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1. GENERAL 3
2. INITIAL OPERATION 4
2.1. Configuration of the calibration equipment 4
3. DETERMINATION OF THE INITAL
CONTAMINATION LEVEL 4
3.1. Preparation of the flushing solution 4
3.2. Measuring the flushing solution 5
3.3. Calculating ideal numbers of particles 7
4. CALIBRATION 8
4.1. Automatic calibration programm AK 11 8
4.2. Preparation of the calibration solution 9
4.3. Measuring of the calibration solution 9
2
1. General
Automatic calibration is carried out using a CCS2 and a
BSS2 in combination with the INT-Software CALSOFT 01.
Based on ISO 11171 CALSUS 01, a fluid for secondary
calibration, is needing during this process.
Comments:
The drifting of calibration values over time is rather
insignificant.
If drastic changes of calibration values (more than 100%)
occur, malfunction is suspected. Especially if very low
values are determined. In such cases it is to assume that
partial contamination of the sensor or contaminations of
the windows are the reason.
3
2. Initial operation
4
Notice:
Be aware of the fact that this process has to be performed
quickly in order to ensure that particles are spread out even
within the sample. This is important for accurate and constant
measurements.
5
Now open the valve of the BSS 2, flush with [2]
(approximate 3 – 4), stop the flushing with [5] and start the
count by hitting [3] on the CCS 2.
Shut the valve of the BSS 2 again when finished with the
measurements.
6
3.3. Calculating ideal numbers of particles
XN = (XZ - XA) x 10
XZ = 6475 particles / 1 ml
XA = 358 particles / 1 ml
XN = (6475 – 358) x 10
= 61170 particles / 10 ml
7
4. Calibration
The purpose is to align the actual and the ideal numbers
of particles.
Activate the input box by hitting [F2], delete the old value
with [DEL] and after entering the ideal value confirm by
hitting [F2] again.
After entering all ideal values close this menu by hitting [5].
8
4.2. Preparation of the calibration solution
Agitate the calibration solution moderately for app. 10
minutes in all directions.
green: 1,5 %
yellow: 3%
red: > 3%
9
Redo the calibration until ideal and actual values of the
measuring channels: > 4 µm, > 4,6 µm, > 6 µm, > 6,4
µm, > 10 µm, > 14 µm do not differ more than 1.5%.
(b) Print-out:
Print your values by hitting [F1].
10
Notice: Unstable values are an indication for insufficient
preparation and/or bad handling of the solution for calibration.
Careful preparation of samples will result in successful
calibration!
After you are done the calibration please flush the BSS
2 and the CCS 2 with cleanded mineral oil ISO VG 22.
11
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