ae BEFORE THE dort STATE OF CALIFORNIA OCCUPATIONAL SAFETY AND HEALTH APPEALS BOARD RECEIVED DEC i 1 2H Jn the Matter of the Appeal of: piri Cal / OSHA MONROVIA EXIDE TECHNOLOGIES - LOS ANGELES BATTERY RECYCLING 2700 South Indiana Street Vernon, CA 90023 DOCKET 08-R4D2-3842 Employer ORDER Good cause having been shown, the stipulation of the parties quoted below is accepted and the matter is resolved as set forth below and in the attached summary table. The undersigned granted the Division's motion (without objection) to amend the alleged violation description of Citation 1, Item 3, to read as follows: “At the time of inspection, it was determined that a shelf next to the telephone in the Smelter Control Room on the east side of the facility located at 2700 South Indiana Street, Vernon, was not maintained as free as practicable of accumulations of lead.” ‘The parties herein agreed as follows: It is stipulated by and between the parties that this stipulation and the terms and conditions set forth herein are not intended to be and shall not be construed by anyone as an admission of any wrongdoing whatsoever by Appellant, except for purposes of administration and enforcement of the California Occupational Safety and Health Act in proceedings before the Appeals Board, and that the stipulation shall not be used in any other proceeding between the parties or involving any other person, whether said proceeding be legal, equitable, or administrative in nature.The parties further stipulate that no findings or coriclusions have been made by any trier-of-fact regarding the citations and fines at issue herein. ‘The parties further stipulate that Appellant has entered into this agreement in order to avoid protracted litigation and costs associated thereto. IT IS SO ORDERED. DATED: December 9, 2008 Ursula L’Clemons Administrative Law Judge ULC:ao Pursuant to § 364.2(d), Title 8 California Code of Regulations, Employer shall post for 15 working days a copy of this Order. Pursuant to § 364.2(b), Title 8 California Code of Regulations, the Division shall serve a copy of this disposition on any authorized employee representative if known to the Division to represent affected employees.SUMMARY TABLE ORDER “Abbreviation Key: In the Matter of the Appeal of: G=General S=Serious EXIDE TECHNOLOGIES - LOS ANGELES BATTERY RECYCLING Er-Employer — DOSH=Division Docket 08-R4D2-3842 [IMIS No. 310491881 Site: 2700 South Indiana Street, Vernon, CA 90020 Date of Inspection: 06/18/2008-08/29/2008 Citation Issued: 09/08/2008 pockxer |c]1| section | T ALLEGED VIOLATION DESCRIPTION | A|Vv| PENALTY | PENALTY | FINAL, if Y MODIFICATION OR WITHDRAWAL F | A| proposeD | PROPOSED | PENALTY TIE P AND REASON F|C| pyposH | pyposH | ASSESSED A\M E yA IN ATPRE- | BY BOARD T R|T| crraTION | HEARING 1 MIE ° E|D N D 08-R4D2-3842 | 1 [3 | SI9siNNIT) | G | [Failure to maintain surface areafree of |X| |S 280/S 280] 6 260 accumulations of lead] Er withdrew appeal ‘Sub-Total S280 [$280 | $ 280 ‘Total Amount Due* S280 NOTE: Payment of final penalty amount should be (INCLUDES APPEALED CITATIONS ONLY) made to: Accounting Office (OSH) *You will owe more than this amount if you did not appeal one or more citations or items containing penalties. Department of Industrial Relation Please call (415) 703-4296 if you have any questions. P.O. Box 420603 San Fh Ca 94142 ALJ:ULC/a0 POS: 12/09/2008DECLARATION OF SERVICE BY MAIL I, the undersigned, declare as follows: lam a citizen of the United States, over the age of 18 years and not a party to the within action; my place of employment and business address is Occupational Safety and Health Appeals Board, 100 North Barranca Street, Suite 410, West Covina, California, 91791. On December 9, 2008, I served the attached Order by placing a true copy thereof in an envelope addressed (o the persons named below at the address set out immediately below each respective name, and by sealing and depositing said envelope in the United States Mail at West Covina, California, with first-class postage thereon fully prepaid. There is delivery service by United States Mail at each of the places so addressed, or there is regular communication by mail between the place of mailing and each of the places so addressed: Kenneth Copeland, Plant Manager EXIDE TECHNOLOGY; LOS ANGELES BATTERY RECYCLING 2700 South Indiana Street Vernon, CA 90023 District Manager DOSH - Monrovia 750 Royal Oaks Drive, Suite 104 Monrovia, CA 91016 Mike Mason - Chief Counsel DOSH - Legal Unit 1515 Clay Street, 19 Floor Oakland, CA 94612 DOSH - Legal Unit 320 W. Fourth Street, Suite 400 Los Angeles, CA 90013 I declare under penalty of perjury that the foregoing is true and correct. Executed on December 9, 2608, at West Covina, California. Bea rant JaoSTATE OF CALIFORNIA oe @ AND HEALTH APPEALS BOARD 2820 VENTURE OAKS WAY, SUITE 300 SACRAMENTO, CA95822 (916) 274-5751 FAX 1916) 274-5785 October 3 1, 2008 Kenneth Copeland, Plant Manager EXIDE TECHNOLOGY; LOS ANGELES BATTERY RECYCLING 2700 South Indiana Street Dockered 09/30/08 VERNON, CA 90023 Re: 08-R4D2-3842 Wov 3 200 yniel Dear Mr, Copeland Enclosed are the docketed copies of each Appeal form that you filed with the Board. The above listed docket numbers should appear on all future correspondence. A copy of any correspondence with the Appeals Board must be served on the Division of Occupational Safety and Health DOSH and any other party to the proceeding You are obligated to notify any affected employees or their representative that an appeal is pending and that they have a right to participate in the proceeding, You are required to past a copy of the docketed Appeal form and a Participation Notice (similar to the sample enclosed) at or near the site of the violation or in a conspicuous place where it will be readily observable by employees. In addition to posting, a copy of the Appeal form and the Participation Notice must be served on the following: 1) any authorized employee representative and 2) any employee lor their representative] who Was seriously injured or killed in an accident related to this appeal. Proof, such as a brief letter, that the forms were posted must be sent to the DOSH District Manager whose address appears on the citation aay Please direct any request for information dealing with the filing of your appeal to the above address and/or telephone number, All other communications prior to the hearing will be handled by the assigned Administrative Law Judge (ALJ) Ursula Clemons (626) 332-1145. Any written motion, such as a request for subpoena, consolidation of cases, or request for party or intervex status must be made by written motion to the ALJ named above at 2520 Venture Oaks Wav, Suite 300. Sacramento, CA 95833 Sincerely, Renee Robinson Office Technician ce: Accounting DOSH District Manager-Monrovia DOSH Legal Unit-San Francisco ! DOSH Legal Unit-Los Angeles IMIS# 310491881OCCUPATIO}.. «. SAFETY AND HEALTH A ec ALS BOARD Venture Oaks Way, Suite 300 Sacramento. CA 95833 . (916) 2745751 RECEIVED PAN 16) 2245785 APPEAL FORM SEP 29 2m OSH Appeals Boarc immanent — -: 2008-R4+DA- 3842 (de Teco Lo ge airy Raye Dns 1. You only have 15 working days Employer Name on Citation from receipt of a citation to appeal. Samo As Above 2. A copy of this form must be attached to each citation or notification appealed. Failure to file a completed form may result Employer Legal Name or DBA (Optional) Address 2700 South indiana Sweet vernon, CA 90023 FIRST READ IMPORTANT INFORMATION ON THE REVERSE SIDE. ‘THEN COMPLETE ONE APPEAL FORM FOR EACH CITATION 1. This isan Appeal from [-ICITATION NOK 4 tem No(s: 2 | [NOTIFICATION OF FAILUREYO ABATE ALLEGED VIOLATION CITATION NOs ‘usm Novs: ECIAL ORDERISPECIAL ACTION NO: Thema No(s Specific uroundts or this appeal are (Cheek al that apply) |. [The safer onder was not violated [The classification i. serious. will repeat) is income. [the abatement requirements ae unreasonable [Required changes | [Time allowed to compte changes |} The proposed penalty is unreasonable Explain any other reasons for appeal or issues to be raised on appeal irmative defenses must be specifically sted ‘Some important affiemative defenses ar ised on the OSHAB website a: hlpswwwdir.es.2o.OSHABVoshab um] ‘Tre station references @ wipe sample result of 140 oles as the basis for he ctaton. Exide is unaware of any surface lovotwine sample ent for ead or indus! cotings that would apply for comparsan this real as an nckcator of compliance wth the housekeeping requirements of Tle 8 CCR secon 5196.. tee hf (Signatur of Employer or Exploye"s Rep Hf there i any change in representation after you fi aa our gp you nus. ot the Appeals Boar in wt Kenneth Copeland Tipe or princ rae) Plant Manager Titer 2700 South Indiana Street (Adatress) {Address where all communications from the Appeals Board will be sent) Vernon CA 90023 (Ci) (Sta (Zip Code) (323) 262-1101 kenneth.copeland@exide.com 9/25/08 (Telephone) (E-Mail Address) (Dae) {All comespondence from the Appeals Board will Be sent tothe representative ahove a the address above, I there is any change in addres, telephone number, andor e-mail address afte you file your appesi you must molly the Appeals Board ‘of the change(s). All such notifications must be in writing} IMPORTANT INFORMATION A. Use this form o appeal a Citation, Notification of Failure ts Abute Alleged Violation, or Special OrdeeSpecial Action 1B, You must complete a separate appeal form far cach ciation or notification you wish wo appeal and atach a copy ofthe complete cation oF notification that vou are appealing. 1 the ciation ornotitieation being appealed includes more than one item do mot use separate appeals forms for each item, Instead, spovify the items you are appealing vn te space provided in No, 1m the Iront ofthis form, (fr example, “Citation No. 1, em Nos. 2, 5 and 8) D. Besure t sign your appeal form and provide al the information requested in No, 4 above, TE. Yourappea! form shall be deemed no: completed unless you ata a copy of each citation oF notification tha you are appealing. and failure to fle a completed appeal orm may result in dismissal othe appeal F. Ifyou or your representative change address, telephone number, andor e-mail addres itis your responsibilty to notify the Appeals Board in writing of the ebangets). Otherwise the Appeals Board will continue to use the address it has on File and you risk not receiving notices or other communications irom the Appeals Board. Appeals Board reaulations make it the employer's ‘obligation to notty the Appeals Board of any changes w the employer's andlor represemative’s cont: information, G. Mail each completed Appeal fore and citation or notiication tothe Occupational Safety and Health Appeals Board. 