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D1 50
D2 70
B 0
t 2.66
R Rv calc medido
1.10E+13 8.1197E+14 7.30E+14
18.6737547
t g delta g/t
0.2 8.84 4.33 44.20
0.4 8.84 4.24 22.10
0.6 8.84 4.16 14.73
0.8 8.84 4.07 11.05
1 8.84 3.98 8.84
1.2 8.84 3.89 7.37
1.4 8.84 3.80 6.31
1.6 8.84 3.71 5.53
1.8 8.84 3.63 4.91
2 8.84 3.54 4.42
2.2 8.84 3.45 4.02
2.4 8.84 3.37 3.68
2.6 8.84 3.28 3.40
2.8 8.84 3.20 3.16
3 8.84 3.11 2.95
3.2 8.84 3.03 2.76
3.4 8.84 2.96 2.60
3.6 8.84 2.88 2.46
3.8 8.84 2.80 2.33
t g delta g/t
2 0.5 0.02 0.25
2 0.6 0.04 0.30
2 0.7 0.05 0.35
2 0.8 0.06 0.40
2 0.9 0.08 0.45
2 1 0.10 0.50
2 1.1 0.12 0.55
2 1.2 0.14 0.60
2 1.3 0.16 0.65
2 1.4 0.18 0.70
2 1.5 0.21 0.75
2 1.6 0.24 0.80
2 1.7 0.26 0.85
2 1.8 0.29 0.90
2 1.9 0.33 0.95
2 2 0.36 1.00
2 2.1 0.39 1.05
2 2.2 0.43 1.10
2 2.3 0.46 1.15
2 2.4 0.50 1.20
2 2.5 0.53 1.25
2 2.6 0.57 1.30
2 2.7 0.61 1.35
2 2.8 0.65 1.40
2 2.9 0.69 1.45
2 3 0.73 1.50
2 3.1 0.77 1.55
2 3.2 0.82 1.60
R
D1
D2
T
ro 4.00E+13
D 4.1
d 1.8
R 52.3931202
B g/2-delta g/2-delta/t
0.020 0.088 0.44
0.040 0.177 0.44
0.060 0.265 0.44
0.080 0.353 0.44
0.100 0.441 0.44
0.120 0.530 0.44
0.140 0.618 0.44
0.160 0.706 0.44
0.180 0.794 0.44
0.199 0.881 0.44
0.219 0.968 0.44
0.239 1.054 0.44
0.258 1.139 0.44
0.277 1.223 0.44
0.295 1.305 0.44
0.313 1.386 0.43
0.331 1.464 0.43
0.349 1.541 0.43
0.365 1.615 0.43
1.800
1.200
1.000
0.800
B g/2-delta 0.600
0.902 0.226
0.883 0.265
0.400
0.864 0.302
f(x) = 0.0968015488x + 0.0034420416
0.845 0.338 R = 0.9995070992
0.827 0.372 0.200
0.000
0 0.5 1 1.5 2 2.5 3 3.5
espesor mm
0.600
0.400
f(x) = 0.0968015488x + 0.0034420416
R = 0.9995070992
0.200
0.808 0.404
0.790 0.435 0.000
0.773 0.464 0 0.5 1 1.5 2 2.5 3 3.5
0.755 0.491
espesor mm
0.738 0.517
0.721 0.541
0.705 0.564
0.688 0.585
0.673 0.605
0.657 0.624 1.20E+15
0.642 0.642
1.10E+15
0.627 0.659
0.613 0.674 1.00E+15
0.559 0.727
7.00E+14
0.547 0.738
0.535 0.749 6.00E+14
0.511 0.767
0.500 0.776
0.490 0.783
8.00E+12 B Rv
5 0 7.85E+14 69%
7 0.1 8.17E+14 72%
0.2 0.2 8.49E+14 75%
0.3 8.82E+14 78%
0.4 9.16E+14 81%
0.5 9.50E+14 84%
0.6 9.85E+14 87%
0.7 1.02E+15 90%
0.8 1.06E+15 93%
0.9 1.09E+15 97%
1 1.13E+15 100%
0.50
0.48
0.46
0.44
B
0.42
Linear (B)
g/2-delta
0.40
Linear (g/2-delta)
g/2-delta/t
0.38
0.36
0.34
0.32
0.30
3 3.5 4
0.36
0.34
0.32
0.30
3 3.5 4
Medicion de dureza Shore A por duplicado
65 Placa 3x2
Manta Taco 6mm
61
59
57
55
11/27/2009 11/28/2009 11/29/2009 11/30/2009 12/1/2009
1 75
2 73
3 72
4 72
5 72.5
10 71
15 71
20 70
25 70
30 69.5
35 69.5
40 69
45 69
50 69
55 69
