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Composites: Part A
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Article history: Damage evolution in wound glass bre reinforced tubes due to impact (8.4 J and 14 J) and subsequent
Received 12 July 2011 biaxial cyclic loading is studied. Nominally defect-free and impact damaged specimens are compared
Received in revised form 30 November 2011 to investigate the effect of the impact damage on the fatigue life of multiaxial composites. Non-destruc-
Accepted 1 December 2011
tive inspection (air-coupled guided waves, thermography, high-speed photography, and microscopy) is
Available online 8 December 2011
applied to a subset of tubes. Air-coupled guided wave scans for characterisation of the delaminations
due to impact agree well with visual inspection. Decline in guided wave velocity is consistent to a
Keywords:
decrease in stiffness caused by fatigue damage. Using thermal imaging the impact is detectable during
A. Polymermatrix composites
B. Fatigue
cyclic loading. Strong anomalies of the surface temperature in the vicinity of the impact at the end of
B. Impact behaviour the fatigue life correspond to the initiation spot of nal failure observed by high-speed imaging. The con-
D. Non-destructive testing siderable effect of impact damage on the durability of the specimens is discussed.
2011 Elsevier Ltd. All rights reserved.
1359-835X/$ - see front matter 2011 Elsevier Ltd. All rights reserved.
doi:10.1016/j.compositesa.2011.12.002
538 F. Schmidt et al. / Composites: Part A 43 (2012) 537546
Kang and Kim [11] investigated the fatigue behaviour and variabil- damages due to impacts represent typical operational defects
ity of fatigue life in carbon/epoxy laminates with impact induced and non-destructive test inspections are applied to characterise
damage under tensile fatigue loading. A fatigue life prediction impact-induced delaminations and to monitor the evolution of fa-
model for impacted laminates was derived and veried by fatigue tigue in pre-damaged composites.
tests using constant amplitude loading. Mahinfalah and Skordahl
[12] determined the effects of hail damage on the fatigue tensile
2. Specimen preparation and pre-damage procedure
strength of a graphite/epoxy composite laminate. After impacting
by iceballs and aluminium spheres each coupon was subjected to
Nominally defect-free wound tube specimens for the investiga-
constant amplitude tensiontension fatigue. It was found that an
tion of biaxial loading fatigue are made of E-glass bre rovings
iceball impact with energy up to 27.4 J did not affect the fatigue
from Owens-Corning (OC111A) and a common resin material from
performance of this particular laminate, whereas an aluminium
Momentive (resin/hardener combination of RIM135/RIMH137 in a
(hard particle) impact at the same maximum energy signicantly
ratio of 100:30). These hollow cylinder specimens with 46 mm
degraded this material. Freeman et al. [13] investigated the low-
outer diameter, 328 mm length and approximately 2 mm wall
velocity impact properties and fatigue properties of carbon bre
thickness are produced using a custom-made winding machine
sandwich composites after impact in four point bending tests.
(enables manufacturing of arbitrary lay-ups) and resin transfer
However, the interaction of multiaxial fatigue damage mecha-
moulding (RTM). During the winding process, guide clamps with
nisms and operational defects such as impacts has been far less
pins are used for redirecting the rovings at the end of a sample
widely investigated.
and for uniform placement in arbitrary orientation angles. While
Several techniques (thermography, electric resistivity, ultra-
the rovings are wrapped around a mandrel, an integrated mecha-
sound, etc.) have been proposed for detection of manufacturing de-
nism for the adjustment of the thread tension and a variable num-
fects and operation-induced damage in composites. Optical lock-in
ber of guide rollers ensure accurate alignments and high tension.