2520 Veenture Oaks Way, Ste 300, Sacramento. CA 95833, 4 “Late appeals will not be accepted unless ood cause is shown, OSHAB S/08:State of California Inspection Number: 310491881 Division of Occupational Safety and Health Inspection Dates: 06/18/2008 -08/29/2008 Monrovia District Office (0950642; 4042) Issuance Date: 09/08/2008 750 Royal Oaks Drive, Suite #104 CSHO ID: D1549 Monrovia, Ca 91016 Optional Inspection Nbr: 068-08 RECEIVED Citation and Notification of Penalty SEP 28 2008 OSH Appeals Boart Company Name: Exide Technologies; Los Angeles Battery Recycling Inspection Site: 2700 South indiana Street, Vernon, CA 90020 Citation 1 Item 3 Type of Violation: General CALIFORNIA CODE OF REGULATIONS; TITLE 8 Subchapter 7. General Industry Safety Orders Group 16. Control of Hazardous Substances Article 109, Hazardous Substances and Processes Section 5198 (h)(1) Housekeeping. Surfaces. All surfaces shall be maintained as free as practicable of accumulations of lead. VIOLATION At the time of the inspection, it was determined that a shelf next to a telephone in the smelter control room on the east side of the facility located at 2700 South Indiana Street, Vernon, had a lead dust contamination level of 140 micrograms lead per cubic centemeter of area, and that said room was a “clean zone" under positive ventilation pressure, and that such area Was not maintained as free as practicable of accumulations of lead. Date By Which Violation Must be Abated: ABATED Proposed Penalty: s 280.00 See pages I through 4 of this Citation and Notification of Penalty for information on employer and employee rights and responsibilities, Citation and Notification of Penalty Page § of 9 CaVlOSHA:2 Rev 7107eXIDE TECHNOLOGIES RECEIVEp SEP 29 2008 September 26, 2008 Department of Industrial Relations Occupational Safety and Health Appeals Board OSH Appeais Board 2520 Ventura Oaks Way, Suite 300 i Sacramento, CA 95833 Re: _ Inspection Number 310491881 Certified Letter/Return Receipt Number: 7006 2150 0003 1247 9836 Dear Appeals Board Member: Exide Technologies hereby provides your office with the completed appeal form for Citation 1 Item 3. Item 3 references a wipe sample result of 140ug/cc as a basis for the citations. Exide is unaware of any surface level wipe sample limit as an indicator of compliance with the housekeeping requirements of Title 8 CCR section 5198. (Exide Technologies petitions the board to either withdraw item 3 from the record or remove the reference of the sample test result.) 1. Citation 1 Item 3Type of Violation: General California Code of Regulations: Title 8 Subchapter 7. General Industry Safety Orders Group 16, Control of Hazardous Substances Article 109. Hazardous Substances and Processes Section 5198 (h) (1) Housekeeping Should you have any questions, please fee! Sree to contact me at 323-262-1101 Ext 2175 Sincerely, ZO Kenneth Copeland Exide Technologies Plant Manager Vernon, California Ce: _ F. Ganster/ Exide Technologies J, Bolea/Exide Technologies ‘Mark Pisani/DOSH District Manager08/22/2008 14:48 FAX 16263594291 CAL /OSHA_MONROVEA Boot seevereersreeseereete wrx TK REPORT x aexeaetaesesssieninty TRANSMISSION OK TX/RX NO 2089 DESTINATION TEL # 313292620642 DESTINATION To ST, TINE 99/22 14:57 TIME USE gorat PAGES SENT 2 RESULT ox State of Calitomia Amold Schwargenogger, Governor Department of Industrial Relations DIVISION OF OCCUPATIONAL SAFETY AND HEALTH 780 Royal Oaks Drive, Suite 104 Monrovia, CA 91016 Tol.# (626) 256-7919 Fax # (626) 359-4291 ‘September 19, 2008 Vieney Mendez Exide Technologies; Los Angeles Rottery Recycling 2700 South indiana Streat Vernon, CA 86020 Dear Employer: Pursuant to your recent request of September 19, 2008, the Division of Occupational Safety and Health will hold an informal conference. The informal conference is schaduled as follows: Date: October 14, 2008 Time: 10:00 A.M. Place; DOSH Monrovia District Office 750 Royal Oaks Drive, Suite 104 Monrovia, CA 31016 It is the responsibility of the employer to notify affected employees, or thelr representatives, of the date, time and locetion of the informal conference and to encourage tham ta attend. Perticipation by the employer, an employee or an employee's representative in an informal conference does not expand or diminish the rights of the employer, the employee or the employee's representative in a praceading before the Occupational Safety and Health Appeals Board, If an employer wishes to appeal a Citation and Notification of Penalty, the empfayer must file an appeal with the Occupational Sefety and Health Appeals Board in Sacramento within fifteen (15) days of the date ofJanet Castelo Subject: {Exide Technologies; Los Angeles Battery Recycling 310491881 (01549) Location: 1549 Tue 10/14/2008 10:00 AM Tue 10/14/2008 10:30 AM (none) Meeting organizer Mark Pisani; Paul Grier; Tomas Micheo; Edward Valdivia Categories: Informal Conference VIANEY MENDEZ TEL 323-262-1101 X276 FAX 323-262-0642State of California Arnold Schwarzenegger, Governor Department of Industrial Relations DIVISION OF OCCUPATIONAL SAFETY AND HEALTH 750 Royal Oaks Drive, Suite 104 Monrovia, CA 91018 Tel.# 1626) 256-7913 Fax # (626) 359-4291 September 19, 2008 Vianey Mendez Exide Technologies; Los Angeles Battery Recycling 2700 South Indiana Street Vernon, CA 90020 Dear Employer: Pursuant to your recent request of September 19, 2008, the Division of Occupational Safety and Health will hold an informal conference. The informal conference is scheduled as follows: Date: October 14, 2008 Time: 10:00 A.M Place: DOSH Monrovia District Office 750 Royal Oaks Drive, Suite 104 Monrovia, CA 91016 It is the responsibility of the employer to notify affected employees, or their representatives, of the date, time and location of the informal conference and to encourage them to attend. Participation by the employer, an. ‘employee or an employee's representative in an informal conference does not expand or diminish the rights of the employer, the employee or the employee's representative in a proceeding before the Occupational Safety and Health Appeals Board. If an employer wishes to appeal a Citation and Notification of Penalty, the employer must file an appeal with ‘the Occupational Safety and Health Appeals Board in Sacramento within fifteen (15) days of the dete of ‘ocourrence of the Citation. The Occurrence of the informal conference does not affect the employer's right to file an appeal with the Occupational Safety and Health Appeals Board. DISABILITY ACCOMMODATION Disability accommodetion is available upon request. Any person with a disability requiring an accommodation, auxiliary aid or service, or a modification of policies or procedures to ensure effective communication and access to the programs of the division of Occupational Safety and Health, should contact the Disability Accommodation Coordinator at the local district office or the Statewide Disability Accommodation Coordinator at 1-866-326-1616 (toll free). The Statewide Coordinator can also be reached through the California Relay Service, by dialing 711 or 1-800-735-2929 (TTY) or 1-800-855-3000 (TTY-Spanish),Exide Technologies; Los Angeles Battery Recycling Page 2 Accommodations can include modifications of policies or procedures or provision of auxiliary aids or services. Accommedations include, but are not limited to an, Assertive Listening System (ALS), a Computer-Aided Transcription System or Communication Access Realtime Translation (CART), a sign-language interpreter, documents in Braille, large print or on computer disk, and audio cassette recording. o Accommodation requests should be made as soon as possible. Requests for an ALS or CART should be made no ‘ater than five (5) days before the hearing or conference, Please bring with you to informal conference any documents which you beliave are relevant. Sincprely, lt Mark Pisani District Manager fic File No. 310491881-01549-068-08STATE OF CALIFORNIA Resor SONROVIA District Ofte - CaLOSHA DEPARTMENT OF INDUSTRIAL RELATIONS Royal Oaks Drive, st #108 DIVISION OF OCCUPATIONAL SHEETY AND TH avin, C4 31046 ‘ran ce) 266913, EMPLOYER'S SIGNED STATEMENT OF ABATEMENT OF REGULATORY AND/OR GENERAL VIOLATIONS EMPLOYER: Exide Technologies; Los Angeles Battery Recycling ADDRESS: 2700 South Indiana Street Vernon, CA 90020 ‘The law requires that violations observed during the inspection/Investigation completed on 08/29/2008 of the place of employment located at 2700 South Indiana Street, Vernon, CA be corrected within the ime Limit specified. Please notify the Divison as soon as these conditions have been corrected by returning this completed farm. Your response by signing and mailing this form to the issuing office on or before the compliance date may avoid a follow-up inspection of your facilites PLEASE COMPLETE AND MAIL BY 9/29/08 LIST THE SPECIFIC MEASURES TAKEN TO CORRECT EACH OF THE UNSAFE CONDITIONS This certifies that all unsafe conditions listed in the Division's citation dated 8/29108 have now been corrected, Signature Date: ame: Tite: NOTE: This form does not serve asa request for atime extension. If here ace serious problems beyond your contol dat prevent meeting a specified abatement date, conact the Division early, well within the 15-day limit allowed for an appeal OFFICE USE ONLY Safoty Engineor/industrial Hygienist: Date. Distriet Manager: Date [] Close / Comments Sha Roh Feel Yer O58PROPOSED _Dewonisieer - sina we. 30 om Ace Barz pertain, revere Blogeise/ woes 27 S. Kia AS?) (oC uod Oe 68 ro a a =n ae ae | Terie i - el le fly meee | EE . 3 ve i a | A) le 2 | §|"mauroven'| yy | 83 | % 3 we 56 e Be | ey f)e ame HEE Te |Eyil 2 a a sengan | ie | BE PRG p]e mre aba 885 [8 fee) og LS ot ren | gad ¢ | Gb fs | Ree __ | Pt fie $557 OQ) B |G | ~ eee -250 Be S00 ~ BS, |37S \ve7 Vé3 a lo 62s 1 |G |- welt 50 — ‘las [375 87 85 Zs 3 Be) | 1 |G Ineelem| © Ko ~~ 7166 Sé2/287 260 [|__| I | _| _ r T y | al | Le __L | |_— | | T — |_| {—— \ | |__ ANd an | | — _| |_{ _ ee 7G? 188 “JOTAL PROPOSED PENALTYS i ey TOTALS mann onirronmnsa cers | ewe a pewsvroasmenracrons | & Genera PERCENT (wireRcem fe recut San | see ston frora SN Tae [reson [rors Se Reet em BPREREE aS =REPE Ee) pcomnemewmer ae ies [ix bs fot te F DroneOF CALIFORNIA ~ Recaro MONROVIA Distr OMe - ALOHA DERARTuENT OF INDUSTRIAL RELATIONS Royal Oaks Drive Ste #104 DIVISION OF OCCUPATIONAL SAFETY AND fy 7H arora, Ca 1016 rar 6 2562913 EMPLOYER'S SIGNED STATEMENT OF ABATEMENT OF REGULATORY AND/OR GENERAL VIOLATIONS Exide Technologies; Los Angeles Battery Recycling 2700 South Indiana Street - Vernon, CA 90020 ‘The law requires that violations observed during the inspection/investigation completed on 08/29/2008 of the place of employment located at 2700 South Indiana Street, Vernon, CA be corrected within the time limit specified. Please notify the Division as soon as these conditions Ihave been corrected by returning this completed form. Your response by signing and mailing this form to the issuing office on or before the compliance date may avoid a follow-up inspection of your facil se ABATED LIST THE SPECIFIC MEASURES TAKEN TO CORRECT EACH OF qe u PLEASE COMPLETE AND MAIL BY 9229/08 for CONDITIONS * Crration i Lteey 1 a act ote fF sis wos Veplasect doa ped sigan . (Condition auated toy witoi03) titatiow Lt. The Miccing Krectet of tye 120 volt yunetion 5 vere ( Cond + ns alonted 2 it Cation {Lees 3 wot na soacd 4 “This certifies that al unsafe condions listed in the Division's cation dated 8/99/08 have ow Been corrected Signe: 7. Date 2/3 Name: _heanetin Coocland Tie B lant Manaoee ‘This form dues mot serve as 9 reques for a time extenion. F there are cerns problems beyord your control that prevent meeting a specified abatement date, contact the Division early, well within the 15-day limit allowed for an appeal y (bene oe ghar Safety Engineer/industrial Hygienist oatel>/ vat) e District Manager: 1} Close / CommentsEXIDE TECHNOLOGIES September 26, 2008 Department of Industrial Relations Division of Occupational Safety and Health CalVOSHA 750 Royal Oaks Drive, Room 104 Monrovia, CA 91016 ‘Attn: Mark Pisani Re: __ Inspection Number 310491881 Inspection Dates 6/18/08 and 7/22/08 Certified Letter/Return Receipt Number: 7006 2150 0003 1247 9823 Dear Mr. Pisani: Exide Technologies hereby provides your office with a copy of the Employer's Signed Statement of the following Abatement of Regulatory and/or General Violations. 