60 68.5
65 68.5
70 68
15 -0.0921121468
76
72
70
68
66
64
0 10 20 30 40 50 60 70 80
segundos
66
64
0 10 20 30 40 50 60 70 80
segundos
70.5
71.0
70.5
71.0
71.0
70.5
70.0
70.0
5 Tiempo 10'
Manta
Placa 3x2
Manta Taco 6mm
pellet taco 6mm
2/1/2009
medicion 10min
manta
100
90
0 phr carb
84 25 phr carb
80 60 phr carb
shore a
72
70
60
58
50
46
40
37
30
20 30 40 50 60 70 80 90 100 110 120
phr epoxi
24 hs
manta
100
90
0 phr carb
25 phr carb
60 phr carb
80
100 phr carb
shore a
70
60
50
40
30
20 30 40 50 60 70 80 90 100 110 120
phr epoxi
48 hs
manta
100
90 0 phr carb
25 phr carb
60 phr carb
80 100 phr carb
shore a
70
60
50
40
30
20 30 40 50 60 70 80 90 100 110 120
phr epoxi
72 hs
manta
100
90
0 phr carb
25 phr carb
80 60 phr carb
100 phr carb
shore a
70
60
50
40
30
20 30 40 50 60 70 80 90 100 110 120
phr epoxi
30 phr epoxi
manta
98
96
94
92
shore a
90
0 phr carb
25 phr carb
88 60 phr carb
86
84
82
80
78
0 10 20 30 40 50 60 70 80
horas
30 phr epoxi
manta
10
7
shore a
6
0 phr carb
25 phr carb
5 60 phr carb
0
0 10 20 30 40 50 60 70 80
horas
50 phr epoxi
manta
90
88
86
84
shore a
82
0 phr carb
25 phr carb
80 60 phr carb
100 phr carb
78
76
74
72
70
0 10 20 30 40 50 60 70 80
horas
50 phr epoxi
manta
12
10
shore a
0 phr carb
25 phr carb
6 60 phr carb
100 phr carb
0
0 10 20 30 40 50 60 70 80
horas
70 phr epoxi
manta
80
75
shore a
70
0 phr carb
25 phr carb
65 60 phr carb
100 phr carb
60
55
50
0 10 20 30 40 50 60 70 80
horas
70 phr epoxi
manta
12
10
shore a
0 phr carb
25 phr carb
6 60 phr carb
100 phr carb
0
0 10 20 30 40 50 60 70 80
horas
90 phr epoxi
manta
65
60
shore a
55
0 phr carb
25 phr carb
60 phr carb
100 phr carb
50
45
40
0 10 20 30 40 50 60 70 80
horas
90 phr epoxi
manta
14
12
10
shore a
8 0 phr carb
25 phr carb
60 phr carb
0
0 10 20 30 40 50 60 70 80
horas
110 phr epoxi
manta
55
50
shore a
45
0 phr carb
25 phr carb
60 phr carb
100 phr carb
40
35
30
0 10 20 30 40 50 60 70 80
horas
110 phr epoxi
manta
14
12
10
shore a
8 0 phr carb
25 phr carb
60 phr carb
0
0 10 20 30 40 50 60 70 80
horas
Tipos de preparacion de muestras
Condiciones de medicion
10 minutos
24 horas
48 horas
72 horas
MM
Formula Ensayo Resina Carbonato Epoxi MM_10 MM_24 MM_48 MM_72
65/10 29 K65 0 10
65/10/25 30 K65 25 10
65/10/55 31 K65 60 10
65/10/100 32 K65 100 10
65/30 33 K65 0 30 84 92 93 93
65/30/25 34 K65 25 30 86 92 94 94
65/30/55 35 K65 60 30 88 93 95 96
65/30/100 36 K65 100 30 90 93 95 96
65/50 37 K65 0 50 72 80 81 82
65/50/25 38 K65 25 50 74 84 84 84
65/50/55 39 K65 60 50 80 84 85 85
65/50/100 40 K65 100 50 83 87 87 87