thermography has shown to provide reliable results for detecting
The specimens consist of eight layers with a [0/45/90/45]S
delaminations in carbon bre reinforced plastic (CFRP) in a thick-
lay-up and relative mass fractions of 49% (0), 23% (45), 5% (90)
ness range of a few millimetres [14]. However, this technique fails
and 23% (45). Regarding the lay-up and the specimen congura-
for evaluation of mechanically induced stiffness degradation
tion the inner and outer 0-angled plies are parallel to the axial
caused by formation of matrix cracks. Measuring the increase in
direction of the tube specimen. Bonded steel inserts and GFRP-
electric resistivity due to evolution of matrix cracks has yielded
doublers of 70 mm length are used for reinforcement of both tube
some promising results for investigating fatigue in glass bre rein-
ends to prevent failure caused by the xing pressure of the ten-
forced plastic (GFRP) but additives such as carbon nanotubes are
siontorsion machine. In contrast to other specimen types, tube
required to provide conductivity [15]. Conventional ultrasound
specimens allow to investigate biaxial loads (combination of ten-
technique is being widely-used in industry to detect defects such
sion and torsion) with arbitrary load ratios and to prevent the
as delaminations in composites. Ultrasound attenuation and the
free-edge effect occurring in at specimens.
related stress wave factor revealed to be indicators for fatigue
For the assessment of impact related damage and its inuence
and impact damage [16]. However, this methodology involves
on the biaxial fatigue behaviour of composites, the nominally de-
structure-integrated sensors or complex coupling of the transduc-
fect-free tube specimens are pre-damaged in an impact test rig.
ers to the structural component to be tested. In recent years air-
The test rig is driven by pressurised air and consists of control pa-
coupled ultrasound in transmission conguration has been
nel, pressure tank, electrical high speed valve, barrel, velocimetry,
increasingly utilised in industrial applications such as aerospace
specimen, xture and containment (Fig. 1). An electrical controlled
engineering. Based on mode conversion between ultrasound in
valve is used to re the gun and two photoelectric beams measure
air and Lamb (guided) waves, single-sided inspection of composite
the velocity of the projectile. The specimens are clamped on both
plates was proposed [17]. Thermal and fatigue damage results in
sides. A hemispherical polyamide-projectile with a constant mass
decrease of guided wave velocity due to stiffness degradation of
of m = 100 g and diameter of 40 mm is used for low velocity im-
the composite [18]. Attenuation and phase velocity of guided
pacts with energies of 8.4 J and 14 J.
waves are sensitive to moisture content and micro-cracking [19].
Fatigue damage in tube specimens induced by mechanical cyclic
loading has been monitored using air-coupled guided waves [20]. 3. Mechanical testing
The present work investigates the effects of impact-induced
pre-damage on the damage mechanisms and fatigue behaviour The fatigue experiments are performed with a servo-hydraulic
within a German research-project (PAK 267). Pre-damaging by im- tensiontorsion machine. The theoretical maximum loads are
pacts is performed at the TU Dresden (ILK), single-sided air-cou- 250 kN in tension/compression and 2200 Nm in torsion. All fati-
pled guided wave measurements are conducted at the University gue tests are conducted in a force-controlled manner with R = 1
Stuttgart (IKT-ZfP), and mechanical testing and further non- and a frequency of 3 Hz. In order to distinguish different multiaxial
destructive testing are done at the TU Braunschweig (IFL). The load cases, a biaxiality ratio (parameter b) is introduced as follows:
Fig. 1. Impact test rig with tube specimen xture for impact pre-damage.
F. Schmidt et al. / Composites: Part A 43 (2012) 537546 539
b arctans=r 1 fatigue testing, can be related to the static failure load. For an over-
view of these relations between fatigue loads and static loads
With the normal stress r and the shear stress s, the biaxiality
Table 1 is added.
ranges from pure tension/compression (b = 0) to pure shear
In order to monitor the damage mechanisms and to estimate
(b = 90) loads. The fatigue tests discussed in this paper are per-
the fatigue behaviour, all fatigue tests are divided into three repet-
formed at two different biaxial load ratios:
itive steps (Fig. 2): a characterisation step, a fatigue damage step,
and a discrete damage monitoring step. The characterisation steps
1. b = 30: combination of tension/compression and torsion with a
are quasi-static tests at a low maximum stress level conducted
predominant tension/compression part (relation s/r is 0.58).
with force-controlled ramps (pure tension force, pure compression
2. b = 60: combination of tension/compression and torsion with
force, pure positive and negative torsion moment, respectively) in
the shear part being dominant (relation s/r is 1.73)
order to calculate the Youngs and shear modulus throughout the
fatigue tests. The required axial displacements and the torsional
Various load amplitudes are selected on the basis of biaxial sta-
angle are measured by the internal displacement sensor of the test-
tic test results. These static tests were conducted with the same
ing machine and an external laser measurement system. The
biaxiality ratio b mentioned above and a combination of tension
fatigue damage steps consist of a specic number of load cycles
and positive shear load. By using measured static strengths the
with several loading congurations involving various cyclic fatigue
various cyclic fatigue loads, which lead to low-cycle and high-cycle
Table 1
Single values of loading programme, bre-volume ratios, and lifespan for selected specimens.