1. Citation 1 Hem Type of Violation: General California Code of Regulations: Title 8 Subchapter 7. General Industry Safety Orders Group 16. Control of Hazardous Substances Article 108. Confined Spaces ‘Section 5157 (c) (2) 2 Citation 1 Hem 2Type of Violation: General California Code of Regulations: Tile 8 Subchapter 5. Electrical Safety Orders Section 2340.12 (a) Mechanical Execution of Work 3. Citation I Item 3Type of Violstion: Generat Sent to the Appeals Board on 09-26-08 for review Should you have any questiors, please feel free to contact me at 323-262-1101 Ext 2175 Sincerely, 2 Kenneth Copelafid Exide Technologies Plant Manager Vernon, California Ce: F. Ganster/ Exide Technologies J. Bolea/Exide TechnologiesState of California me Division of Occupational Safety ath ealth 4 Inspection Report ‘Tha Aug 28, 2008 11:57am Rpr ID [Assignment Nr. [CSHO 1D [Supervisor 1D [Inspection Nr. [Ope li 0950642 0 D1s49 [oss 8-08 [Establishment Name Site 2700 South Indiana Street Site ](323) 262-1101 |site Address | Vernon, CA 90020 Phone FAX Mailing |2700 South Indiana Street Mail Mail Address [Vernon, CA 90020 Phone FAX Controlling [Employer 1D Comp ‘Ownership [A. Private Sector Ciy_ [4030 (County [037 [Legal Entity A. Corpor’ Previous Activity (Swe Oniy)_[I- Inspection 126071026 Related Activity Type Number Satisfied Type Number Satisfied [C. Complaint 206632150 Health | [Employed in Establishment ‘BD Advance Nowe? No [Category [H. Health (Covered: By Taspection 14] Union? No [Primary SIC 3691 [Controlled By Employer 600] Walkaround? Yes |Secondary SIC interviewed? Yes [Inspected inspection Type |B. Complaint [Reason No Inspection Scope of Taspection|B. Partial Inspection ‘Classification, Strategic Tnitiatives [National Emphasis [Local Emphasis [Anticipatory Warrant Served? No [Denial Date [Date Refintered [Date ReDenied __[ReEntered [Anticipatory Subpoena Served? No Eniry 0618708 First Closing Conference ‘Opening Conference 6/18/08 Second Closing Conference Walkaround (06/18/08 Exit 6718708 Days On Site 2 [Case Closed No Citations Issued Type] 1D Optional Information| Ss 14 (SCF N 16__|LEAD 4. oO (CSHO Signatur D: signature fata Ce : ate 4 hss, OSHA-1(Rev. 6/93)STATE OF CALIFORNIADIVISION OF (| "JPATIONAL SAFETY AND HEALTH aon Distt Name Title AAT PONDER 2 SBEET) DADRA (4. CSEnH 12 BL NO. fad Ta. insp. No, X {6 Employer ZOTAR 7. Management Offials Coniacied: (* Denotes Phone Contact Oni) Brosent Dung Opening Inspect Closing ai iscuss Violations Obs. | B.gAr0rd Keeping Beces vostro, | PSE Glasing Date Anticipates | Beesrscton Recor eeredie toes aining Recor / Union Reprateniaiives Corfacled Present Dariig Name Tite Labor Union / Phone Opening Inspect’ Closing fa Dae ta be Sabsetuent Vis i ee 10. Smal Emaloyer Relief EeMOSGocumentstion —ineure™ 11 Openina Conference ~) 18 TP Program Review 79 Evalualion ol Seb) 8 Heath Proaram now 0 IPE Efecive Average Poor Explain Purpose Zornes soley Reepnsoiny °F a ES [BCallOSHA Program Brees Employee Participation EY 6 [BP Employee Rights Eretously Reviewed Training g 5 Fo S| Paget ag | selena | g eDparse escent Pcan OA eee ametionnforcement austen Faster In SPermitveriance Eeoresicaton “Goatram Se, an spectans ° - PeGancent to inspect [investigation Procedures AS average 30128 SFair [72 Ext Conference "| Ex Correction Provecures ( a Poor (3202660 OPoot ' Training 5 981-100 *Does not apply to penalties for accident related serious, wilful, repeat, ora Serious violation with lack of an crevatve Injury & tings Prevention Program. ise | 16, Hazard Gommynication Program BypSesneconlerence (Piritten Progrem Emipioyer sing oF ZEmoioyees Feobein eyeaton Bepee Ziaions ISDS Available SaateiConsut | enalties 2 Sie aaa aVOSHA Poster Posted Posting [evoralContrence | gece of cate ates pees Bist as xt low-up rained Fest Alder LO Variance ee | Posinesicn (prostes — February Se ‘Respiratory Program CoctouBiockout REASON [Fatety Process Mem GConfined Space — ating Conservation Blooabarne Pathogens | 24. CommentsiNotes She Hupeue> CUS. Cebpend LECEES b See ile ped S7Hb4 HEL T BA) (EAD FED ECM 78, Cross jurisdictional Revert EXProof of Workers’ Comp. Ipsurance fadustrial Welfare Commission Poste: Posted ee CaWOSHA 14 (12101100)STATE OF CALIFORNIA DIVISION OF © -“UPATIONAL SAFETY AND HEALTH Page 2 of 2 (722. Employees/Persons Inlerviowed During Inssection. Enler name, home address and phone Aumbar Below. fs tf ‘Name/Title: Name/Titl: roe eS a Phone Phone 2 a ianemtite Samet (ee: ec) ‘adtose aaece Phone Pho 3B. Mali Employes Werkale? Yee CIN PRT yes, cba pTolowirig wore oh each employer nverved a. Employer: Oe BAZ7CPY Sg, Emptoyer Address: Adctess: Activities: Activities: —- i Contract Governing Employer's Work atthe Site L Contract Goverring Employer's Work atthe Site Dawareness of Violation Ci Awareness of Violation 1D Violation Foresecable to Employer D Violation Foreseeable to Employer steps Taken by Employer to Protect Employees: steps Taken by Employer to Protect Employees it yes, what specific steps? ‘Byes, wnat speciic steps? Employer Category (Check al that apply) Employer Category (Check all that apply) 3 Conteling 2 Conectng 2 Exposing L] Creating L) Contrling L) Cerrecting CI Exposing (1 Cre 2. Employer: 4. Employer: Address: Adress! Activities: 7 - Activities: Ccontract Governing Employer's Work at the Site 2 Contract Governing Employer's Work at the Site D Awareness of Violation Awareness of Violation Di Violation Foreseeabie to Employer Di Violation Foresceable to Employer T steps Taken by Employer to Protect Empioyoos {Cl steps Teken ay Employer to Protect Employees Ityes, what specific steps? yes, what specific steps? Employer Gatagony (Check al that apply) Employer Category (Check all that apply) Exposing [] Creating [] Controting L] Correcting C Exposing (3 Creating C) Contating L Coreating [I [BE Opening and Cosing Conference Sunitnary and AdeHional Comments L Compronenave (AFertal PRIS COP > WHE? Of UIMAeT WMEMOE? / Candr7te) Opening BK} atl WIS wn OO? ELWUTW Cayseur7 To WPI CUT OF? DEID HNCMNOS OBseUED WD 2955 8CE : ARR TENIEND S2bDeEES Chosuce ee a falig Je pen 0f AnvT WAGE se cover cerrmzo craw | a BL" GHB 25. Previous Cation History E7Ves LIN ifyes, ech cfalion hslony 8. Pupicalons Provided “Wee & eine ee 2 Gopsunttern 8 ‘ ‘i 5 27. Wadaiional sheets are attached, Check this box: CT CalOSHA 1 (1201/00)STATE OF CALIFORNIA DEPARTMENT OF INDUSTRIAL RELATIONS DIVISION OF OCCUPATIONAL SAFETY AND HEALTH CALIOSHA 750 ROYAL OAKS DRIVE, ROOM 104 MONROVIA, CA 91016 (626) 256-7913 . FAX (626) 359-4291 CITATION AND NOTIFICATION OF PROPOSED PENALTY September 8, 2008 Vianey Mendez Exide Technologies Los Angeles Battery Recycling Division 2700 South Indiana Street Vernon, CA 90023 INSPECTION NUMBER: 310491881 CERTIFIED LETTER/RETURN RECEIPT NUMBER: 7004 2510 0006 5012 9442 Dear Ms. Mendez: Division of Occupational Safety and Health (DOSH or “the Division”) did conduct an inspection of the work site located at 2700 South Indiana Street, Vernon on 6/18/08 and again on 7/22/08. ‘The proposed findings of the inspection are enclosed in this package. To serve as a re-cap, when I met with you I provided you with a booklet entitled User's Guide to Cal/OSHA. The booklet discusses how employers in the State of California are required to make use of known controls to reduce or eliminate recognizable hazards in the occupational setting. The booklet also explains that employees have a right to file a complaint and discuss concerns with Cal/OSHA, and that there are protections under the Labor Code against any sort of discrimination against a worker who speaks with Cal/OSHA. The booklet enlarges on the issues we discussed, including that there are actually two “Cal/OSHAs.” One, the Enforcement Unit, conducts inspections in workplaces based usually on accidents or complaints, and may issuePage 2 citations carrying monetary penalties if violations of Title 8, California Code of Regulations (CCR) are observed. The Consultation Unit, on the other hand, will give employers an inspection on their request without the issuance of citations, penalties or fees, and a visit from Consultation will not prompt an inspection from the Enforcement Unit. The Cal/OSHA Consultation Service does not share information discussed with employers with the Cal/OSHA Enforcement Unit. It has been determined that the following proposed citations be issued as outlined below: GENERAL VIOLATIONS: 8CCR 5157 (012) Permit Required Confined Spaces: Not adequately marked/warning signs. 