the high strength steel bar; the pretension stored
initially established in the water and gas chambers so that the in this bar is assured by the blocking device (number 3 in
forces acting on the two faces of the piston are in equilibrium. The Fig. 4);

Section A-A

Cavity

L*
A A

Press platen

a b
Fig. 2. Test set-up, press platens and glued specimen: press device (a); press platens and glued specimen (b).
A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38 31

Fig. 3. Hydro-pneumatic machine (HPM).

b) the second operation is the rupture of the fragile bolt in the expandable signal conditioning system which allows the user to
blocking device, which gives rise to a tensile mechanical pulse congure each individual signal conditioner from any host
of duration 2.4 ms and with a linear loading rate during the rise computer with IEEE-488 or RS-232 capability. Individual channels
time. The pulse then propagates along the input and output may be addressed, or an all channel command will simultaneously
bars, leading the specimen to failure. address all channels, for fast initial setup.
In Fig. 5, the raw signals measured on the input and output bars
As with the classical Hopkinson bar apparatus, the pulse prop- are shown. The clean resolution of the incident, reected and
agates along the input bar with the velocity of the elastic wave transmitted pulses, the sharp rise time of the incident pulse (of the
equal to C0, and constant shape. When the incident pulse (3 I) rea- order of 30 ms), and the almost constant amplitude of the incident
ches the HPFRCC sample, it is partly reected by it (3 R). The portion pulse can be observed. In the rst phase of the tests, when the
of pulse that is not reected, passes through the specimen (3 T) and mechanical wave reaches the samples the equation 3 I 3 R 3 T,
propagates into the output bar, as shown in Fig. 5. The relative hence one hypothesis of the Hopkinson bar theory is not respected.
amplitudes of the incident, reected and transmitted pulses The duration of this phase depends on the wave velocity of the
depend on the mechanical properties of the specimen. Strain- material and on the length of the sample: the shorter is the spec-
gauges glued on the input and output bars (800 mm from the imen, the lower time needed to reach the equilibrium is. In the tests
specimen) are used to measure the elastic deformation over time reported, samples length was equal to 20 mm this means that the
generated by the incident, reected and transmitted pulses. The unbalanced phase was limited to 100 ms or less. While the signals
variable measures were registered by a 6 channels AlazarTech data (3 I 3 R) and 3 T are equal after the initial phase and the specimen is
acquisition system (ATS330). The system is designed to provide in equilibrium throughout the fracture process. However, it should
high precision (12 bit) waveform acquisition with a maximum be notice that the unbalanced phase is a peculiar aspect of Hop-
50 MS/s real-time sampling rate, 25 MHz full power bandwidth and kinson technique and can be observed in tests performed on
acquisition memory of 128K samples per channel. Each individual different types of material: brittle materials like rocks, concretes
board has its own independent trigger circuitry and time base, so and ductile materials like metals and alloys. Nevertheless, the
that each channel can be recorded with different time windows. Hopkinson bar is considered as a protable technique to charac-
The data acquisition system receives the signals from the Pacic terize the material behaviour at high strain rate and a large amount
Instrument 6120 programmable transducer ampliers. This is an of papers was published in order to proof it. Thereafter, the stress
and strain in the sample can be derived from Equations (1)e(3)
where L is the specimen length (20 mm):

A0
st E0 3 t (1)
A T

2C
3_ t  0 3 R t (2)
L

Zt
2C
3 t  0 3 R tdt (3)
L
0

On the other hand, the history of the crack opening displace-


ment (COD) can be calculated:
Zt
CODt 2C0 3 R tdt (4)
0

In the case of high performance bre-reinforced cementitious


Fig. 4. Modied Hopkinson bar (MHB). composite specimens, the strain rate can be calculated as for metallic
32 A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38

strain in input and output bars [m/m]


0.0005 30 300
input stress strain-rate
output
25 250
0.0004

stress [MPa]
20 200

strain rate [s ]
0.0003 reflected pulse
15 150
0.0002 incident
pulse 10 100

0.0001 5 50
raw signals
transmitted pulse
0 0 0
0 0.0005 0.001 0.0015 0.002 0 0.0002 0.0004 0.0006 0.0008
time [s] time [s]