Specimen b () FVR (%) r (MPa) s (MPa) Cyclic load over static Lifespan (cycles)
failure load (%)
Nominally defect-free specimens
Tube60-1 60 52.02 44.9 77.8 45 11,890
Tube60-2 60 51.32 42.2 73.1 43 33,987
Tube60-3 60 51.19 37.9 65.6 38 179,891
Tube30-1 30 50.73 122.2 70.6 43 2450
Tube30-2 30 52.08 114.3 66.0 41 10,948
Tube30-3 30 51.97 107.0 61.8 37 36,154
Specimens with impact 14 J
Tube60-14 J-1 60 57.05 29.1 50.4 30 3537
Tube60-14 J-2 60 54.49 26.3 45.5 26 23,922
Tube60-14 J-3 60 54.69 21.5 37.3 22 130,128
Tube30-14 J-1 30 53.66 74.1 42.8 26 9249
Tube30-14 J-2 30 54.62 67.2 38.8 24 25,848
Tube30-14 J-3 30 53.64 61.5 35.5 22 94,930
Specimens with impact 8.4 J
Tube60-8.4 J-1 60 52.61 29.7 51.4 30 15,721
Tube60-8.4 J-2 60 52.20 28.7 49.8 28 95,593
Tube60-8.4 J-3 60 53.25 25.1 43.4 26 143,170
Tube30-8.4 J-1 30 50.88 87.7 50.6 32 3037
Tube30-8.4 j-2 30 53.07 78.4 45.3 28 38,584
Tube30-8.4 j-3 30 54.94 73.8 42.6 26 135,588
Fig. 2. Alternating fatigue and characterisation steps with respective discrete damage monitoring.
540 F. Schmidt et al. / Composites: Part A 43 (2012) 537546
load amplitudes (sinusoidal wave form) and biaxial load ratios. The lected fatigue damage steps are depicted at the right hand side of
maximal loading of fatigue damage steps is taken as a percentage Fig. 3. Higher values of T T0 imply a higher and faster heating
of static strength. During each fatigue damage step, an infrared of the specimen during the analysed 100 sinus cycles of the se-
camera and a high resolution camera in high-speed mode are used lected fatigue damage steps. Furthermore, the thermal imaging re-
to measure surface temperatures and observe the damage evolu- veals spots with higher thermal activity (hot-spots).
tion, respectively. After several characterisation steps and fatigue
damage steps the fatigue test is stopped and the specimen is re- 4.2. Optical damage and fracture analysis
moved from the tensiontorsion machine in order to monitor in
more detail the damaged regions and the impact area (discrete During each characterisation step of the fatigue tests, digital
damage monitoring). Thus, different non-destructive test methods images are taken with a high resolution camera to observe the
such as crack monitoring with a light microscope and air-coupled qualitative crack densities along the tube specimens, the initiation
guided wave measurements can be applied. or sizes of delaminations, and the damage development caused by
impacts. Using the aluminium mirrors allows for optical imaging of
4. Methodologies for non-destructive inspection 90% of the tube surface. By using the integrated loop function of
the high resolution camera during the fatigue damage steps, the -
Aim of the current work is to observe the different damage nal fatigue fracture of each tube specimen is recorded. The camera
mechanisms (matrix cracking, delamination development, damage is triggered by the testing machine and the limit set of displace-
development caused by impacts and nal failure process) occur- ment control. Consequently, an analysis of the reason for nal fail-
ring during fatigue. Therefore, various non-destructive inspections ure (tension, compression or torsion failure and the effect of
such as thermography, optical damage and fracture analysis, crack impacts) and of the location of the fracture can be performed. In
monitoring, and air-coupled guided wave measurements are addition, circumferential photos of the tubes are used for optical