8 CCR 2340.12 (@) Opening in 120 volt live electrical junction box. BCR 5198 (AX) ‘Lead-containing dustin smelter control room (designated as a clean zone). Also enclosed is 2 U.S. Department of Labor print-out listing the most-frequently cited OSHA standards at the federal level for companies having the same SIC (Standard Industrial Classification) code as Exide Technologies Battery Recycling. The print-out is for your information only, to assist you in future hazard recognition inspections in your workplace. At the time of the inspection | also provided a flyer that discussed how the Title 8 Safety Orders can be obtained without charge, on-line at: hitp:/\www.dir.ca.gov/samples/search/query.htm again invite your attention to this informative webpage, and suggest you consider contacting the State of California’s free, confidential Cal/OSHA Consultation Service, so that you might expand on issues pertaining to occupational safety and health that we discussed. Citations initially carry what are called “proposed” penalties. Penalties and penalty amounts do not become permanent until after employers are offered an orfunity to come into the Monrovia office and meet with the Dist ager in what is called an “informal conference.” At that time you may bring up any disagreements you may have with a Cal/OSHA finding. It is strongly recommended that you contact the Monrovia District Office and set up an appointment with the District Manager for an informal conference as soon as possible if you have any disagreements with these findings. Currently, the total proposed penalty for the violations listed above is currently set at $650.Page 3 If an informal conference does not prove to be satisfactory, you may request a formal appeal, You have 10 working days from date of receipt of citations to file for an informal conference and 15 working days from date of receipt of citations to file for a formal appeal. The directions for filing a formal appeal are contained in this package. An informal conference may be requested anytime after an appeal is filed up to the hearing date. California Code of Regulations, Title 8 requires that copies of the enclosed citations be posted in a conspicuous place in the work area for three working days or until the conditions are abated, which ever is longer. Also enclosed is a form entitled "Statement of Abatement of General Violations." This form needs to be filled out and returned to the Monrovia District office of DOSH with statements indicating what steps your establishment has taken to abate the cited violations. If Exide Technologies elects to appeal a Cal/OSHA finding, the forms are not due until after a final determination in the appeal has been issued by the appropriate jurisdiction. Unless the matter is filed for an appeal, if the abatement forms are not received by the Division by the date indicated on the forms, a follow-up inspection may result. PAUL M. GRIER, M.S. Associate Industrial Hygienist/Safety Engineer Division of Occupational Safety and Health Enforcement Unit Enels.STATE OF CALIFORNIA DEPARTMENT OF INDUSTRIAL RELATIONS DIVISION OF OCCUPATIONAL SAFETY AND HEALTH CalOSHA 750 ROYAL OAKS DRIVE, ROOM 104 MONROVIA, CALIFORNIA 91016 TEL: (626) 256-7913 FAX: (626) 359-4291 June 19, 2008 Vianey Mendez Health and Safety Manager Exide Battery Recycling 2700 South Indiana Street Vernon, CA 90023 REGARDING: INSPECTION OF 6/18/08 OSHA NUMBER: 310491881 Dear Ms. Mendez: Per our conversation, Division of Occupational Safety and Health would like to request copies of the following documentation: -Copy of OSHA Log 300 Recordable Incidents pages for this year and previous three years. -Copy of the site facility map or a floor plan layout similar to the one I looked at prior to the inspection yesterday. -Copy of your company written Lead Compliance Program as required in 8 CCR 5198 (¢)(2). -Copy of current certification for the{§ ton overhead gantry crane we looked at in the smelting building, IENISTISAFETY ENGINEER DIVISION OF OCCUPATIONAL SAFETY AND HEALTHFORM C1Bs AND CITATIONSState of California Division of Occupational Safety and Health Worksheet ‘Thu Aug 28, 2008 12:25pm Tnapection Number] 310491881 Opt. Insp. Number 068-08 Establishment Name [Exide Technologies; Los Angeles Battery Recycling [Type of Violation G General [Citation Namber | 01 |ltem/Group oor [Number Exposed 14 No. Tistances 3_ [REC C Complaint Sid, Alleged Vio HIS7( 02) ‘Abatement] ___MultiStep Abatements__| Final Abatement 7 Action Type/Dates Period [PPE Period] Plan [Report £ 3 Corrected During Inspection [Abatement Documentation Required [Date Verified | 08728708 Siistance Codes AVD/Variable Information: CALIFORNIA CODE OF REGULATIONS; TITLE 8 Subchapter 7, General Industry Safety Orders Group 16. "Control of Hazardous Substances Article 108. Confined Spaces Section 5157 (c)(2) Permit-Required Confined Spaces. General requirements. If the workplace contains permit spaces, the employer shall inform exposed employees and other employees performing work in the area, by posting danger signs or by any other equally effective means, of the existence, location of and the danger posed by the permit spaces. Note: A sign reading "DANGER -- PERMIT-REQUIRED CONFINED SPACE, DO NOT ENTER" or using other lar language would satisfy the requirement for a sign. VIOLATION: ‘At the time of the inspection, it was observed that Mud Tanks #1, 2 and 3 on the west side of the facility located at 2700 South Indiana Street, Vernon contained Permit-Required Confined Spaces in which the warning signs posted on same as, ‘manadated by 8 CCR 5157 (c) were either missing or partially torn off. Penalty Calculations z "Adjustment Factors ed Adjusted Severity | Probability | Gravity [GBP Sizé [Good Faith] History | Penalty 0.00[ 0 0 0 185.00 (OSHA. 1B/1BIHprin(Rev, 993)Page 2 Exide Technologies; Los Angeles Ba,,..y Recycling Inspection Nr. 3 ‘Tau Aug 28, 2008 12:25pm 1881 Citation Nr. O1 Item/Group 001 (Occupation [Smelting Control [Employer [Exide Technologies Nr of Employees [39 Duration [5 days/week [Frequency [8 hrs/day Employee Name [Marshall Pitts INF of Employees [39 [Duration |5 days/week _ [Frequency [8 hrs/day Employee Name Tgnacio Silva Address Phone = (Occupation Smelting Operator [Eniployer [Exide Technolo, INr of Employees |39 [Duration _|5 days/week i hrs/day Address Employee Name ‘Alvin Richardson | Tnstance Description: A, Hazard Bi, Equipment C. Location "By Injurylliiness —E, Measurements Event [Even Cove Retion Code canon pe Penal [Abate] Fial Date L Date [order [oso [AAda 1G General 785.00] 09712708, (OSHA-1B/1BIHprin(Rev. 9/93)Documentation Worksheet fEsisb. Name] __EXIDE BATTERY Issue Date Resion-¢ ~ overt (RRGSSSSSA 2 FTA [3 cSHOW [4 Optional Repot |S DateTime Fi oss | 08 | eitei0a Fem IGEREC” [onto | 11 na 2seveny 13. beet | Utes Anes leat 14 Low Low | Low 15 Total Adi Factors in 7 Abstant Panes) |f@Acion Die | Tifis Savencetcor Ta? [Comments |Group 16. Control of Hazardous Substances \Article 108. Confined Spaces \Section 5157 (c)(2) Permit-Required Confined Spaces. |General requirements. es and other employees. If the workplace contains permit spaces, the employer shall inform exposed empl ‘means, of the existence, lperforming work in the area, by posting danger signs or by any other equally effecti llocation of and the danger posed by the permit spaces. INote: A sign reading “DANGER ~- PERMIT-REQUIRED CONFINED SPACE, DO NOT ENTER” or using other similar| language would satisfy the requirement for a sign. VIOLATION: [At the time of the inspection, it was observed that Mud Tanks #1, 2 and 3 on the west side of the facility located lat 2700 South Indiana Street, Vernon contained Permit-Required Confined Spaces in which the warning signs lposted on same as manadated by 8 CCR 5157 (c) were either missing or partially tom off. (22. Elemental Analysis - List numerically each descapive element ofthe cted Tle-8 CCR secion in he Elements column. Inthe Evidence ‘Summary column, specty each tem of evidence found during the Inspection which substantistes the descriptive elemert (e.g, hazards, (Operation, equment, location andlor measurements). Under Typels) of Evidence, speciy the classiicaton ofthe evidence described under Evidence Summary (see Legend at bation of page) (caVOSHA 18 (07/01/95)Elements [Evidence Summary CALIFORNIA CODE OF REGULATIONS; TITLE 8 ‘Subchapter 7. General Industry Safety Orders (Group 16. Control of Hazardous Substances lArticie 108, Confined Spaces ‘Section 5157 (c)(2) Permit-Required Confined [Spaces. |General requirements. It the workplace contains permit spaces, the employer |Mud Tanks #1, 2 and 3 loB, PH [shall inform exposed employees and other employees lperforming work in the area, by posting danger signs lor by any other equally effective means, of the lexistence, location of and the danger posed by the [on the east side of the facility \0B, PH permit spaces. Note: A sign reading "DANGER ~ PERMIT- REQUIRED CONFINED SPACE, DO NOT ENTER’ or|located at 2700 South Indiana Street, Vernon lB, PH lusing other similar language would satisfy the lrequirement for a sign |contained Permit-Required Confined Spaces in 0B, Pt |which the warning signs posted on same as Imanadated by 8 CCR 5157 (c) |were either missing lop, PH lor partially tom off joB, PH * Observation (OF). Employer Admission (EA), Employer Oral Satemen (EOS), Evidence Wiiten Satement (EWS), Oher Wien Statement (OWS) ‘Photograph (PH), Business Recors (BR), Document (00), Sample Measurement (SM), Monitoring Measurement (MM), [EquipmentParsitachinery(EPM), Other please speciy! cavosta 1B (07101185)Documentation Worksheet — continued [5 Pht y [oman a taste ono of pty ee Fe FSS ee Ea TOS ETT TSTSETE eeraanay ad | ae | 53 ae Ex Ga * Provide evidence only when temporary employees at mulliemployer worksites are involved, 25. Additional Witness Documentations the name, address and phone numberof each person having percipient information lof the factual elements in Section 22, Afler each name litte element number for Section 22 which the person is able to personally very, 126. Citation Classification '_ Assuming that an accident or exposure occurs, what are the ely consequences? ‘Atmospheres of confined spaces are required to be tested prior to entry. Exposure to harmful atmospheres may be likely in the event that confined spaces are not labeled with required warning signs 'b.___L) Actual Management Knowledge or Bd Constructive Management Knowledge? (Check all that apply: [Bl Violation Common Practice At Jobsite TT Accident At Jobate Previously From Same Vilaton(s) |B Proximity OF Supenisors to Violation 1D Special Duty To Inspect - Competent Person At Excavation ==] 1B] Violation Readily Visible To Anyone Passing By 'T Empoyer Reosived Complaints From Other EE's a Violative Condition |B Obigation Anicipatec: Foreseeable Hazards (8, Asbestos Containing consiructon Materials in Older Buldings [Bl Condon Existed Long Enoush Fer Employer Awareness Other (please state) ~. Documentation as to Why Violation is Serious, General or Regulatory. ITo classify a violation as "Serious" pursuant to Labor Code Section 6432 (a), Division of Occupational Safety and Health Imust establish by a preponderance of the evidence, that should an accident occur as a result of the violation, that there is ja substantial probability that death or serious injury could result from a condition which exists from one or more of the Iractices used in the place of employment, unless the employer did not, and could not with the exercise of reasonable Idligence, know of the presence of the violation. This violation was classified as "General" as probability of death or [serious injury arising directly from the aforementioned violative condition was not regarded as "substantial" ‘Use the documentation continuation sheet to document evidence of any of the following f 4. Prior Violations (Repeat) €. Intentional, Knowing, or Reckless Conduct (Wilf - Wiltl Elements Worksheet must be attached, F Falureto Abate tems) Cont'd ‘Severity = Extent Likelihood CCaVlOSHA 1B (07/01/95)State of California Division of Occupational Safety and Health Worksheet ‘Thu Aug 28, 2008 12:25pm Taspection Number 310491881 ‘Opt. Insp. Number| 068-08 [Esblishment Name [Exide Technologies; Los Angeles Battery Recycling Type of Violation’ G General [Citation Namber | Or [em/Group 002 [Number Exposed 14 INo, Instances; T__[REC [Complaint Std; Alleged Vio. 2340.0012( a) } ‘Abatement]_— MulliSiep Abatements Final Abatement “Action Type/Dates, Period [PPE Period] Plan [Report 3 Corrected During I Inspection [Abatement Documentation Required Date Veritied [08/28/08 ([Sibstance Cotes [AVDiVariable Information: CALIFORNIA CODE OF REGULATIONS; TITLE 8 SUBCHAPTER 5. ELECTRICAL SAFETY ORDERS Section 2340.12 (a) Mechanical Execution of Work. Unused openings in boxes, raceways, auxiliary gatters, cabinets, equipment cases, or housings shall be effectively of 2 4. Check one: Ose Bin 2. Region bistrict_2 depts Suomived (626 4.Name Maud a1. Chek 5. Phone No. 835-429 FAX No 97°29/ 6. Address 752 Bord apne 3 Obtes FE IO Vuorpou nA A_tiwb ‘Sireat om oy 7. Inspection entiation: De ot No, 7 8, Sample Information: 9. C1] Urgent Lab Service Request istrict Manager Approval Taitiate ry Type of Sane Iran (eran op (ceotaw) | Volume Feld Information Requested c Most # 13,3 | Seow 3 132 —~ Tater = Bag= 8 Rovorbing Tube © AT Grab Sample = @ tmplngar= 1 Bobller © Bu Fir Paper =F Oar = Wie 40. Comments: VES TET Loe (EAD Released By Received By: Time: Date: «& ow taaape 3 loalek ~~ 42, Date Received by Lab: ¥/ 24 o 19 Cal/OSHA 1H (08/01/94)leas ies QD. Bevis Peeoeaay se) ETc Cina) Fae 1+ 205 + 15430 = 7 pw Fire. @ BrlO+ t+! 