Fig. 5. Signals measured on the input and output bar vs time curves of HPFRCC and stress and strain rate vs time curves.

and ductile materials, in which the plastic zone is well dened. It has where samples are glued, Fig. 2(b)) is approximately considered as
to be highlighted that the displacement rate between the two a rigid zone. It is interesting to observe that steel bres are able to
sample ends is the principal data and the strain rate is then obtained favour stable propagation at room temperature up to a strain of
as an average dividing the displacement rate for the sample length. about 4%, computed according to Equation (5). The pre-peak
In order to emphasize this concept the values of displacement rates behaviour is well described by a parabolaerectangular model,
in the paragraph concerning the dynamic tests results were also where the plateau is very close to a value of 2% (Table 2).
reported. Considering the peak strength computed in the paper, the The low values of the elastic stiffness obtained in these tests
transmitted wave was used to compute nominal stresses in the could be caused by the visco-elastic behaviour of the glue. In order
samples (see Equation (1)). When a region close to the peak is to account for the contribution of the visco-elastic behaviour of the
considered, it could be observed that the transmitted wave is always glue, the results were compared with some preliminary tests aimed
a little lower than the sum of incident and reected wave, hence the at evaluating the elastic modulus of the material. These tests
transmitted wave leads to a little lower values of nominal stresses. showed an upper limit for the elastic modulus equal to 40 GPa. The
Stresses computed in this way give values of the peak strength useful elastic deformation for a stress level equal to the peak strength
for engineering applications from a safety point of view. computed with an elastic modulus of 40 GPa was compared to that
computed with the elastic modulus obtained in the tensile tests. It
4. Test results was then possible to estimate the maximum value of the error
affecting the strain measures. The difference between the two
4.1. Quasi-static tests strain values discussed above (D3 peak) is equal to about 1%. The peak
strains, for the undamaged material, could be thereafter over-
Test results are shown in Fig. 6(a,b) in terms of nominal stress estimated at a maximum of 1%.
(sN) versus crack opening displacement (COD) and fracture energy According to the Italian Guidelines, the material can be dened
(Gf) versus crack opening displacement, respectively. Moreover, in as a hardening material. The rst cracking strength is close to
Fig. 6(a) a detail of the peak zones is plotted to highlight the rst 3 MPa, while the peak strength is about 10 MPa. This means that,
linear elastic and the post-peak behaviour, close to the peak. The even if a notch depth ratio equal to 0.15 is used, the cracking
nominal stress is dened as the ratio between the applied load P process is distributed over the entire length. Again, the geometrical
and the area of the cross section A0. defect introduced by the notch and the gluing procedure prevent
Peak strengths and the corresponding crack opening displace- with a correct evaluation of the actual ductility measured in terms
ments are listed in Table 2; the values of the peak strains (3 peak) can of the strain of the peak plateau.
be calculated as follow: On the basis of these results, the total energy absorbed by the
specimen during the test up to the reaching of a negligible stress
wpeak transmitted by bres (Gf; Table 2) can be computed. The energy
3 peak (5)
L* absorbed was always computed up to a crack opening displacement
where L* is the clear span equal to 10 mm (Fig. 2(b)), and repre- equal to 5 mm, if the tests were not nished yet, a vertical cut-off
senting the equivalent specimen length. According to this was applied. Gf represents the fracture energy computed as the
assumption, the cavity depth of the platens (5 mm for each side, subtended area in the stresseCOD plain (see Equation (6)).

a 12.5 S0-1
b 25
S0-2
S0-3 20
10 average
12.5
10
G f [kJ/m2 ]

15
N [MPa]

7.5

5 10
4

2.5 5 S0-1
S0-2
S0-3
average
0 0
0 1 2 3 4 5 0 1 2 3 4 5
COD [mm] COD [mm]

Fig. 6. Quasi-static test results: stress vs COD (a); fracture energy vs COD (b).
A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38 33

Table 2
Peak strengths, crack opening at the peak and fracture energy.