conducted. damage analysis outside of the testing machine. This allows inves-
tigation of fatigue damage such as development of delaminations
4.1. Thermography and the damage development caused by impacts in more detail.
In order to use thermography as a non-destructive test method, 4.3. Microscopy for monitoring crack densities and delamination
a cooling chamber between the clamping grips is installed, which developments
assures a constant ambient temperature of 19 C. Therefore, the
initial surface temperature of the tube specimens is also approxi- The tube specimens are transparent (similar refraction index of
mately 19 C. By using a mirror system of polished aluminium resin and glass bre) allowing for monitoring of crack densities
plates, the surface temperatures of the rear side of tube specimens with an optical microscope via transmitted light method during
can also be observed. During each fatigue damage step the heating the discrete damage monitoring step of fatigue tests. Cracks in each
of tube specimens caused by cyclic loads is measured. Since the layer orientation become visible as white lines in the respective
heating due to the considerably smaller characterisation loads is directions. Up to 15 different areas of each nominally defect-free
marginal, the tube specimens cool down to the initial surface tem- specimen and up to 20 different areas of each specimen with an
perature of approximately of 19 C during each characterisation impact are studied using an optical microscope. For adjustment
step. Therefore, heating and cooling down repeat continuously of the images these areas are marked with a black or red dot, which
during each fatigue damage step and characterisation step, respec- is visible in the middle of the images (compare Figs. 9 and 10). Ten
tively. The maximum surface temperatures of the tube specimens of these areas are close to the eld of the impact. Matrix cracks are
reach no more than 30 C preventing potential damage of the ma- counted using photographically documented cracking states and
trix due to high temperatures during each fatigue damage step. the number in each layer (0-,+45-, 90- and 45-direction) is re-
The thermographic camera is triggered by the testing machine. lated to the respective length of each direction depending on the
The surface temperatures after 100 sinus cycles of selected fatigue size of the digital image to calculate the crack densities. The result-
damage steps of different specimens are evaluated to compare the ing crack densities of each layer are average values of all observed
surface temperature development of all nominally defect-free areas.
specimens and specimens with an impact. Thereby, the average
and maximum temperature differences T T0 (subtraction of a 4.4. Air-coupled guided waves
background image taken at the initial temperature from the infra-
red image after 100 sinus cycles) of two different areas are deter- The principle of single-sided inspection using air-coupled ultra-
mined in several thermographic images (see left side of Fig. 3). sound transducers is illustrated in Fig. 4. The basis of this testing
These temperature increases T T0 after 100 sinus cycles of se- methodology is selective excitation of guided wave modes in the
Fig. 3. Typical surface distribution with evaluation areas (left) and development of surface temperature during fatigue life (right).
F. Schmidt et al. / Composites: Part A 43 (2012) 537546 541
Fig. 5. Photo of tube60-8.4 J-1 after impact (top, left); photo of tube30-14 J-2 after impact (top, right); schematic sketch of area and cross section of the main delaminations
(bottom).
Fig. 6. Amplitude area scan of tube30-14 J-2 before (left) and after impact (right).
the delamination depths. The unwrapped phase shift (Fig. 7, right) without impact damage, the impacted composite tubes fail after
reveals a decrease in velocity in vicinity of the impact spot. The a few hundred cycles. To ensure a reasonable number of load cycles
phase shift shows the typical arrangement of delaminations in- till nal failure the external biaxial loads are reduced for the pre-
duced by the impact event in the experiments. A small decrease damaged tubes. The normal stresses r (for the biaxial load ratios
in velocity due to large deep-seated delaminations on the periph- of b = 60 and 30) over the cycles till nal failure are depicted in
ery of the impact site leads to a perceptible phase shift. A large Fig. 8. For a subset of specimens (18 out of 46) with and without
phase shift and, hence, decline in velocity due to delaminations impact damage detailed information is given in Table 1. This in-
closer to the outer surface of the tube is observable in immediate volves the typical relations between fatigue and static loads, abso-
vicinity of the incident spot (compare Fig. 5, right, and Fig. 7, right). lute loading magnitudes, bre volume ratios, and number of cycles
till nal failure (the detailed data for the other specimens is very
5.2. Durability study similar and hence omitted). The results of the durability study
show that the slopes of all SN curves are nearly the same but
Forty six specimens with and without impact are investigated the stresses are considerably shifted to lower levels for pre-dam-
for the durability study. At fatigue loads used for specimens aged tubes: 33% and 26% at load ratios of b = 60 and 30, respec-
F. Schmidt et al. / Composites: Part A 43 (2012) 537546 543
Fig. 7. Deviation image between intact and impacted tube30-14 J-2 (left) and phase shift scan with colour bar using radian/p (right).