645 437795/ = RY mol Vilma QD +54 = ke mun cere © Sr 24 ye = 10S mw | eq. LERACIO SLCUA S me Citas |Eecze® tHE ZH /O4 22484 B04 17TH = INT wes koe QZ i-p /d0+ C+ sy tbs r Ft = [67 mw FecruB boty = CE wandLicepposon CAB Plene Vaames —— Adins LUtHPAOSON Aa 1452 pare Q (Fea) Ss eS Bogs rl. 928 F 2035 a Ags tt TEE TE = 2.023 Lpn es Zope + L829 ev7 = z Poe x 7 end el@& @ — asfog rekon Ceo Crews Recesseoseu_) Chew.) 1S US Zio35 + 2,035+ 1998 9.923 1pm 3 2,625 < etd- @ @ 1l23(06 UbcemteS GCeastewes) Sth = SiLUA CAE One Ipsec Seva S-fB = sim Kao Biouc fev || & Cones) Pup _@e ove 5 Sty | Ww us ay UF Ss —— Zest 2.035 TIE FPF TTS = Z.0lf ww per SOL 293.6 4. = ha eeO_ ALuis 216492059) BR srewes — Covau ) US NY NS Wy NS MZ Wo ug UF US 4 QD 2035 1.978 ZR. OFF 4.998 (99S 1999 LPH ROH (IE Ze OBS 2,035 HVE By = 24/6 uM KY = BE = 2.03 cpm renpeverlevt . © rears “Sie - re ae UZ a3 as Ie D209 cogs 1 be MS AGF IS 1 777 49831433 10827 By 83 ew —@®(Brera Sibu metas” Fees Sudcger of Qu Fr26 cy fund on S48 WS OW far ye ow 0 ie ea F493 Rine®) us _ 5 10F _ ~~ Wn3£ 102 Ay A Coie oté Da (¥5 7 | IACI (LLCREALO Ton SUATGE Opeten To | We eaus | H Slt ow Us SES Dw get bo OF \'S 61tt ow Uy List ak us VSS (cs —— 4:5! off No S53 iN 105% oi Ly (37 ond Wise ad as (Ue oft ny —_. @ FA Pree rey OU — Bis Cra ge eae Femme © Fecget @ oll ee ® LS heme @TY fob 1:46 aun e Li O5¥4 28 Bos WET AL Nost Conde CAP Ol 607 | Copoesr Ciera gsr Cieedibeeicn! | 2© Petirur_erek MG! 2,65) £ lL mes | vnc) Aesobebe oe Sms ALLELE af FTRLS || Apes aaa 67 es 2057 & COA OBS bp BOTY | Cok Ou HEE Mes 2PS9 & CoA 81852 (6, Bode Oa YF (6 i 2.055 Rethurxe2 RL 20 Frenewirsd 121; C5 arenes)Certificate State of Cafornia DOSH, Cateo Lab « 41555 Doce Ove aryl, A San Leandro CA 84577 ees Suir ubcon font PO Wo. Jona Corperation test number PROS-2 Rev 6 or PROI-10 Rev D using high-purity bolted nitrogen, ____caipate_bue bate a aE == sorza2007 101222008 _ — = Lab. Pressure 753. mmHg Lab Standaré Allowable Condition Unie No. Deviation Deviation Shipped . sosar 081% 0% Intolerance. 102877, 0.08% 00% Intolerance. onal Corporation st number PROS-2 Rev 8 or PRO-10 Rev D using high-purly bates nitrogen calDate ove Date 7 a a 5112008 2 : Lab, Pressure 755 mmHg Lab standard Allowable Conuition “i1a7es___0.08% 1.00% in erence, 13761 38% 1.00%. intolerance 113761 041% 1.28% In tolerance ‘by comparing it toa laboratory standarc primary piston rover of much higher accuracy ‘ples. Flow-generotors of 20.03% stably ae.ueed for the-comparison-Use of provers of ‘ures the validity of the flow generator asa transfer standard. The primary laboratory A iheicfiomonsinns itiamatee loath of mast nah tne hnee) anainst NIST traceableELEMENTS by ICP 7300 (Nitric/Perchloric Acid Ashing) MW: Table 1 CAS: Table 2 RTECS: Table 2 METHOD: 7300, Issue 3 EVALUATION: PARTIAL. enue 1: 15 August 1900 tesue 3: 18 March 2003 OSHA: Tabie2 PROPERTIES: Table 1 NIOSH: Table 2 ACGIM: Table > ELEMENTS: aluminum’ eaigum lanthanum ike stontum tungsten antimony" Chromium’ ni potassium felluium —— vanadum* arsonie cobalt magnesism phosphorus tn viru batium cope manganese’ Selenium thalium ne er molvederum’ —siver ‘Wan ——2rtonium* feaet "Some compounds ofthese eloments require special sample treatment ‘SAMPLING. MEASUREMENT SAMPLER: FILTER TECHNIQUE: INDUCTIVELY COUPLED ARGON [0.8-um, colulose eter membrane, or PLASMA, ATOMIC EMISSION 5 sim, plynytehirige membrane} SPECTROSCOPY (CP-AES) FLOWRATE: tio 4 Limin ANALYTE: elements sbove vou-mn Tables ASKING “MAK Tobie + REAGENTS: cone. HNO,/ cone. HCI, (1), ml 2m ineremenisadde0 6 needs SHIPMENT: routine CONDITIONS: room temperate, 30 min; 180 Co nest SAMPLE ryness STABILITY: stable FINAL SOLUTION: A% HNO, 1% HCIO,, 25 mL BLANKS: 20 10 lot bianks pers WAVELENGTH: depends upon element: Table 3 ACCURACY BACKGROUND CORRECTION: spectral wavelength shit fone: erusee! oy CALIBRATION: — elements in 4% HNO,, 19 HCIO, ee a RANGE: varies wih element [1 OVERALL PRECISION (&,): not deerminas ESTIMATED Lo; Tables $ and 4 pen ot determined PRECISION (8): Tables $ ana 4 [APPLICABILITY: The working range of hs metha i 0.005 2.0 mas? for each slementn a 50D alr sample. This is Sirukanmous elements anatysis.n9t compound speci. Very int the ypes of compounds Int samples are selble with the ashing groceduie selected INTERFERENCES: Spectra intrerences ae the pay inerferences engountered In ICP-AES analyls. These ae ‘mininized by uaicous wavelengin seecton,intrelomem corecten factor end background comection [1-8 OTHER METHODS: his sve update sees 1 and 2 of Mebiod 7300, which eplaced PACAM 351 [3] for Wace elements. Flame atomic absorpign spectioscapy (eg. Mathes 70XX)'s an aera ancl lectnique for many of hese ements GGaghite timace RAS (o.g, 7102 for Be, 7105 for Pb s more sensive, NIOSH Manual of Anaitical Methods (NMAM), Fouth EditionELEMENTS (ICP). METHOD 7300, issue 3, dated 15 March 2003 - Page 2 of 8 REAGENTS: EQUIPMENT: 4. Nitric acié (HNO), cone., ultra pure 1, Sampler: cellulose ester membrane filter, 2. Perchloric acid (HCIO,), cone,, ultra pure.” 0.8-pm pore size; oF polyvinyl chloride 3, Ashing acid’ 4:1 (viv) HNO;HCIO,. Mix 4 membrane, 5.0-um pave size; 37-mm volumes cone. HNO; with 1 volume cone slameter, in cassette fiter holder. HCIO, 2, Personal sampling pump, + to 4 Limin, with 4, Calibration stock solutions, 1000 ygimt flexible connecting tubing Commercially available, or prepares per 3, Inductively coupled plasma-atomic emission instrument manufacturers recommengation spectrometer, equipped as specified by the (see step 12) manufacturer for analysis of elements of 5. Dilution acid, 4% HNO,, 1% HOIO,. Add 50 imerest. mL ashing acid to 600 ml water; diute to1L. 4. Regulator, two-stage, for argon, 6. Argon. 5. Beakers, Philips, 125-mL, or Griffin, S0-mL, 7. Distiled.deionizes water. with watchglass covers."* 6, Volumetric flasks, 10-, 25-,100-mL., and 1-L** 7. Assorted volumetric pipets as needed." + See SPECIAL PRECAUTIONS. 8 Hotplate, surface temperature 150 °C. ** Clean all glassware with cone. nitric acid and rinse thoroughly in distiled water before use. SPECIAL PRECAUTIONS: All perchloric acid digestions are required to be done in a perchloric acid hood. When working with concentvated acids, wear protective clothing and gloves. SAMPLING 1. Calibrate each personal sampling pump with a representative sampler inline 2. Sample at an accurately known flow rate between t and 4 L/min for a total sample size of 200 to 2000 L (see Table 1) for TWA measurements, Do not exceed afilter loading of approximately 2 mg total dust SAMPLE PREPARATIO 3, Open the cassette fiter holders and transfer the samples and blanks to clean beakers. 4. Add 5 mL ashing acid, Cover with a watenglass. Let stand 30 min at room temperature, NOTE: Start a reagent blank at this step. 5. Heat on hotplate (120 °C) unt ca, 0.5 mL remains, NOTE 1: Recovery of lead from some paint matrices may require other digestion techniques. See Method 7082 (Lead by Flame AAS) for an alternative notplate digestion procedure or Methos 7302 for a microwave digestion procedure NOTE 2: Some species of Al, Be, Co, Cr, Li, Ma, Mo, V, and Zr will notbe completely solubilized by this procedure. Alternative solubilization techniques for most of these elements can be found elsewhere [5-10]. For example, aqua regia may de needed for Mn (6,12) ‘Add 2 mL ashing acid and repeat step 8. Repeat this step until the solution is clear Remove watchglass and rinse into the beaker with cistiled water. Increase the temperature to 150 °C and take the sample to near dryness (ca. 0.5 mL}, Dissolve the residue in 2 10 3 mL dilution acis Transfer the solutions quantitatively to 25-ml, volumetric asks, Dilute to volume with dilution acid. NOTE: Hf more sensitivity is required, the final sample volume may be held to 10 mL [NIOSH Manual of Anaya! Methods (NAM), Fourth EditonELEMENTS (ICP): METHOD 7300. Issue 3. dated 18 March 2003 - Page 3 of 8 CALIBRATION AND QUALITY CONTROL: 12, Calibrate the spectrometer according 1o the manufacturers recommendations, NOTE: Typically, an acid blank and 1.0 g/mL multielement working standards are used. The following ‘muttielement combinations are chemicaly compatibe in 4% HNO,/1% HCIO, a, Al, As, Ba, Be, Ca, Cd, Co, Cr, Cu, Fe, La, In, Na b. Ag, K.Li, Mg, Mn, Ni, P, Pb, Se, Sr, TLV, ¥, Zn, Se © Mo, Sb, Sn, Te, Ti, W, Zr d, Acid blank 13, Analyze a standard for every ton samples. 14. Check recoveries with at least two spiked blank filters per ten samples. MEASUREMENT: 18, Set spectrometer to conditions specified by manufacturer. 16. Analyze standards and samples. NOTE: If the values for the samples are above the range of the standards, dilute the solutions with dilution acid, reanalyze and apply the appropriate dilution factor in the calculations. CALCULATIONS. 17. Obtain the solution concentrations for ne sample, C, (yg/mL), and the average media blank, Cy (ugimL}, from the instrument. 