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Chemistry 11
Titration Lab Report
Suparuek Saetoen
Parinada Suriyaworakul
Phatsakorn Rodphol
Wanwarisa Krittiyasrisumet
Natanicha Sangprakai
Tanakom Kaweewuthisinp
ABSTRACT
In this experiment, we did a titration which is
the method that we add the base solution to
make the unknown solution become neutral. In
another way, we want to know the amount of the
unknown so we use the solution that we known
to measure it. The pH of the mixed solution will
be different depends on the indicator that we
use. To start the experiment, we have to clean all
of the glassware that we want to use in the
experiment. For the buret and pipette, we have to
clean it by the solution that we want to use by
them. On the other hand, the beaker and flask
that we use can be cleaned with the distilled
water. After we done with the cleaning part, we
have to do the rough titration first to estimate the
amount of base that we need to change the color
of the solution. After that, we can do the real
titration and slow down when the amount of base
we use is close to the rough titration amount.
ABSTRACT
MY SCHEDULE
The color that we want it to be is green for
the Bromophenol Blue indicator and light pink
for Phenolphthalein which means endpoint of
the solution. We have three Erlenmeyer flasks
for each indicator. Therefore, we have three
chances to do the titration. The end point is
when the color of the solution is over the
endpoint. The pH result of the Bromophenol
Blue indicator that we got is 3.64 which is the
endpoint compared to the table. 5.03 ml of
NaOH is added to make the solution with
Bromophenol blue indicator reaches the
endpoint. Also, 5.15 ml of NaOH is added, so the
pH result of the Phenolphthalein indicator of
our group is 8.19, which is also the endpoint for
this indicator.
O b j e c t i v e
M = mol/L
M = 0.00423 / 0.01
M = 0.423 M
DATA&
CALCULATION
DATA&
CALCULATION
Phenolphthalein
Trial 1:
NaOH: HCl:
Amount = 5.30 mL = 0.0053 L Amount = 10 mL = 0.01 L
Molarity = 0.1 M Molarity = ______ M
Trial 2:
NaOH: HCl:
Amount = 5.15 mL = 0.00515 L Amount = 10 mL = 0.01 L
Molarity = 0.1 M Molarity = ______ M
Trial 2:
NaOH: HCl:
Amount = 5.03 mL = 0.00503 L Amount = 10 mL = 0.01 L
Molarity = 0.1 M Molarity = ______ M
pipette?
concentration.
DISCUSSION
POST-LAB
the vinegar?
NaOH: CH3COOH:
= 2.2930.00908 M = 0.84 M
Mol = 0.021
Error
We found the error in both indicator group. In
the first group that uses Bromophenol Blue as
an indicator found that we drop the base
solution too fast. In the second titration after the
rough titration, we drop base solution to the
point that we have to slow down. However, the
record of the amount of solution that we use in
rough titration is not clear. Also, we did not pay
as much attention as we should to it. So, we did
not slow down the drop to one drop or half
dropper time that make our color changed to
purple. We tried to shake it but the color does
not change. However, we got the perfect titrate
for the third trial.
For phenolphthalein titration, our solution
turned pale pink once, so we thought that it had
reached the endpoint. However, after we swirled
it for several times, the color disappeared.
CONCLUSION
This lab report is discussing the titration. Titration
is used to calculate the concentration of the
unknown solution. In the experiment, approximately
0.515 mL (0.000515 mol) of NaOH is used to turn
unknown- concentration HCl with Phenolphthalein
indicator from clear color into a light pink, implying
there are 0.000515 moles of H+. The concentration of
acid can be calculated using this the concentration
of H+ that we get, and it is around 0.0515 M. For
Bromophenol Blue, around 0.53 mL (0.00053 mol) of
NaOH is used to change unknown-concentration HCl
mixed with Bromophenol Blue from yellow to light
green, which means there are 0.000503 moles of H+
and its concentration is about 0.0503 M. According to
the experiment and calculation, the concentration of
acid solution - HCl - is roughly the same, even
though, the different volume of basic is added.
This lab report is discussing the titration. Titration
is used to calculate the concentration of the
unknown solution. In the experiment, approximately
0.515 mL (0.000515 mol) of NaOH is used to turn
unknown- concentration HCl with Phenolphthalein
indicator into a light pink, implying there are
0.000515 moles of H+. The concentration of acid can
be calculated using this the concentration of H+ that
we get, and it is around 0.0515.
SUGGESTION
In the next experiment, our group
suggests doing the titration slower
and more carefully even in the first
rough titration, because it provides
us with the more accurate amount of
the titrant needed for the next rough
titration. Another suggestion is to
ensure that the solution completely
reaches the endpoint. In some case,
the solution that seems to already
reach the endpoint and change the
colour of the indicator will restore its
original colour after resting or
shaking for a while, because the
reaction needs time, be patient!
REFERENCE
- Acid - Base Indicators and Titrations. (n.d.)
Retrieved 27 January 2018, from:
http://www.ch.ic.ac.uk/vchemlib/course/indi/