65/70 41 K65 0 70 58 66 68 68
65/70/25 42 K65 25 70 60 67 69 69
65/70/55 43 K65 60 70 63 70 71 71
65/70/100 44 K65 100 70 69 75 76 76
65/90 45 K65 0 90 46 56 58 58
65/90/25 46 K65 25 90 49 57 59 59
65/90/55 47 K65 60 90 52 59 60 60
65/90/100 48 K65 100 90 55 62 62 62
65/110 49 K65 0 110 37 46 49 49
65/110/25 50 K65 25 110 41 48 50 50
65/110/55 51 K65 60 110 43 50 52 52
65/110/100 52 K65 100 110 45 53 53 54
0 24 48 72
88 14.726 97 21.066 96 7.6665 97 17.506 0 8
92 31.645 99 40.294 98 14.671 99 22.361 0 6
97 71.168 101 66.059 101 33.111 101 27.015 0 5
102 126.9 105 135.89 104 83.304 104 69.403 0 3
71 0.3083 80 0.3765 81 0.0836 82 0.0009 0 8
75 0.7573 82 2.3821 83 0.6788 83 0.2638 0 10
79 0.4444 85 0.0173 85 0.0468 85 0.0499 0 5
83 0.3869 88 0.4373 88 0.6875 88 0.6175 0 5
57 0.0259 66 0.027 68 0.0019 68 0.0328 0 9
60 0.0034 68 0.66 70 0.2586 70 0.2217 0 7
64 0.6048 71 0.2139 72 0.5771 72 0.3393 0 7
68 1.9424 74 1.0977 74 2.1965 74 2.2273 0 6
46 0.0487 55 0.3575 57 0.0225 57 0.0256 0 10
49 0.0015 57 0.0006 59 0.0218 59 4E-06 0 8
52 0.0836 59 0.2308 61 0.0018 60 0.0042 0 7
55 0.1744 62 0.036 63 0.0747 63 0.2874 0 8
38 0.3473 46 0.0609 49 0.0009 49 0.0012 0 9
40 0.9858 48 0.0462 50 0.0002 50 4E-11 0 7
43 0.0451 50 0.0869 51 0.2009 52 0.0603 0 7
45 0.0877 53 0.1262 53 0.1125 54 0.0229 0 8
6.2474 6.1569 4.9663 4.1548 0 24
9 9
8 8
7 8
5 6
9 10 73.50 78.50 82.50
10 10 80.60 82.60 83.50
6 6 83.00 86.00 87.00
5 5 85.50 88.50 89.00
11 11 61.50 66.50 67.50
9 9 62.00 68.50 69.50
8 8 64.00 71.00 72.00
7 7 72.50 77.00 79.00
12 12 47.00 52.50 54.00
10 10 48.00 56.50 57.00
9 9 51.00 60.00 60.00
8 8 56.50 64.00 64.50
12 12 36.00 44.00 44.50
9 9 39.00 46.50 48.50
9 9 42.00 48.00 50.00
8 9 47.00 54.00 55.00
48 72
76 6.68 79 0.65 82 0.25 0 5 9
78 5.29 82 0.66 84 0.05 0 2 3
82 1.09 85 0.45 87 0.20 0 3 4
87 2.02 89 0.97 90 1.87 0 3 4
60 2.73 66 0.46 67 0.00 0 5 6
62 0.00 68 0.04 69 0.01 0 7 8
66 2.54 72 0.73 72 0.24 0 7 8
70 4.08 76 0.98 77 5.65 0 5 7
47 0.15 54 1.77 55 1.03 0 6 7
49 0.53 56 0.03 57 0.01 0 9 9
52 1.52 60 0.02 60 0.24 0 9 9
57 0.29 64 0.00 65 0.18 0 8 8
36 0.14 43 0.43 45 0.01 0 8 9
38 0.32 46 0.44 47 2.57 0 8 10
42 0.02 49 1.94 51 0.28 0 6 8
47 0.16 54 0.19 55 0.08 0 7 8
27.57 9.76 12.69
98 98 98.5
98.5 98.5 98.5
98.5 98.5 98.5
98.5 99 98.5
80.5 82.5 84.5
83 85.5 86.5
86.5 88 88.5
89 90.5 90.5
61.5 66 67.5
64 69 70.5
67.5 72.5 74.5
70.5 75 76
48.5 55.5 57
50.5 57 58
55 61 62
59.5 63 64
41 47.5 49.5
43 48.5 49.5
46 51 52
49 53.5 55
98 0.2 97 0.7 98 0.37
99 0.1 99 0.0 99 0.11 0 0 0