18, Using the soliton volumes of sample, V, (mL), and media blank, V, (mL), calculate the concentration, C (mgim?), of each element in the air volume sampled, V (L} ov, C8¥s~ Cos 6 C= me ti NOTE: gil + mgim? EVALUATION OF METHOD: Issues 1 and 2 ‘Method, 7300 was originally evaluated in 1981 {2,3}. The precision and recovery data were determined at 2.5 ‘and 1000 ug of each element per sample on spiked fiters. The measurements used for the metho evaluation in issues + and 2 were determined with a Jarrel-Ash Mode! 1160 Inductively Coupled Plasma Spectrometer operated according to manufacturer's instructions. Issue 3 Inthis update of NIOSH Method 7300, the precision and recovery data were determined at approximately 3x ‘and 10x the instrumental detection limits on commercially prepared spiked fillers [12] using 25,0 mL. as the final sample volume. Tables 3 and 4 list the precision and recovery dala, instrumental detection limits, and analytical wavelengths for mixed cellulase ester (MCE) and polyvinyl chloride (PVC) fillers. PVC Filters which can be used for total dust measurements and then digested for metals measurements were tested and ound to give good results. The values in Tables 3 and 4 were determines with @ Spectro Analytical Instruments Mode! End On Plasma (EOP)(axial) operated according to manufacturer's instuctions. MOSH Manual of Analyica! Metneds (NAM), Fourth ationELEMENTS (IGP). METHOD 7300, Issue 3, dated 15 March 2003 - Page 4 of @ REFERENCES: [1] Milison (#, Andrews R [2002]. Backup data report, Method 7300, unpublished report, NIOSH/DART. [2] Hull RO [1981], Multielement Anaiysis of Industral Hygiene Samplas, NIOSH Internal Report, presented at the American Industrial Hygiene Conference, Portland, Oregon, [3] NIOSH [1982}. NIOSH Manual of Analytical Methods, 2nd ed., V. 7, P&CAM 351 (Elements by ICP), U.S. Department of Health and Human Services, Publ. (NIOSH) 82-100. [4] NIOSH [1994). Elements by ICP: Method 7300, Issue 2. In: Eller PM, Cassinelli ME, eds., NIOSH Manual of Analytical Methods, 4® ed, Cincinnati, OH: U.S, Depariment of Health anc Human Services, ‘Centers for Disease Controland Prevention, National instilute for Occupational Safety an¢ Health, DHHS. (NIOSH) Publication No. 94-113, [5] NIOSH [1994]. Lead by FAAS: Method 7082. In Eller PM, Cassinelli ME, eds., NIOSH Manual of Analytical Methods, 4" ed. Cincinnati, OH: U.S. Department of Health and Human Services, Centers for Disease Control and Prevention, National Insitute for Occupational Safely an¢ Health, DHHS. (NIOSH) Publication No. 94-113, [6] NIOSH [1977], NIOSH Manual of Analytical Methods, 2nd ed., V. 2, $5 (Manganese), U.S, Department of Health, Education, and Welfare, Publ. (NIOSH) 77-157-6, I7| NIOSH [1994], Tungsten, solubleinsolubie: Method 7074. In: Eller PM, Cassinelli ME, eds., NIOSH Manual of Anaiytical Methods, 4" ed. Cincinnati, OH: U.S. Department of Health and Human Services, Centers for Disease Controland Prevention, Nalionat Institute for Occupational Safely and Health. DHHS (NIOSH) Publication No. 94-113, [8] NIOSH [1979]. NIOSH Manual of Analytical Methods, 2nd e¢., V. 5, P&CAM 173 (Metals by Atomic ‘Apsorption), U.S. Department of Health, Eeucation, and Welfare, Publ. (NIOSH) 79-141 [9] NIOSH [1977], NIOSH Manual of Analytical Methods, 2nd ed., V. 3, $183 (Tin), $185 (Zirconium), and '$376 (Molybdenum), U.S. Department of Health, Education, and Welfare, Publ. (NIOSH) 77-157-C. [10] 180 [2001]. Workplace air - Determination of metals and metalioids n airborne particulate matter by inductively coupled plasma atomic emission spectrometry - Part 2: Sample preparation. International Organization for Standardization. ISO 18202-2:2001(E), [11] ASTM [1985}, 1985 Annual Book of ASTM Standards, Vol. 11.01; Standard Specification for Reagent Water, ASTM, Philadelphia, PA, D1193-77 (1985). [12] Cerification inorganic Ventures for spikes. METHOD REVISED BY Mark Milgon and Ronnee Andrews, NIOSH/DART. Method originally written by Mark Millson, NIOSH/DART, and R. OeLon Hull, Ph.0., NIOSH/OSHEFS, James B. Perkins, David L, Wheeler, and Keith Nicholson, OaiaChem Laboriories, Sat Lake City, UT. MOSH Manual of Anayical Methods (NAM), Fourh ExtonELEMENTS (ICP): METHOD 7300. Issue 3. dated 18 March 2003 - Page $ of 8 TABLE 1. PROPERTIES AND SAMPLING VOLUMES. Properties Element Atomic AirVolume, L @ OSHA PEL {Symbol weight MP.*C. MIN, MAX Siver (Ag) 107.87 961 250 2000 Aluminum (Al) 26.98 660 5 100 ‘Arsenic (As) 74.92 817 5 2000, Barium (fa) 197.34 710 50 2000 Berium (Be) 8.01 1278 1250 2000 Calcium (Ca) 40.08 az 5 200 Caamium (Cd) 172.40 321 13 2000 Cobalt (Co) 58.93 1495 25 2000 Chromium (Cr) 52.00 1980 5 4000 Copper (Cu) 63.54 1083 5 1000 Iron (Fe) 55.85 1535 5 100 Potassium (k) 39.10 63.65, 5 1000 Lanthanum 138.91 920, 5 1000 Lithium (Li) 6.94 179 100 2000 Magnesium (Mg) zany 651 5 67 Manganese (Mn) 54.94 1244 5 200 ‘Molybéenum (Mo) 95.94 651 5 7 Nickel (Ni) 58.71 1453 5 1000 Phosphorus (P) 30.97 44 25 2000 Lead (Pb) 207.19 328 50 2000 Antimony (Sb) 121.75 630.5 50 2000 Selenium (Se) 78.96 217 13 2000 Tin (Sn) 118.68 2319 5 1000 Strontium (Sr) 87.62 769 10 1000 Tellurium (Te) 127.60 450 25 2000 Titanium (Fi) 47.90 1675 5 100 Thallium (71) 206.37 304 25 2000 vanadium (V) 50.94 1890 5 2000 Tungsten (W) 183.85 3410 5 1000 Yurium (Y) 88.91 1495 5 +4000 Zine (Za) 65.37 419 5 200 Zirconium (Ze) 91.22 1952 5 200 NIOSH Manual of Anaial Metnods (NAN), Four EatonELEMENTS (ICP): METHOD 7300, Issue 3, dated 15 March 2003 - Page 6 of & TABLE 2. EXPOSURE LIMITS, CAS #, RTECS Element Expceure Lis, mgm? (Ca = carcinogen) (Symoe) case Rrecs Osta NOSH ACG ‘iver (09) 7440-22-4 — VW3500000 0,01 (dus, fe, metal) 0.0% (metal semble) 0.1 (meta) 0.01 fsoube ‘Auimioum(Al) 7428-905 80990000 15 (tal cust) 10 (va ut) 0 (cus 5 respeade) S esprabie fume) 5 (poms, fare) 2 (sats, ays) 2 cea, aoe) ‘Arsene (AS) 7440-382 660525000 ares 0.002, Ga 001, ca ‘Barium (8a) 7aeo-30-3 — cass7000 0.5 05, os Eoryiom (80) 7440-41-7 —DS1750000 0.002, c 0.05 0.0008, ca 0.007, ‘Catone (Ca) 70-702 ares. vanes varies cadmiumico) —7aeo-a3-9—EU9800000 0.005 lowestfeasile, Ca 0.1 (lta), Ca (0.902 esp .Ca cobalt (Co) 7440-46-4 —GFB7S0000 0.1 0.05 (sus, fume) 6.02 (du, sme) ‘cromum (Cr 7440-47-38. Gbsong0DD 05 os os. Copper (00) 7440-508 GLSS25000 + (ust, mists) 4 oust 1 (dust, mist) (uma) 0.4 ume) 02 (ume) tron (Fe) 7430-88 NO4565800 10 (ust, ume) 5 (oust, tue) 5 (lume) Potassium (kK) 7440.00.7TS0460000 — _ - Lantana 7439910 . - Lithium 7430-90-2 : Magnesium (Mg) 7499.05-4 OM2100000 15 (ous!) as oxde 10 (fume) as onde 10 (ume) as oxide Sresorabie) Manganese Mn) 7439.98 008275000 cS asreta S (aus) TSTEL 3 (me) Moiybderum (Mo) 749898-7 QA4G80000 5 (sotble) 5 (souble) 5 (cobble) ¥8{(olalinsolusie)——_—10 incluso) 10 nso.) Wicket (Ni 7440020 RS950000 1 0015,ca sou Phosohowus(P) —-772346-0 —THaso0000 04 os oa Lead Po) 7499921 OF7525000 005. 005, 005 Amimeny(Se) «7440380 04025000 05 os. os. Selenium (Se) «7782492 vS7T00000 02 02 02 Tin (Sn) yagoats — xP732000 2 2 2 ‘Sonu ($1) raozs : - - “Teluiom (72) séo0-80-9 wv2628000 0.1 os oa ‘Tania (79 ras0-926 — xR1TO00 _ : ‘Traor (1 7440-20.0 XG3425000 0.1 (shin) (sduble) 0. akin) (tole). akin) \vanaaum (¥) 7440822 ywae0000 cons _ “Tungsten r40397 = 5 5 5 10 (STEL) to (sTeL) iia (8) vasosss — Z6298000 1 Na 1 Zinc (Zn) 74e0556 — z@8600000 — - zconur (20) raeoe7-? _ZHTo7O000_5 5,sTEL10 5,STEL 10 NIOSH Manus of Anaiial Methods (RAM), Fourth EatonELEMENTS (ICP): METHOD 7300, issue 3, dated 15 March 2003 - Page 7 of & TABLE 3. MEASUREMENT PROCEDURES AND DATA [1], cod Cellulose Ester Filters (0.45 ym) wavelenglh Est, LOD| LOD | Centiied % Recovery Percent | Certified _ % Percent Element nm uot |ngimt) 3xL0D (e) RSD | 10x LOD Recovery RSD 2) Filler o) we25) |) (c)__(N=25) Ag 280.042 | a7 | 077 t0r9 264 | 321 983183 Al ey ootts | as | tsa 10540115 | 640) Ors. As. 199 0.140 | 56 | 308 969 ©6228 | 129 938 130 Ba 455 0.008 |o2| 031 tore 172 | 129 977 © 0.69 Be 313 0.008 | 02| 031 100.0 1.44 129 9840.78 ca 317,908 | ana] 154 987 = B85 | 640 100.2 1.30 ca 226 © 0.0075 | 03 | 031 998 199 | 129 975 0.88 co 228.0012 | 08 | 031 00.8 ©=—.97 | 1.29 © 840.80 cr er 0.020 | 08 | ost 934 16.3 | 129 © 1012-279 cu 324 0.088 | 27 | 154 © 628 «= 1.47 || 640 10068 © 0.92 Fe 259 0.0ss | 38] 1.54 ©1033 8.46 «| 640 © 98.00.95 K 766 173 Joss] 230 08 181 | 964 876 0.80 La 40s 0.048 | 1.9] 077 028 «= 2.23: | 321 © 1001.92 ui e70 001d | 04 a1 1100191 4290 97.70.81 Mg -279—= 0.098 | 59] 154 1011 8.35 | 640 © 98.01.53 Mn 287 0.008 | 02 | 031 oro 1.77 || 1.28 877 Mo -202,-—=S 020 | 08 | 031 105.3 247 | 1.28 «= 8881.09 Ni 231 0.020 | 08] 031 1096 354 | 129 12 1.38 P 178 sz | 3.7 | 154 ase = 6.19 || 6408S TS. po 680.062 | 25] 154 1094 241 | 640 1017 0.88 sb 2068S o.ts2 | 7.7 | 308 902 114 | 1290 ats 2.58 se 19¢ 60.435 | 54] 23 76 6016 | 964 86s 4.78 sn 19 o.oo | 16] 077 902 a0 | a2 ae eis) sr 407 0.008 | 02] 031 to1.0 155. 1290-973 0.65 Te 21g 0.078 | 31 | 154 020 «= 267 | 640 | 971.28 vi 334 0.080 | 20 | 077 984 208 «| 3.21 934 1.08 1 190 0.092 | 37] 1.54 1009 «2.48 | 640 98.1 0.80 v 220.028 | 11 | 077 = to3.2 1.92 | 321 983 Bd w 207 0.075 | 30| 154 722 10.1 B40 57.6 14,72 y am o.ot2 Jos] 031 1005 180 | 129 974 0.75 Zn 213, 0.310 | 124] 4.80 102.2 1.87 123 9530.90 ze 339 0.022 | os | 031 sea 19.4 1.23 ea rer (a) Bold values are qualitative only because of low recovery, (©) Values are certiied by Inorganic Ventures INC. at 3x and 10x the approximate instrumental LOD. (c)_ Values reported were obtained with a Spectro Analytical nstruments EOP ICP; performance may vary with instrument and shouls be independently verified, NIOSH Manual of Analytical Metiods (VAM), Foust titionELEMENTS (ICP): METHOD 7300, issue 3, dated 15 March 2003 - Page Baf 8 TABLE 4. MEASUREMENT PROCEDURES AND DATA [1], Polyvinyl Chloride Filter (5.0 pm) wavelength Est.LOD] LOD | Geritied _ % —Percent|Certiies"” —% Percent, Element nm ug per |ngimL] SxLOD Recovery RSD | 10xLOD Recovery RSD (@ fier (OL (a) _ww=25)| (0) (a)__(=25) ag 328002 | 17 | 078 1082 8.20 318 618 189 al 17 ot5 | ae | 156 174 115.24 640 929 208 As reo o.tao | 56 | 310 1007 «8.13 | 1270 969 © 32 Be 485 0.008 | 02 | ast 1024 3.89 1270 998 © 20 Be = 313, 0.008 | a2 | 031 106.8 3.83 4270 102.8 21 ca 317-0908 | a6 | 158 sea 12.66 | 64.00 98853 ca 226 0.0075 | 03 | 0.31 1052 5.57 127 1019 28 co = 228.-~S 0.012 | os | 0.31 10.3 4.67 127 1028 28 cr 267 0.020 | 08 | 0.31 f094 5.31 127 103.441 cu 326 o.o6e | 27 | 156 1088 5.18 640 118 24 Fe 259 «0.098 | 38 | 1.56 887 46.82 640 981 97 K 7s = 1.73 | a3 | 234 964 470 | 95.00 992 © 22 ta 408. 