Fig. 8. Comparison SN curves (only normal stresses): specimens with and without impact (left: biaxial load ratio of b = 60; right: biaxial load ratio of b = 30).
tively for 8.4 J impacts; 44% and 36% at load ratios of b = 60 and opment of the delamination caused by the 14 J impacts throughout
30, respectively for 14 J impacts. The early nal failure at low fatigue life shows no further growth of the delamination of the
loads of all impacted specimens is initiated by the pre-damage. bottom interface of the 45/0-layers. Nevertheless, growth of the
This results in lower fatigue damage in the area outside of the im- delaminations (upper interfaces 90/45 and 0/45) near to the
pact damage, which leads to a change in damage mechanisms and 14 J impact can also be observed by visual inspection.
fatigue behaviour compared to specimens without impact (ex- Considering lower external biaxial fatigue loads (see Table 1)
plained in the next section). and comparative minor load cycles for these external biaxial fati-
gue loads due to early nal failure at low loads of all impacted
5.3. Fatigue life monitoring specimens mentioned above, less crack formation in the areas re-
mote from the impact is observed (Fig. 10). The averaged crack
The fatigue life monitoring of specimens with 8.4 J and 14 J im- densities (caused by different external biaxial load ratios and mea-
pact is studied using nominally defect-free specimens as refer- sured far away from the impact area) of the 45- and 45-layer
ence. Results of fatigue life monitoring for nominally defect-free orientation for specimens with and without impact are depicted
specimens are presented in [20]. Here, the results of crack moni- in Fig. 11 (left: biaxial load ratio of b = 60; right: biaxial load ratio
toring, stiffness degradation, air-coupled guided wave velocities, of b = 30) and plotted versus the normalised lifespan of the spec-
and thermography are only presented for specimens with an imens. The averaged crack densities of these layer orientations of
8.4 J impact. The phenomena observed throughout the fatigue specimens with impact are lower. The averaged crack densities of
tests using non-destructive testing are basically consistent with the 0- and 90-layer orientations reveal the same differences.
the 14 J impact. However, in the vicinity of the delamination caused by impact a
higher crack density in the outer 0-layer is observed (compare
Fig. 5, top). The crack densities of the other layers in the vicinity
5.3.1. Visual inspection
of the delamination are similar to averaged crack densities far
By analysis of the photographically documented cracking/
away from the impact area.
delamination states and the circumferential photos, the develop-
Consequently, the results of the delamination growth and of the
ment of matrix cracks and size of the delaminations due to an im-
crack densities in the vicinity of the delamination caused by impact
pact are observed throughout lifespan. Cracking/delamination
reveal a local effect of the impact on the damage propagation and
states of the areas of specimens with an 8.4 J impact show in some
the fatigue behaviour.
cases a growth of the delamination (Fig. 9). The size of the delam-
ination of the bottom interface of the 45/0-layers (see Fig. 5) in-
creases about 34 mm throughout fatigue life. Furthermore, the 5.3.2. Stiffness degradation
delaminations near to the impact (upper interfaces 90/45 and The stiffness degradation for specimens without impact is lar-
0/45) also increase until nal failure, which is monitored by vi- ger than the one for impacted specimens (Fig. 12). Normalised
sual inspection using the optical microscope. Looking at the devel- Youngs and shear modulus of nominally defect-free specimens
544 F. Schmidt et al. / Composites: Part A 43 (2012) 537546
Fig. 9. Tube30-8.4 J-1: circumferential images (top) at the beginning (left) and 88% (right) of lifespan; photographically documented cracking/delamination states (bottom)
and growth of the impact area after 1.5% (left), 66% (middle) and 98% (right) of lifespan.
Fig. 10. Development of matrix cracks: nominally defect-free specimen tube60-2 after 95% of lifespan (top) and rear side of specimen with impact tube60-8.4 J-1 after 98% of
lifespan (bottom).