Sample code fpeak [MPa] fpeak,av [MPa] (std) wpeak [mm] wpeak,av [mm] (std) Gf [kJ/m2] Gf,av [kJ/m2] (std) Fibres n
S0-1 9.71 8.62 0.17 0.20 21.23 19.51 75
S0-2 7.83 (0.97) 0.19 (0.04) 18.11 (1.58) 77
S0-3 8.33 0.25 19.19 73

a 20 b 20
S1-1 S2-1
S1-2 S2-2
S1-3 S2-3
average S2-4
15 15 average
20
15
N [MPa]

15

N [MPa]
10
10 10 10

5 5

0
5 0 5 0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8
0 0.1 0.2 0.3 0.4

0 0
0 1 2 3 4 5 6 7 0 1 2 3 4 5 6 7 8 9 10
COD [mm] COD [mm]

Fig. 7. Stress vs COD curves. Dynamic tests performed at: 3_ 0:1 s1 (a); 3_ 1 s1 (b).

Table 3. The values of peak strains can be derived from Equation (5)
Z
COD
using L, the specimen length (20 mm), instead of L*.
Gf sN wdw (6) The total fracture energy absorbed during the tests was always
0 computed up to a crack opening displacement equal to 5 mm. If
a higher opening was measured at the end of the tests, a vertical
The fracture energy, Gf, computed according to Equation (6),
cut-off was performed. When the test control was lost due to bre
takes into account three different contributions: the energy
failure, the energy up to such limit value was computed. The plot of
required to create a new fracture surface in the matrix, the energy
the fracture energy versus the crack opening displacement is
involved in the pull-out process, and the energy eventually needed
shown in Fig. 8, while the results in terms of total energy are listed
for the failure of the steel bres. These contributions could have
in Table 3. As an average, the fracture energy showed an increase at
different COD activation thresholds and different relative impor-
0.1 s1 with respect to that derived for quasi-static tests.
tances. The evolution of the fracture energy with respect to the
crack opening displacement (COD) is shown in Fig. 6(b). During
tensile tests, the generation of a new fracture surface in the matrix 4.3. Dynamic tests at high strain rates
and the bre pull-out are the main mechanisms involved, while the
fracture energy associated with the bre failure is negligible. The displacement rates reached in the tests here reported were
equal to about 3 m s1 (specimen series S3) and 3 m s1 which
4.2. Dynamic tests at medium strain rates correspond to an equivalent strain rates of about 150 and 300 s1
respectively. The high strain rate results obtained on HPFRCC are
For a better understanding of the dynamic behaviour of the reported in Table 4 in terms of peak strength, crack opening
material, a series of tests at strain rates equal to 0.1 s1 (specimens displacement at the peak and fracture energy. In Fig. 9(a,b), the
named S1) and 1 s1 (specimens named S2) were carried out stress versus COD curves of the HPFRCC specimens tested at high
exploiting the hydro-pneumatic device. Fig. 7 shows the results in strain rates are shown. Details of the peak zones are plotted in
terms of nominal stresses versus COD. To highlight the rst linear Fig. 9(a,b) in order to highlight the rst linear elastic branch and
elastic and the post-peak behaviour, details of the peak zones are post-peak behaviour close to the peak. It can be observed that after
also plotted in Fig. 7. The material behaviour is well described by an a remarkable peak strength, which is greater than the peak
elasticeplastic model. In fact, after the peak, a stress plateau, higher observed in the static condition and for a strain rate equal to 1 s1,
than that observed in the quasi-static test (Fig. 6(a)), up to a COD of the specimens show a small drop down to a post-peak stress
0.4 mm, is shown. Finally, the good bre distribution can be plateau up to a COD of 0.4 mm, as highlighted in the quasi-static
appreciated by the very low scatter obtained in the tests. Peak tests. The stress plateau reached a stress level equal to 15 MPa, as
strength and crack opening displacement are summarised in observed in the dynamic tests performed at 3_ 1 s1. This quite

Table 3
Peak strengths, crack opening at the peak and fracture energy at 3_ 0:1 s1 and 3_ 1 s1 .

