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Abstract
The mechanical properties of open-cell 6101 aluminum foams with different densities ( 5 – 10%) and morphologies (4–16 cells
cm − 1) were characterized in compression. It was found that density is the primary variable controlling the modulus and yield
strength of foams. The effects of other variables such as cell size and shape were also studied. Whereas the cell size appears to
have a negligible effect on the strength of foams, at a fixed density, the cell shape was shown to effect the strength of foams. In
the present paper, theoretical models are offered to explain the differences in modulus and strength caused by the differences in
cell shape and size. © 2000 Elsevier Science S.A. All rights reserved.
0921-5093/00/$ - see front matter © 2000 Elsevier Science S.A. All rights reserved.
PII: S 0 9 2 1 - 5 0 9 3 ( 0 0 ) 0 0 6 2 3 - 7
106 T.G. Nieh et al. / Materials Science and Engineering A283 (2000) 105–110
Al–5 Ca–3Ti alloy foam and a open-cell AZ91 (Mg–9 from A1 6101. The use of end plates is to assure
wt.%Al–l wt.% Zn – 0.2 wt.%Mn) alloy foam under a loading alignment between a test sample and the upper/
dynamic strain rate (\103 s − 1). In both cases, it was lower platforms of testing frame, and the ease of han-
found that the plateau stress of the foam materials dling low-density foams. Since the modulus and yield
exhibited a high strain rate sensitivity. Also, the absorp- strength increase rapidly with relative density (Eqs. (1)
tion energy at the dynamic strain rate of 103 s − 1 is and (2)), the facing plates can be approximately treated
significantly higher (by about 150 – 200%) than that as rigid bodies. The constraint to lateral expansion of
obtained at the quasi-static strain rate of 10 − 3 s − 1. the foam during testing may be appreciable at a large
In attempts to understand the mechanical response of plastic strain, but is expected to be small in the initial
foam materials under load, a number of micromechani- loading where data of elastic modulus and yield
cal models have been developed [23 – 25]. For example, strength were taken. For discussion purposes, these
considering bending, Young’s modulus, E, for an open- foams will be designated by: relative density/cpi/orien-
cell foam is related to its relative density through the tation, herein. For example, a foam with a 9% relative
equation: density, 40 cell per inch, and that is tested in a direction
perpendicular to the solidification direction is desig-
E r 2
=A (1) nated by 9/40/T.
E0 r0
For synchrotron X-ray tomography, foam samples
where A 1 [26], E0 is the modulus of the fully dense with dimensions of 10× 10× 10 mm were sliced. X-ray
solid, r is the density of the foam, and r0 is the density measurements were carried out using a beam source at
of the solid from which the foam is made. The plastic SSRL (Stanford Synchrotron Radiation Laboratory).
yield stress, s*pl, is also a function of the relative den- The morphology of the foams was also characterized
sity, specifically, using a conventional scanning electron microscope
(SEM). The pore size is defined as the average value of
spl r 3/2
:0.3 (2) the linear dimension of cell across cell faces. The aver-
sys r0 age value was determined by measuring the statistical
where sys stands for the yield stress of the fully dense values from X-ray tomographs.