100 2.8 100 2.7 100 2.00 0 0 0
101 8.8 101 5.7 101 5.44 0 1 0
79 1.3 82 0.2 83 1.12 0 2 4
81 4.0 84 3.2 85 3.21 0 3 4
83 11.9 86 5.4 86 5.03 0 2 2
85 15.6 87 10.0 88 7.82 0 2 2
64 4.0 68 5.7 70 6.95 0 5 6
66 2.5 70 1.8 72 1.52 0 5 7
68 0.6 73 0.0 74 0.57 0 5 7
71 0.2 75 0.1 76 0.08 0 5 6
50 2.2 56 0.5 58 0.95 0 7 9
53 4.1 58 2.0 60 3.60 0 7 8
56 0.7 61 0.0 62 0.14 0 6 7
59 0.1 64 0.4 65 0.76 0 4 5
39 4.9 45 4.1 47 6.50 0 7 9
42 1.5 48 0.3 49 0.09 0 6 7
46 0.1 51 0.0 52 0.02 0 5 6
50 0.8 54 0.2 55 0.03 0 5 6
66.1 43.016 46.30
K 18.73248 K 24.77201
a -0.0441 a -0.17984
b 0.011283 b -0.04281
d 0.000228 d 0.00053
a1 -0.00047 a1 0.000273
b1 -0.0005 b1 -0.00026
Diferencia con 10 min (MPa)
Traccion
3.00
2.00
1.00
0.00
40 50 60 70 80 90 100
-1.00
-2.00
-3.00
K 25.65658
a -0.19224
b -0.0302
d 0.000685
a1 0.000236
b1 -0.00051
cion
e epoxi (phr)
ELO 10 ELO 24 ELO 48
K 48.64457 K -33.9136 K
a 4.83357 a 7.381699 a
b 0.425995 b -0.14965 b
d -0.00658 d 0.001449 d
a1 -0.01439 a1 -0.03438 a1
b1 -0.00613 b1 -0.00698 b1
encia de elong (%)
60
40
Diferencia de elong (%)
-80
-60
-40
-20
0
20
40
60
40
105.0793 0 -17 -17
0 0 0
67.91156 0 8 -9
69.31202 0 -53 -10
2424.288 0 36 40
1261.728 0 -28 25
129.4173 0 -23 -20
821.0708 0 13 -28
422.3354 0 -25 -42
1834.761 0 -33 9
84.03988 0 0 -17
0.21152 0 -9 -50
177.1453 0 -45 -50
746.4665 0 -27 9
8999.82 0 -20 -58
1927.969 0 -33 8
19071.55
62.76764
5.050514
-0.01402
0.000746
-0.02022
-0.00914
encia de elong (%)
Elongacion
60
40
Diferencia de elong (%)
Elongacion
60
40
20
0
24hs
40 50 60 70 80 90 100 110 120
48 hs
-20
-40
-60
K 1.39E+00
a -3.80E-03
b 3.24E-03
d -1.36E-05
a1 1.64E-05
b1 7.30E-06
24hs
110 120
48 hs
ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
manta 10 minutos
90
80
calculado
70
60
50
40
30
30 40 50 60 70 80 90
medido
epoxi 50 K 119.0021691
carbonato 15 a -1.13034082
dureza 73 b 0.17555308
d -0.00072507
a1 0.003583853
b1 -0.00021927
manta 24 horas
100
90
calculado
80
70
60
50
40
40 50 60 70 80 90 100
medido
epoxi 50 K
carbonato 15 a
dureza 81 b
d
a1
b1
+ b1*(carb)^2 ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
manta 48 horas
100
calculado
90
80
70
60
50
40
80 90 40 50 60 70 80 90 100
medido
epoxi 50 K 122.35330445
carbonato 15 a -0.962648414
dureza 82 b 0.0954901993
d -0.000509131
a1 0.0026833315
b1 2.566093E-05
manta 72 horas
100
90
calculado
80
70
60
50
40
90 100
40 50 60 70 80 90 100
medido
50
40
40 50 60 70 80 90 100
medido
126.2471956 epoxi 50 K
-1.07950768 carbonato 15 a
0.07149457 dureza 82 b
-0.00014986 d
0.00320871 a1
0.000132753 b1