Sample code fpeak [MPa] fpeak,av [MPa] (std) wpeak [mm] wpeak,av [mm] (std) Gf [kJ/m2] Gf,av [kJ/m2] (std) Fibres n
S1-1 13.07 12.36 0.38 0.49 34.61 32.45 71
S1-2 10.30 (1.81) 0.57 (0.10) 28.07 (3.80) 76
S1-3 13.71 0.53 34.68 72

S2-1 14.29 15.25 0.37 0.61 28.03 31.40 76


S2-2 14.09 (1.65) 0.46 (0.23) 24.90 (7.75) 71
S2-3 17.67 0.81 42.57 73
S2-4 14.96 0.82 30.11 77
34 A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38

a 45 b 45
40 40
35 35
30 30

G f [kJ/m2 ]

G f [kJ/m2 ]
25 25
20 20
15 15
10 S2-1
S1-1 10 S2-2
S1-2 S2-3
5 S1-3 5 S2-4
average average
0 0
0 1 2 3 4 5 0 1 2 3 4 5
COD[mm] COD[mm]

Fig. 8. Fracture energy vs COD curves. Dynamic tests performed at: (a) 3_ 0:1 s1 ; (b) 3_ 1 s1 .

Table 4
Peak strengths, crack opening and fracture energy at 3_ 150 s1 and 3_ 300 s1 .

Sample code fpeak [MPa] fpeak,av [MPa] (std) wpeak [mm] wpeak,av [mm] (std) Gf [kJ/m2] Gf,av [kJ/m2] (std) Fibres n
S3-1 20.46 22.36 0.038 0.038 34.59 29.46 79
S3-2 22.28 (1.89) 0.032 (0.01) 31.43 (7.75) 90
S3-3 24.96 0.024 24.75 79
S3-4 21.74 0.056 27.06 e

S4-1 21.88 24.25 0.017 0.018 27.32 29.46 91


S4-2 22.49 (3.60) 0.015 (0.01) 15.89 (7.75) 67
S4-3 28.39 0.021 28.66 90

constant stress plateau seems to be a dynamic material property 5. Discussion


linked to the debonding phase and partially to the rst stage of the
pull-out mechanism. High strain rates mainly affect the peak In order to have an overview of the global material behaviour,
strength rather than the bre pull-out strength. The peak strength the average of the stress versus crack opening displacement curves
in static conditions and for medium strain rates is highly inu- and fracture energy versus crack opening displacement is plotted.
enced by the bres, which contributes to developing multiple Fig. 13(a,b) summarises the experimental results in terms of the
cracks. average curves for the HPFRCC. Each curves represents the material
In Fig. 10(a,b), the evolution of the fracture energy with respect response for a different strain rate. Besides, in Fig. 14(b) a detail of
to the crack opening displacement (COD) for each strain rate is the peak zone is plotted in order to highlight the rst elastic branch
shown. As in the quasi-static tests, the fracture energy is and the region close to the peak. It is worth observing the
computed by using Equation (6). The same criteria mentioned increasing initial stiffness with the increase of strain rates. This
above were followed: when the test curves were stopped due to increase is much more evident when the strain rate is equal to 150
the sudden drop induced by bre failure, a vertical jump or 300 s1.
assumption was used and the energy absorbed was always The material tested at 0.1 s1 has shown a small increment in
computed up to a crack opening displacement equal to 5 mm, by the initial stiffness. A small increment was also expected for the
applying a vertical cut-off. The fracture energy computed shows material tested at 1 s1. On the contrary, the material showed in the
a comparable value with that of the tests carried out at lower pre-peak region a behaviour well described by a parabo-
strain rates. Figs. 11 and 12 show clearly that a single macro-crack laerectangular model with an initial stiffness close to the static
was triggered in the notched section of samples tested at high one (Fig. 13(a)). The behaviour described above could be attributed
strain rates, no other fracture plane can be detected. Some to a pre-cracking problem; nevertheless this explanation seems
external micro- and nano-fracture planes could be present but unlikely because all four samples tested at 1 s1 showed a similar
their contribution to the total energy is negligible if it is compared pre-peak behaviour. Analysing the tests results, several interesting
to the energy involved in the pull-out process which is several considerations can be highlighted. When the strain rate grows, not
orders of magnitude higher even if could play a key role in the only does the initial stiffness increase, but so do the peak strength
pre-peak behaviour. and the post-peak plateaus observed for all the strain rates

a 30 S3-1
b 30 S4-1
S3-2 S4-2
25 S3-3 25 S4-3
S3-4 average
average 30
20 30 20 25
N [MPa]