material [26]. It is obvious from the above two equa- Compression tests were performed directly from the
tions that the single most important structural charac- as-received specimens. The direct measurement of the
teristic of a cellular solid is its relative density, r/r0. elastic modulus from a foam material has subtle aspects
Recently, Nieh et al. [2] studied the elastic properties because of the difficulties associated with sample align-
of an open-cell aluminum alloy (A1 6101-T6). The ment at low loads and the attachment of a strain gage
synchrotron tomographic images indicated that the 3D to the sample. In the present investigation, three exten-
cell structure was slightly anisotropic (8%), and spe- someters were attached, each 120° apart, to measure the
cifically cells were found to be slightly elongated in one displacement of the two faceplates. The crosshead
orientation. Interestingly, both the calculated and mea- movement was monitored by a computer equipped with
sured Young’s moduli along the ‘hard’ axis of the foam a data acquisition system that controlled tests under
was also found to be 5 – 10% larger than that along the either constant crosshead speed or constant true strain
other two ‘soft’ axes. Apparently, cellular morphology rate conditions. Average strain was obtained from the
affects the properties of a foam. In the present paper, readings of the three extensometers. Several loading-un-
we present the effects of cell size and shape, in addition loading steps were taken to obtain the Young’s mod-
to density, on the compressive properties of open-cell ulus and the variation of data is about 9 25 MPa. It
AA6101 aluminum foams. will be shown in the Results section, that this variation
may be acceptable for the ‘high-density’ foams but is
quite significant for the ‘low-density’ foams. Compres-
2. Experimental procedures sion tests were terminated typically at a compression
strain of about 0.8 at which point extensive densifica-
In this study, 6101 aluminum foams (composition tion of the test sample had occurred.
(wt.%) A1–0.6 Mg – 0.5 Si) were fabricated by ERG,
Inc. using a directional solidification technique. These
foams have a relative density ranging from 5 to 10%, 3. Results
cell size from 10 to 40 cell inch − 1 (cpi), and an orienta-
tion that is either longitudinal (L) or transverse (T) to 3.1. Structure and morphology
the solidification direction. The foams were provided in
a cubic shape (dimension: 75×75 ×50 mm). Both the An SEM micrograph of a foam with a relative den-
top and bottom of these compression samples are sity of 6% is shown in Fig. 1. The foam has an open-cell
bonded with 12.5 mm-thick facing plates, also made structure and the cell geometry is remarkably uniform.
T.G. Nieh et al. / Materials Science and Engineering A283 (2000) 105–110 107
The pore size and ligament diameter are about 2.5 and
0.4 mm, respectively. The microstructure of the foam is
shown in Fig. 2, which is a typical cast microstructure
containing large grains and coarse inclusions. Grains
are so large that they often extend across the entire
ligament between cells. The inclusions, analyzed by
EDX, are Fe–Si – A1 particles commonly observed in
6000-series aluminum alloys. No internal voids were
observed within these ligaments.
To examine the 3D connectivity of the foam, syn-
chrotron X-ray tomography was conducted. X-ray to-
mographs of a porous aluminum foam (sample
dimension: 10× 10 × 10 mm) were readily thresholded
into binary images of metal and pore space (see Fig. 3).
Because of the exceptionally high contrast between
metal and pore space there is a broad range of possible
threshold values which lead to nearly identical struc-
Table 1
Properties of AA6101 aluminum foams with different morphologiesa
a
Modulus and yield strength of Al 6101-T6 are 70.3 GPa and 193 MPa, respectively.
T.G. Nieh et al. / Materials Science and Engineering A283 (2000) 105–110 109
as: t%4, Eq. (4) is reduced to
4
El h% t Et t%4
= Cl (3) = Ct 4 (5)
E0 h h E0 h%
where I is the moment of inertia which is proportional Combine Eqs. (3) and (4), and assume Ct =Cl, it
follows that
Et h (t%/h%)4
= · (6)
El h% (t/h)4
Further assume a constant local density, i.e. t%2h%=t 2h,
Eq. (6) can be readily reduced to
5 4
Et h t%
= · B1 (7)
El h% t
since h/h% B1 (and t/t% B1). That is, the longitudinal
modulus is higher than the transverse modulus. In a
similar manner, it can be readily demonstrated that the
elastic collapse stress (yield stress) in the longitudinal
direction is higher than that in the transverse direction,
i.e.
s*ys(t) B s*ys(l) (8)
This explains why the longitudinal orientation has a
Fig. 7. A rectangular unit cell loaded in the longitudinal direction. higher strength than the transverse orientation. In the
110 T.G. Nieh et al. / Materials Science and Engineering A283 (2000) 105–110