90 100
90 100
90 100
125.2913101
-1.02241471
0.064484069
-0.00025513
0.002983455
0.000134385
ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
placa 10 minutos
90
80
calculado
70
60
50
40
30
30.00 40.00 50.00 60.00 70.00 80.00 90.00
medido
epoxi 50 K 129.8035152
carbonato 15 a -1.26192385
dureza 77 b 0.08719658
d -0.0001034
a1 0.003750906
b1 0.000263548
placa 24 horas
100
90
calculado
80
70
60
50
40
40.00 50.00 60.00 70.00 80.00 90.00 100.00
medido
epoxi 50 K
carbonato 15 a
dureza 81 b
d
a1
b1
+ b1*(carb)^2 ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
placa 48 horas
100
calculado
90
80
70
60
50
40
80.00 90.00 40.00 50.00 60.00 70.00 80.00 90.00 100.00
medido
epoxi 50 K 127.2656603
carbonato 15 a -1.03343661
dureza 83 b 0.04464828
d 0.000386441
a1 0.002562538
b1 0.000197193
90.00 100.00
119.59540895
-0.899548353
0.097990672
6.872941E-06
0.0018760532
3.431994E-05
0.00 100.00
ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
taco 10 minutos
100
90
calculado
80
70
60
50
40
30
30 40 50 60 70 80 90 100
medido
epoxi 50 K 129.2545512
carbonato 15 a -1.14375433
dureza 80 b 0.023185848
d 0.000898352
a1 0.002921711
b1 -0.00011266
taco 24 horas
100
90
calculado
80
70
60
50
40
40 50 60 70 80 90 100
medido
epoxi 50 K
carbonato 15 a
dureza 83 b
d
a1
b1
+ b1*(carb)^2 ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
taco 48 horas
100
calculado
90
80
70
60
50
40
90 100 40 50 60 70 80 90 100
medido
epoxi 50 K 121.7088408
carbonato 15 a -0.83670161
dureza 84 b 0.020299452
d 0.000660257
a1 0.001427999
b1 -0.00010708
90 100
122.57050819
-0.902057595
0.0450347897
0.0005324026
0.001829914
-0.000186585
90 100
ShoreA = K + a*(epoxi) + b* (carb) + d*(epoxi)*(carb) + a1*(epoxi)^2 + b1
INGRESAR DATOS
10 min 24 horas
Carbonato de calcio 70 Manta 68 74
Epoxi 66 Placa 70 75
Taco 72 76
oxi)*(carb) + a1*(epoxi)^2 + b1*(carb)^2
48 horas 72 horas
75 75
76
77
FLUORESCENCIA DE RAYOS X
30.00% 2500.00% 400.00% Aspecto
200.00% Embalaje
20.00% 100.00%
200.00% 600.00%
10.00% 100.00% 100.00%
200.00% 100.00%
0.00%
es il s es s l
ra
l
bl ci v do s m na
Ca n za va Fil ici ene
cio C al En ed o
g
c M
tru Us
ns
Co
Acep 2010 Rech 2010 Acep 2011 Rech 2011
Ene 7 3 10 4 2
Feb 4 2 6 6 2
Mar 8 6 14 11 5
Abr 14 13 27 12 8
May 1 8 9
Jun 5 6 11
Jul 2 3 5
Ago 6 6 12
16 Sep 3 5 8
Oct 3 11 14
14 Nov 6 2 8
Dic 5 6 11
12
10
Acep 2010
8 Acep 2011
0
Ene Feb Mar Abr May Jun Jul Ago Sep Oct Nov Dic
30
25
0 6
0 8
0 16 20
0 20
5
15
10
0
Acep 2010 Ene Feb Mar Abr May Jun Jul Ago Sep Oct No
Acep 2011
Dic
2010
2011
Densidad
Densidad