N [MPa]

25
20
20
15 15 15
15
10
10
5
10 5 10
0
0 0 0.1 0.2 0.3 0.4
0 0.1 0.2 0.3 0.4
5 5

0 0
0 1 2 3 4 5 0 1 2 3 4
COD[mm] COD[mm]

Fig. 9. Stress vs COD curves. Dynamic tests performed at: 3_ 150 s1 (a); 3_ 300 s1 (b).
A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38 35

a 35 b 35

30 30

25 25

G f [kJ/m2 ]
G f [kJ/m2 ]
20 20

15 15

10 S3-1
10
S3-2 S4-1
5 S3-3 5 S4-2
S3-4 S4-3
average average
0 0
0 1 2 3 4 5 0 1 2 3 4 5
COD[mm] COD[mm]

Fig. 10. Fracture energy vs COD curves. Dynamic tests performed at: 3_ 150 s1 (a); 3_ 300 s1 (b).

Fig. 11. Photos of the samples tested at displacement rate equal to 3 m s1 (_3 150 s1).

investigated. While the peak strength grows when the strain rate pull-out process. For low strain rates, the bres and the adjacent
increases, the post-peak plateau grows from 8.5 MPa in static area have time to deform themselves and/or develop plastic
condition to about 15 MPa for a strain rate equal to 1; in between, deformation in order to reduce the dynamic frictional force. When
a value of about 11 MPa was reached for a strain rate equal to 0.1 s1. the strain rate increases, the process described above cannot take
For strain rates greater than 1 s1, the post-peak stress plateau was place: there is not enough time to develop such a plastic defor-
always equal to about 15 MPa. This stress level seems to be mation and hence the dynamic frictional force increases. Looking to
a dynamic threshold linked to the pull-out mechanism. During the the matrix behaviour at high strain rates (_3 150e300 s1),
fracture process in a pull-out test, it is possible to divide the bre a remarkable increase of the peak strength can be pointed out
contribution into two principal parts: the rst part is that due to the (see Fig. 13(a)). This strength enhancement can be essentially
debonding phase and the second part is that due to the pull-out. associated to the matrix. When the peak is reached, a localised
The pull-out mechanism for a straight bre is a mechanism crack appears, causing a drop in the stress. The stress drops down to
partially based on friction and it is completely activated for a rela- a value of about 11 MPa for a strain rate equal to 150 s1 and to
tive large crack opening displacement. The plateau stress zone about 14 MPa for a strain rate equal to 300 s1. These break points
(for a COD between 0.2 and about 0.8 mm) is surely dominated by and the following stress recovery could be associated with a stabi-
the pull-out mechanism. Fig. 14(a) shows the pull-out load (P) lisation of the delamination process in the dynamic eld.
versus slip response for a straight bre close to the peak region. Looking to the softening behaviour of the pull-out mechanism
Besides, Fig. 14(a) shows also a schematic representation of the for a for a COD between 1 and 2.5 mm is inuenced by the slope KIII
previous curve by a polyline. When the strain rate increases, the (see Fig. 13(a)). In that COD range an embrittlement of the material
level of the stress plateau gradually jumps to a limit stress value of response with the increase of strain rate can be highlighted. The
about 15 MPa for strain rates grater then 1 s1. This limit seems to embrittlement can be related to a decrease of KIII with the increase
be a dynamic property of the material. This increase in the plateau of strain rate. Analysing Fig. 13(a) at higher crack opening
could be explained by an increase of the point (I) and the slope (KII) displacements (from COD equal to 2.5 mme5 mm), an alignment of
in Fig. 14(a) with the strain rates. the material response can be pointed out for all the strain rates
The rising of the point (I) could be linked to the delamination investigated.
process along the bres in the debonding phase. This delamination In Fig. 15(a) the dynamic increase factor (DIF) versus strain rate
consists in a propagation of a crack in the matrix surrounding the is plotted. The dynamic increase factor is computed as the ratio
bre along the bre length. The delamination process could sta- between the dynamic strength of the material (fpeak,dynamic) and the
bilise with the increase of the strain rates. Instead, the increase of static strength of the material (fpeak,static). The DIF parameter can be
KII with the growth of strain rate could be related to the deforma- used to quantify the rate sensitivity of this material. The DIF curves
tion capability of the bres and the surrounding zones during the are compared with the curves proposed by Model Code 90 (MC90),