0.048 | 19 | 078 455 4.19 318 988 26 ui sro g.010 | oa | 0.31 1077 4.80 127 1104 27 Mg 273, 3.098 | 39 | 1.56 548 20.58 640 645 57 mn 287, a.005 | 02 | ast wig 4.18 127 99324 Mo 202,» 0.020 | 08 | 031 1058 = 5.82 127 981 38 Ni 21 0.020 | o8 | ot 1105.89 127 1036 32 P 17a o.092 | 37 | 156 © 101.9 17.82 640 865 104 Pb 168 = 0.062 | 25 | 756 1088 «6.12 640 1032 29 Sb 208 = ote | 77 | 3.40 46 22.54] 12.70 38.1 305 se 1960135 | 54] 230 31 26.23 950 760 172 Sn reo 0.040 | te | 078 857 27.28 3.18 520 294 sr 407-0005 | 02 | oat 18 4.08 Gian eit) ar te 21a ore | 31 | 158 0968 «7.49 640 973 38 Ti 3s¢ 0.050 | 20 | 78 1010 8.48 318 924 55 1 190 0.002 | 37 | 158 © 1103 4.04 640 1019 20 v ez 0.028 | 11 | 078 1083 3.94 318 1025 26 w 207 0.075 | 30 | 156 749 18.79 640 447 196 y sm g.ot2 | 08 | 03t 1015 3.63 127 14 a5 zn 213, ost | 124] 4.70 910 68.69 191 1010 96 ze 339 0.022 | 09 | ost 707 54.20 427 408 424 (a) Values reported were obtained with a Spectro Analytical nsiruments EOP IGP:performance may vary with instrument and should be independently verified. (b) Values are certified by Inorganic Ventures INC. at 3x and 10x the approximate instrumental LOD (12) (c) Bold values are qualitative only because of iow recovery. Other digestion techniques may be more appropriate for these elements and thelr compounds. ‘MOSH Manual of Anaytic! Methods (NMAM), Fount EditonELEMENTS ON WIPES 9102 MW: Table 1 CAS: Table 1 RTECS: Table 1 METHOD: 9102, lssue 1 EVALUATION: PARTIAL tase 1: 15 Mareh 2003 OSHA: Nia PROPERTIES: Table 1 NIOSH: Nia ‘ACGIH: NIA ELEMENTS: Arsene tron Seleniom Zine Barium Lanthanum Stver Zion Berylium Lens Strontium Cagmium Manganese Telurium Cosatt Motyodenum ——Thatium Cooper Nickel Vanadium CGromiom Phosphorus Yiu SAMPLING MEASUREMENT SAMPLER: WIPE TECHNIQUE: INDUCTIVELY COUPLED ARGON PLASIWA, ATOMIC EMISSION FLOW RATE: NIA ‘SPECTROSCOPY (ICP-AES) VOLMIN: NA ANALYTE: Elements above OMAK: ASHING SHIPMENT: Routine REAGENTS: Gone. HNO, 20 mL: ang core. HCI, mt SAMPLE STABILITY: Stable CONDITIONS: Room temperature, 30min; 190°C to near dyress BLANKS: 21010 felt blanks perset le FINAL SOLUTION: 4% HNO,, 1% CIO, 10m ‘ACCURACY WAVELENGTH: Table? RANGE STUDIED: Not Studied oo a oe CORRECTION: Spectral wavelength shit OVERALL PRECISION (5,): Not detrmined CALIBRATION: Elamonis in 4K HNO, 1% HCIO, ACCURACY: Not determined eae Tebie 2 ESTIMATED LOD: Table2 PRECISION (8: Table 2 "APPLICABILITY: This method [sa simultaneous elemental analysis, nol compound specific. Vony that tho types of Compounds inthe samples are solublo with ie ashing procedure selected. Bacouse ths method desis wih wipes sample itis Important te Keepin mind thal the values obtained ae qualive INTERFERENCES: Specualinterferences are the primary interferences encountered in ICP-AES analysis. These are mniozed'by udsious wavelength selection inteeiomentcorecien factors ang Background cortetion, OTHER METHODS: This method supplements NMAM Mettod 73001]. Addtonal element methods, whether single lament ‘oc mulb-ateent, may be found in NMA Allemateinsinmentaion includes Name atom absorption spectroscopy fr cea flements and grophte fumace AAS for nereased sersviy NIOSH Manual of Anayical Methods (NAM, Fourth EssionELEMENTS ON WIPES: METHOD 9102, Issue 1, dated 15 March 2003 - Pago 2 of 5 REAGENTS: EQUIPMENT: 1. Nittic acid (HNO,), cone, ultra pure." 4. Sampler: Wash 'n Dri or ASTM equivalent{2) 2. Perchloric acid (HCLO,), cone,, ultra pure." [pre-packaged moist disposable towelette 3. Calibration stock solutions, 1000 p/m (wipe) ‘commercially available, or prepared per 2. Inductively coupled plasma-atomic emission instrument manufacturer's recommendation spectrometer, equipped as specified by the (see step 20). manufacturer for analysis of elements of 4. Dilution acid, 4:1 HNO,HCIO,. Mix 4 interest volumes conc. HNO, with 1 volume cone. 3. Regulator, two-stage for argon HCI0, Beakers, Philips, 125-mL. or Griffin, S0-mL, 5. Argon with watehglass covers."* 6. Disliled, de-ionized water. Volumetric flasks, 10-and 100-mL*" Assorted volumetric pipettes as needed."* Hotplate, surface temperature 150°C. Polystyrene centrifuge tubes, S0-mL and 15-mb. Hard-walled sample container. * See SPECIAL PRECAUTIONS ** Clean alll glassware with cone. nitric acia ‘and rinse thoroughly in de-ionized water. ‘SPECIAL PRECAUTIONS: Nitric and perchloric acids are strong oxidizers and extremely corrosive. Perform all perchloric acid digestions in a perchloric acid hood. When working with acids use gloves and avoid inhalation or contact with skin or clothing SAMPLING:(3], 1. Wearing a clean pair of powder-less, plastic gloves, place the template over the area to be sampled and secure it. If the area to be sampled is in a confined area and a template cannot be used, measure the sampling area, and delineate the area to be sampled with masking tape 2. Remove a mipe from its package, and untold it 3. Wipe the surface to be sampled using fingertips held together and applying firm pressure. Use an overlapping 'S' patter to cover the entire surface with horizontal strokes. Fold the exposed side of the wipe in, and wipe the same area using vertical ’S!-strokes, Fold the wipe again to reveal an unexposed surface, and wipe the surface a third time as described in step 3 6. Fold the wipe, exposed side in, and place it into a clean hard-walled sample cantainer (¢.9., 50-mL centrifuge tube). Seal securely and label the sample container. NOTE: Compositing of wipe samples is not recommended, because (a) they cause sample preparation and analytical aitficulties, and (b) site-specific analytical information is lost 7. Clean the template in preparation for the next wipe sample using water or a wipe. A disposable template may also be used. 8. Remove gloves and discard, Clean gloves should be worn for each new sample. 9. Field blanks: 10% of samples, at least three per batch. Remove unexposed wipes from packaging land place into sample containers. The field blanks should be collected at the beginning. middle, and fend of sampling SAMPLE PREPARATION: 410. Transfer the samples and blanks to clean beakers. 14, Add 20 mL concentrated nitic acid and 1 mL concentrated perchioric acid. Cover beaker with a watchglass. Let stand 30 min at room temperature. Start a reagent blank at this step. 412, Allow samples to heat for approximately 8 hours @150 °C. 18. Remove watchglass and rinse into the beaker with de-ionized water AIOSH Manual of Analyical Methods (NAM), Fouth EitonELEMENTS ON WIPES: METHOD 9102, Issue 1, dated 15 March 2003 - Page 3 of 5 14, Continue to heat on hotplate (120 °C), NOTE: Some species wil not be completely solubilized by this procedure, Alternative solubilization techniques for most of these elements can be found elsewhere. 18, Add additional amounts of HNO,, if necessary, until the solution is clear and the wipe media is. completely destroyed 16, Take the sample to near dryness (ca. 0.5 mL}. 17. Dissolve the residue in 0.5 mL dilution acid 18. Transfer the solutions quantitatively to 15-mL centrifuge tubes cr 10 mL volumetric flasks. 19. Dilute te 10 ml with de-ionized water. CALIBRATION AND QUALITY CONTROL: 20, Calibrate the spectrometer according lo the manufacturers recommendations NOTE: Typically. an acid blank and 10 pg/mL multi-element working standards are used. The following mutt-etement combinations are chemically and spectrally compatible in 4% HNO,/1% HCIO, a. Al, As, Ba, Be, Gd, Ca, Cr, Co, Cu, In, Fe, La: b. Pb, Li, Mg, Mn, Ni, P, K, Se, Se, Ag, Sr, TI, V. ¥, Zar ©. Sb, Mo, Te Sn, Ti, W, Ze; 6. Pt 21. Analyze a standard for every six samples. 22. Check recoveries with at least Wo spikes media blanks per ten samples. MEASUREMENT: 23. Set spectrometer to conditions specified by manufacturer. 24. Analyze standards and samples NOTE: If the values for the samples are above the range of the standards, dilute the solutions with dilution acie, re-analyze and apply the apprapriate dilution factor in the calculations, CALCULATIONS: 25, Obtain the solution concentrations for the sample, C, (ug/mL), and the average media blank, ©, git}, from the instrument. 26, Using the solution volumes of sample, V, (mL), and media blank, V, (mL), calculate the concentration, © (ugiom’), of each element on the surface area sampled, S (om?) CW, - CY, cs Sets EVALUATION OF METHOD: This method was evalusted using wipe media spiked with aqueous standards (fortified samples) and wipe media spiked with SRM 2711 (Montana Soil). Recoveries for the twenty-three elements listed on page 9201-1 were within the range of 75-115% for the fortified samples. Ten of the elements found in SRM 2711 were recoverable within the same range. These are: silver, arseric, cadmium, cobalt, copper, manganese, nickel, phosphorus, lead, and zine. NIOSH Manual of Anaiticl Methods (NMAM), Fouth EatonELEMENTS ON WIPES: METHOD 9102, Issue 1, dated 15 March 2003 - Page 4 of 5 Because this method is @ simultaneous elemental analysis, itis not compound specific. The data provided is for hose compounds compatible with the acids used inthe digestion. Verification of the solubilty of specific compounds of interest should be completed and the sample matrix carefully examined. For example, if silicates are present total elemental values will not be measured without the use of hydrothioric acid in the digestion process, REFERENCES: [1] NIOSH [1994]. Elements by ICP, Method 7300 in: Eller PM, Cassineli ME, eds. NOSH Manual of Analytical Metnods, 4th ed,, Cincinnall, OH: U.S. Department of Health and Human Services, Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety 4 Health, DHHS (NIOSH) Publication No. 94-113. [2] ASTM [2002]. Annual Book of ASTM Standards, Standard Specification for Wipe Sampling Materials for Lead in Surface Dust. West Conshohocken, PA: ASTM International, E 1792-01 [3] ASTM [2002], Annual Book of ASTM Standards, Standard Practice for Field Collection of Settled Dust ‘Samples Using Wipe Sampling Methods for Lead Determination by Atomic Spectrometry Techniques, West Conshohocken, PA: ASTM Intemational, E 1728-88. METHOD WRITTEN BY: Ronnee N. Andrews, Mark Millson, and Donald D. Dollberg. NIOSHIDART TABLE 1. PROPERTIES Eloment (Symbol) Atomic Weight _MP (°C) cas# RTECS Silver (Ag) 107.87 961 7as0-22-4 —_yww3675000 ‘Arsenic (As) 74.92 at7 7440-382 60525000 Barium (Ba) 137.33 725 7440-393 C8370000 Berylium (Be) 9.01 sa? 7440-41-7 —_0S1750000 Cadmium (Cd) 1241 a2 7440-43.9 —EU9800000 Cobatt (Co) 58.93 1493 7aa0-48-4 — GF8750000 Chromium (Cx) 2.00 1900 7440-87-3 GB4200000 Copper (Cu) 63.54 1083, 7440-508 GL5325000 Iron (Fe) 55.85 1535 7439-89-56 _NO4565500 Lanthanum (La) 138.91 920 7499.91-0 Manganese (Mn) 54.94 1248 7439.96-5 009275000 Molybdenum (Mo) 95.94 2622 7439-98-7 — @QA4680000 Nickel (Ni) 5869 1855 7440-020 _QR5950000 Phosphorus (P) 2087 4 7723140 TH3495000 Less (Pb) 2072 328 7439-92-1 —OF7525000 Selenium (Se) 7896 217 7782-48-2 _vS7700000 Strontium (S1) 8762 768 7480-26 WKT849000 Tellurium (Te) 127.60 450 13494.80-9 _WY2625000 Thallium (M7) 204.38 304 7a40-28-0 _x@3425000 Vanagium (V) 50.04 1917 7aa0-622 _YW1355000 Yetium (¥) sect 1509 7a40-65-5 262980000 Zine 2n) 65.39 420 7440-68-6 28600000 e122 1887 7aa0-67-7 247070000 NIOSH dtanual of Analytical Methods (NMAM), Fourth EtonELEMENTS ON WIPES: METHOD 9102, Issue 1, dated 15 March 2003 - Page 6 of 5 TABLE 2. WAVELENGTH, LIMITS OF DETECTION (LOD), RANGE & PRECISION Element (Symbol) Wavelength _ Instrumental Range Precision” (nm) Lop (ugiwipe) (Ss) (ugivpe) siner (Ag) 328 0.035 0.118-25.0 0.0701 Arsenic (As) 189 0.078 0.261-105. 0.0549 Barium (Ba) 455 0.010 0.0333-10.0 0.0370 Berylium (Be) 313 0.010 0.0333-10.0 0.0267 Cadmium (Cd) 226 0.010 0.0333-41.7 0.0273 Cobalt (Co) 228 0.010 0.0333-10.0 0.0301 Chromium (Cr) 267 0.010 0.0333-10.0 0.0287 Copper (Cu) 324 0.042 0141-114 0.0317 Iron (Fe) 259 0.074 0.246-60.0 0.0516 Lanthanum (La) 408, 0.018 0.0893-28.0 0.0279 Manganese (Mn) 257 0.010 0.0333-638. 0.0333 Molybdemum (Mo) 202 0.010 0.0333-10.0 0.0441 Nickel (Ni) 231 0.010 0.0340-206 0.0629 Phosphorus (P) 178 0.043 0.142-860. 