Fig. 11. Crack densities over normalised lifespan for specimens with and without impact (left: biaxial load ratio of b = 60; right: biaxial load ratio of b = 30).
reveal the typical behaviour of a rapid decrease within the rst 10 crease of local stiffness caused by the small local critical damage
15% of lifespan followed by a slow, almost linear decrease till nal is negligible compared to the constant stiffness of the other areas
failure. The expected rapid decrease of both moduli within the last of the specimen. Due to the lower external biaxial fatigue loads
5% of the fatigue life cannot be monitored, because the rapid de- for specimens with impact (see Table 1, Fig. 8) and the lower num-
F. Schmidt et al. / Composites: Part A 43 (2012) 537546 545
Fig. 12. Normalised Youngs and shear modulus over normalised lifespan for specimens with and without impact (left: biaxial load ratio of b = 60; right: biaxial load ratio of
b = 30).
Fig. 13. Normalised guided wave velocity throughout normalised lifespan for specimens with and without impact (left: biaxial load ratio of b = 60; right: biaxial load ratio of
b = 30).
Fig. 14. Temperature development over normalised lifespan for specimens with and without impact (left: biaxial load ratio of b = 60; right: biaxial load ratio of b = 30).
ber of matrix cracks in the areas away from the impact (Fig. 11), change in the area damaged by the impact. The interfaces impede
the Youngs and the shear modulus decrease more slowly and re- light and ultrasound transmission thereby hampering visual and
main at higher values till nal failure. ultrasonic monitoring of damage advancement in the area of
delaminations.
5.3.3. Air-coupled guided waves velocities
The decrease in guided wave velocity (Fig. 13) corresponds to
the observed stiffness degradation (Fig. 12) due to cyclic loading 5.3.4. Thermography/optical fracture analysis
for both the defect-free and the impacted specimen. A steep des- Similar to the stiffness degradation of nominally defect-free
cent in velocity within the rst 10% of the lifetime merges to a specimens, the average and maximum surface temperatures
gradual decrease till catastrophic failure. The difference in stiffness (T T0) of nominally defect-free specimens (analysed after the rst
degradation between the nominally defect-free and the impacted 100 sinus cycles of selected fatigue damage steps) decrease within
tube over their lifetimes agrees well with the decline in velocity the rst 1015% of lifespan (Fig. 14). In this phase of the fatigue life,
which is large (78%) for the nominally defect-free and small higher energy dissipation (heating) occurs due to the crack initia-
(about 2%) for the impacted specimen. A standard deviation of tion and propagation and shows a decrease due to crack saturation.
1.3 m/s (0.1%) was calculated as discussed in Section 4. Following this decrease in thermal energy dissipation and after
Visual inspections of 8.4 J impacted specimens reveal if any matrix cracks reach saturation (compare Fig. 11), a uniform devel-
only small delamination growth of a few millimetres, which is opment of heating is measured. Throughout that part of lifespan
observed using air-coupled guided waves as well. During cyclic local delaminations initiate randomly along the nominally defect-
loading and even just before catastrophic failure, visual as well free specimens and grow concurrently. The critical local damage
as ultrasonic inspection showed only a minor (hard to characterise) leads to a local temperature increase (hot-spot) and therefore,
546 F. Schmidt et al. / Composites: Part A 43 (2012) 537546
lower external fatigue loads for specimens with impact the average
crack densities (in the areas remote from the impact), the stiffness
degradation and the surface temperature development differed
from nominally defect-free specimens. All specimens with impacts
showed less fatigue damage (crack density, stiffness degradation
and corresponding guided wave velocity drop). The delamination
due to these low velocity impacts caused the earlier catastrophic
failure which has been revealed by thermography and optical frac-
ture analysis. Specimens with impacts showed an earlier develop-
ment of areas with higher thermal activity (within the last 2025%
of lifespan) compared to nominally defect-free specimens (areas
with higher thermal activity within the last 10% of lifespan). Hence,
thermography can be applied for the detection of fatigue damages
and impact damages being crucial for nal failure in an early stage
of lifespan. The air-coupled guided wave has revealed to be a
promising measure for fatigue damage state even for applications
where stiffness measurements and crack counting is hampered.
Acknowledgements
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