Fig. 12. Photos of the samples tested at displacement rate equal to 6 m s1 (_3 300 s1).
36 A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38

a b 35
25 S0
S1 30
S2
20 S3 25
S4

G f [MPa]
N [MPa]
15 20

15
10
10 S00
S
S1
5 S2
5
S3
S4
0 0
0 1 2 3 4 5 6 7 0 1 2 3 4 5
COD[mm] COD[mm]

Fig. 13. Tests results: average curves. Stress vs COD (a) and fracture energy vs COD (b) at different strain rates.

Model Code 2010 (MC10), Malvar and Ross [25] and Birkimer [26] micro concrete by exploiting a split Hopkinson bar. The micro
for plain concrete (the tests performed by Birkimer do not concrete tested in their experiments was characterised by
provide any information for the strain rates lower than 2, hence a maximum aggregate size, as used in the HPFRCC object of the
a linear trend was supposed in this range). Different from what is present paper, equal to 2 mm but with a lower strength. Analysing
proposed by the codes, Malvar and Ross [25] the HPFRC investi- the experimental results the authors pointed out a drastic increase
gated here has a change in its DIF slope at 0.1 s1. A transition zone in the total fracture energy: the value computed at 120 s1 is three
between 0.1 and 150 s1, with a slope lower than the slope times higher than the static one. In Fig. 15(b) the results in terms of
proposed by all the formulations taken into account, could char- the ratio between dynamic and static fracture energy versus the
acterise the DIF trend of the material. Up to 150 s1 a zone with strain rate is plotted. It can be highlighted that the material had
higher slope than the previous one could be dened. More data for always a dynamic fracture energy higher than the static one, as
strain rates higher than 300 s1 are needed in order to conrm the reported by Schuler and Hansson [29]. The dynamic increase factor
different slope for strain rates higher than 150 s1. However the DIF for the fracture energy (DIFGf) does not appear to be rate dependent
trend for high strain rates has a slope lower than that suggested by as shown for the plain high performance concrete by Schuler and
the codes. Finally, even if the transition zone is neglected and a bi- Hansson [29], but it is close to 1.6 up to a strain rate equal to 150 s1
linear curve is used to describe the DIF trend, the slope would and it decreases to 1.2 for a strain rate equal to 300 s1. However, it
change for a strain rate equal to about 10 s1. To the best knowledge is difcult to compare directly the results in terms of fracture
of the authors, no studies have been reported on the effect of strain energy for plain and bre concrete where the presence of bres
rates on fracture energy in bre-reinforced cementitious compos- plays a signicant role. The mechanism of failure for plain concrete
ites. As mentioned previously, many experiments have been per- at high loading rates is characterised by the propagation of many
formed to study the tensile strength over a wide range of strain micro-cracks at the same time. This mechanism could explain the
rates, but little data is available for the fracture energy in plain increase in fracture energy. At high strain rates the micro-cracks
concrete [27e30]. Weerheijm [27] measured in direct tension tests could not have enough time to follow the minimum energy path
with a Hopkinson bar over the complete stressecrack opening as in the quasi-static tests where the micro-cracks nucleate in
relation. The author reported the fracture energy at strain rates a macro-crack which can propagate with a certain velocity. At high
between 101 and 100 1/s: from those results an increase in the strain rates the micro-cracks are forced to propagate along the
fracture energy with the strain rate or crack opening velocity shortest path characterised by a higher resistance [25,30,31]. This
cannot be seen. On the other hand, Schuler et al. [28,29] focussed phenomenon can explain the drastic increase in fracture energy
their studies on the fracture energy at strain rates between 101 and observed in plain concrete at high strain rates (>1 s1). On the
102 by exploiting a split Hopkinson bar. In spall experiments, it is other hand, bre-reinforced cement-based materials are charac-
not possible to measure stress over strain or crack opening as can terised by high fracture energy due to the pull-out mechanism.
be done in a quasi-static tension test, and for this reason, Schuler at The energy involved during the bre pull-out represents the prin-
al. computed the fracture energy from the reduction of the frag- cipal energetic contribution in the failure process. The pull-out
ment velocities. From the experimental results they observed mechanism and its rate dependancy are completely different
a dynamic increase factor for the fracture energy between 2 and 3. from the failure behaviour of plain concrete as Figs. 13 and 15(b)
Also Brara and Klepaczko [30] performed several dynamic tests on show. Finally, it should be noted that the good bre orientation

a P b 25
P S0
S1
20 S2
S3
S4
15
N [MPa]

10

0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8
0 COD[mm]

Fig. 14. Expected pull-out behaviour for straight bres (a); stress vs COD for different strain rates: detail of the peak zone (b).
A. Caverzan et al. / International Journal of Impact Engineering 45 (2012) 28e38 37

a 3 b 2

2.5 HPFRCC 1.5


MC1990
MC2010
Malvar

DIF Gf
Birkimer

DIF
2 1

1.5 0.5

1 0
1e-06 1e-05 0.0001 0.001 0.01 0.1 1 10 100 1000 1e-06 1e-05 0.0001 0.001 0.01 0.1 1 10 100 1000
.

Fig. 15. Static and dynamic results: comparisons. DIF vs strain rate (a) and fracture energy ratio vs strain rate (b).

obtained in the samples produced a fracture energy stabilisation in 0.8 mm. This value of the stress plateau (15 MPa) appears to be
the whole strain rate range investigated. an upper bound limit and a dynamic property of the investi-
gated material.
6. Conclusions e The high strain rates seem to modify the strain localisation
process. In fact, for low strain rates the stable crack propagation
The behaviour of an advanced high performance bre- seems to be associated to the growth of a process zone char-
reinforced cementitious composite when subjected to different acterised by a stable multi-localisation. On the contrary, at high
strain rates was investigated. An extensive experimental investi- strain rates a strain localisation takes place for very small crack
gation was carried out by means of uniaxial tension tests in the opening favouring, the uncoupling of unstable mode I crack
static eld. Furthermore, a dynamic characterisation was per- propagation from the pull-out delamination.
formed in uniaxial tension by exploiting a hydro-pneumatic e The dissipated energy up to a large crack opening (5 mm)
machine and a modied Hopkinson bar. remains almost constant for growing strain rates up to a value
From the experimental results presented in this research work of 150 s1 and scantly decreases at 300 s1.
some important conclusions can be drawn:

Acknowledgements
e With reference to the material self compacting properties,
a good bre alignment was obtained by imposing a unidirec-
The Authors are grateful to Matteo Dotta and Daniele Forni of
tional casting ow. This result is conrmed by the low scatter
the University of Applied Sciences of Southern Switzerland, Matteo
observed in the material response. The low scatter was
Colombo and Giulio Zani of the Politecnico di Milano for their
observed in the overall test series carried out, and at all the
precious collaboration in the execution of the laboratory tests. The
strain rates investigated. The material so cast, and thus char-
research was partially nanced by the project ACCIDENT ID
acterised by a good bre alignment, showed a very high
7629770 in the frame of INTERREG IT/CH 2006-2013 program.
performance compared with other cementitious composites at
comparable cost.
e On the basis of the results coming from the static and dynamic
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