0.128 Lead (Pb) 168 0.042 0.141-1160 0.0267 Selenium (Se) 196 0.10 0.338-75.0 0.0364 Strontium (St) 407 0.010 0.0333-10.0 0.0368 Tellurium (Te) 214 0.047 0.156-50.0, 0.0359 Thallium (11) 190 0.041 0.136-50.0 0.0256 Vanadium (V) 292 o.010 0.0333-25.0 0.0284 Yttium (Y) an 0.010 0.0333-10.0 0.0280 Zine Zn} 213 o77 256-350, 0.101 Zirconium (2) 339 0.026 0.0877-10.0 0.944 * Values were obtained with a Spectro ICP-AES: LOD may vary with instrument and shout be independently verti. NIOSH Manual of Anayical Methods (NAM), Fouth Esstion6-10 VAT Tuk Aesowd State of Calieria ——— Deparment of Industrial Relations 35 BQ 6 6 4 0. pivision oF OCCUPATIONAL SAFETY & HEALTH 4. check one: Ose Yd in 2.Region_% pistia_2 3. Date Submited x rT 4.Name PALL M. GRICL Cac/osyA _ 5. Phone NoC2)ESFYYE? FAX No. 359-427/ 6. Address 750 ROvAL CAKS WeiUC; Loom 10%, MoNeaUIA. my Volk (Stree (cy) (2p) r meant [OTs |h | De We 8, Sample information: s. C1 Urgent Lab Service Request District Manager Approvat TR Bate Tapas octal caftectes voume etd formation Requested ines {lables |UihE [Ma Jor ‘Mess! 2 alee | ae Wie | wave Fok TWalorat Bap = B Bash BY Grav Sample © Taplogar = Babbin By Fil Foner swe Tr 40. Comments: FD Bb SADC bP DN S2e0ud bbiZk LNT pistleptlep = Carol. Laer DeSK uber -to Khowt Puort , bLbase rest mee EAD TAWhaze 7 70 cue x (0 com 44. Custody Record: Released By: Received By: Time: Date: STM) H:2Py Talo | 12, Date Received by Labs dab usa.ony) Cl intact [) Broken C1 ing Cal/OSHA 18 (08/01/94) B10440 875FORM C1BX NOTES EMPLOYEE/WITNESS INTERVIEWS) eo. DEPARTMENT OF INDUSTRIAL RELATIONS DIVISION OF OCCUPATIONAL SAFETY AND HEALTH FIELD DOCUMENTATION WORKSHEET 7. Establishment Name: OE 2 Page oF 3 The company is engaged BAPE DECC LIAR: DCH SOS “Tsing the Tollowing operation(s) 4, Description of Sqaipment, processes and raw materials used in the operation(3) S. Flow Diagram: LJNO LIVES Page ‘Sketch or Map; JNO L]YES Page 6. Production rates are 7. Work Hours: The company’s buildings or worksite consist of 8. Ambient weather conditions were! 10. Windows and/or doors were: JOPEN CJCLOSED Th Heating systems LJ ON CJOFF Type: 12. Kir Conditioning: (JNO LIVES CON CIOFF 75 Hazards evalualed [a-General ndustiy Construction Tonner General Physical Conditions and [Hand and Portable Powered Tool [1] Excavation, Trenches, Earthwork Spructures & Equipment wSpecial Design Requirements [PF inausirial Trucks, Tractors, CO Vehicles, Traffic Control Haulage Vehicles & Earth Moving ef Access Workplace & Work Areas (Powered Transmission Equip.,. Floor, Root & Wall openings rime Movers, Machines & Parts Z Sanitation 2 Points of Operations & Other -Seatols jazardous Parts of Machinery Window Cleaning Zr Sompressed Gas Air Equipment [A Ladders © Powered Platforms for Exterior Cranes & Other Hoisting Equip. [] Saws-power Er Buiicing Maintenance 5 Noise (Powder Actuated Tools Sire Pactows and Porson 1 Control of Haz, Substances 1 Misc. Construction Toois/Equip Pratection C1 Miscellaneous Sate Practices [2-O6Et, Fumes, Mists, Vapors, Rooting operations & Equipment at. 1 Satety Belts, ete 1 Confined Spaces Other: © Personal Satety Devices and Hazardous Substances & Safeguards Processes Gi Genera! Piant Equipment and (Regulated Carcinogens ‘Special Operations Tree Work, atc. [2 Flammable Lig., Gases & Vapors ©) Agricutural Operations Spray Coating Operations Marine Terminal Operations []_Dip Tanks 5% < er Equipment ‘quipment and Fire Protection $ (ee (Jog W Diggit I Fe v Opt Feet De oy on 5 8/ ea ‘cavosta 1Bx (ons‘Sate of Caiforia DEPARTMENT OF INDUSTRIAL. RELATIONS DIVISION 0? OCCUPATIONAL SAFETY AND HEALTH FIELD DOCUMENTATION WORKSHEET Establishment Name LAD ra Page L-7 of Tr GO ey mama SMA DEEL Managements representative name: Job Tite Years with company: iness card? Ts there guing ta be a problem with my doing an inspection today? Ves (Ko) Consent granted? Cayo [Time consent was granted Gansent granted oy: NYAS. wy Adee [Are aitnese youremsloyees? Uf DS ‘Are there any workers here today who are nal employees of His company? ie —_— Soume Caarancrd aries present al opening conference AQUD (Lp5 RAD LAK = Renqre bbe HOSES 1 L —firine wate er HEV USE) — / ho L EON Coe = st LWIOT Sea | = tue tama price! Lubled Lite = (Mpeed Yenrianl Wo oterg — Nevewsg “SS OF LAT eH | = (UCreese PlesineS yr Uenriaz 5 ee — = TA [ (Mh oo District ident. No. ‘Opt Rept. No. TOYA 95 ( ‘CaOSHA TBX SignatureState of California DEPARTMENT OF INDUSTRIAL RELATIONS. DIVISION OF OCCUPATIONAL SAFETY ANO HEALTH FIELD DOCUMENTATION WORKSHEET Establishment Name: Page of I £ is) ie = / EN - a Ese {os = ! worttau 2 HE) i v : \ GHENT \ \— = Coty A eT i v xe a “lA wean — Daa Te We OF Ree mani (66 CaliOSHA TBXState of Chora DEPARTMENT OF INDUSTRIAL RELATIONS DIVISION OF OCCUPATIONAL SAFETY AND HEALTH FIELD DOCUMENTATION WORKSHEET t Establishment Name: | Page 7 of Signature Date Ul (lA Region Disiriet Tent. No. Opi. Repi. No op rsdalge( CaVOSHA TBXSue of California DEPARTMENT OF INDUSTRIAL RELATIONS DIVISION OF OCCUPATIONAL SAFETY AND HEALTH FIELD DOCUMENTATION WORKSHEET Establishment Name: Page 7 of VRE headed — Tneral steg tuwudy ~ " ‘Signature ["¢ [fa lee "BSA S4 ( ‘CaVOSHA TBX | Region District Tent, No. ‘Opt. Rept. No,Establishment Name: eis Pours [ele PK, Cond) 7 INDUSTRIAL RELATIONS ‘OCCUPRTIONAL SAFETY AND HEALTH FIELD DOCUMENTATION WORKSHEEL —~ tName: ___ | Page oR — { tAStt cal ep ASTI De =SWelae Be Nl (Re 9 ——— Bercy Cypast A af SA Gi Ue celurn Sige / Signature: - ‘Opt. Rept. No. Pda Pals Region District Tent No. CaVOSHATBXDEPARTMENT OF INDUSTRIAL RELATIONS DIVISION OF OCCUPATIONAL SAFETY AND HEALTH FIELD DOCUMENTATION WORKSHEET 5 Establishment Name: Rans Le Page / of | Becpecer as Uimnk? pro — Dobos pve Gawd lem Wwouctory 7 M23 Tuy (Ceep Come youn cleun — Lede syed = Vey IED Cn FT bac posure Splery WeIg§ tg — 15 [Siew olla Region District Taent. No. ‘Opt. Rept. No. Insp. oF. (<1 ‘Ca/OSHA TBXCASE FILE RESEARCHDescription for 3691 Seige e@ Page | of | << U.S. Department of Labor f ri) | occupational Safety & Health Administration www.osha.gov | Search 84 advanced Search | A-2 Index SIC Description for 3691 Description for 3691: Storage Batteries Division D: Manufacturing Major Group 36: Electronic And Other Electrical Equipment And Components, Except Computer Equipment Industry Group 369: Miscellaneous Electrical Machinery, Equipment, and Supplies 3691 Storage Satteries Establishments primarily engaged in manufacturing storage batteries. «= Alkaline cell storage batteries +» Batteries, rechargeable = Lead acid batteries (storage batteries) = Nickel cadmium storage batteries ['SIC Search | Division Structure | Major Group Structure | OSHA Standards Cited ] sack to Top wnw.osha.gav wvw.dol.gov Contact Us | Freedom of Information Act | Customer Survey Privacy and Security Statement | Disclaimers Occupational Safety & Health Administration 200 Constitution Avenue, NW Washington, DC 20210 hup:/Avww.osha.gov/pls/imis/sic_manual.display?id=835&tab~description 6/11/2008, Except Cop... Page | of | Description for 3356: Role and Extruding oFNonteo ag U.S. Department of Labor i Occupational Safety & Health Administration SS’ www.osha.gov , Search BO advanced Search | A-2 Index SIC Description for 3356 Description for 3356: Rolling, Drawing, and Extruding of Nonferrous Metals, Except Copper and Aluminum Division 0: Manufacturing Major Group 33: Primary Metal Industries Industry Group 335: Rolling, Drawing, Aad Extruding OF Nonferrous 3356 Rolling, Drawing, and Extruding of Nonferrous Metals, Except Copper and Aluminum Establishments primarily engaged in roling, drawing, and extruding nonferrous metals other than copper and aluminum. The products of this industry are inthe form of basic shapes, such as plate, sheet, strip, bar, and tubing. Establishments primary engaged in recovering nonferrous metals and alloys from scrap or dross are classified in Industry $3341; those manufacturing geld, silver tin, and other foils, except aluminum, are classified in Industry 3497; and those manufacturing aluminum foil are classified in Industry 3353. Battery metal Britannia metal, rolling end drawing Extruded shapes, nonferrous metals and alloys, Gold and goid alloy bars, sheets, strip, and tubing Gold rolling and drawing Lead and lead alloy bars, pipe, plates, rods, sheets, strip, and tubing Lead rolling, drawing, and extruding Magnesium and magnesium alloy tars, rods, shapes, sheets, strip, and Magnesium rolling, drawing, and extruding Nickel and nickel alley pipe, plates, sheets, strips, and tubing Nonferrous rolling, drawing, and extruding except copper and Platinum and platinum atloy sheets and tubing Platinum-group metais rolling, drawing, and extruding Silver and silver aloy bars, rods, sheets, strip, and tubing Silver rolling ard drawing Solder wire, bar acid core and rosin core Tin and tin alloy bars, pipe, rods, sheets, strip, and tubing Tin rolling and drawing Titanium and titanium alloy bars, rods, billets, sheets, strip, and Tizanium from sponge Tungsten basic shapes Welding rods Wire, nonferrous except copper and aluminum made in rolling mills Zinc and zinc alloy bars, plates, nipe, rods, sheets, tubing, and wire Zinc rolling, drawing, and extruding Zirconium and zirconium alloy bars, rods, billets, sheets, strip, and {cept copper and [SIC Search | Division Structure | Major Group *ructure | OSHA Standards Cited } ‘Back 10 Top ww. osha.cov ww d0l. gov Contact Us | Freedom of Information Act | Customer Survey Privacy and Security Statement | DSciaimers Occupational Safety & Health Administration 200 Constitution Avenue, NW ‘Washington, Dc 20210 hitp://\www.osha.gov/pls/imis/sic_manual display ?id=705 &tab=description 6/11/2008California Secretary of State - “alifornia Business Search - Corporation Search Results Page | of | sr Corporations yrmpeemea SSagacere see para of 2 zoe nto ny Roa [Name Availability Corporation x Panter Friendly Page eaoene Exe CORPORATION \eraertace noes Number: C0681 193][Date Filed: 5/21/1973]|status: surrender| — Duredition: DELAWARE = — aera —o TL SeRTRRD = esnn ERSHAN PA 1008 = | —— Agent for Service of Process. CT CORPORATION SYSTEM 1S WEST SEVENTH ST LOS ANGELES, CA SOOT New Search '© For information about certication of corporate records or for adeltional corporate Information, please reter to Corporate Records 1 Blank flee incicate the information aot contained in the computer file 1 ifthe status ofthe corporation is "Surrenger" the agent for service of process Is Butomatically revoked, Pease refer to Caforns Corporations Code Section 2144 for information flating o service upon corporations that have surrendered http://kepler.sos.ca.gov/corpdata/ShowAlIList?QueryCorpNumber=CO68 1 193 8/28/2008Naming Your Business: Fictitious Business Name Search Results Page 1 of | Sia RecorderiCouny Cork County Clerk Operations Voter & Election Information| Bonnet Saeten De ee Recorder Operations General information res crore http://www lavote.ne/CLERK/FBN_Results.cfm 8/28/2008poised va ph cio © Barmy BL 2-200 5. wou gx ucew Ta02-8 ae age a UP a as aEMPLOYER SUBMITTALS=XIDE CHNOLOGIES RECEIVED ne 27,2008 JUN 3 0 2008 peal M Gat Cal/ OSHA MONROVIA Associate Industrial Hygienist/Safety Engineer Department of Industrial Relations Division of Occupational Health and Safety 750 Royal Oaks drive, Room 104 Monrovia, CA 91016 Dear Mr. Grier: Per your request, I have enclosed the following documents: 1, OSHA Log 300 Recordable Incidents for this year and previous three years. 2. Site facility map 3. Lead Compliance Plan 4. Certificate of 15 ton overhead crane If you have any questions, please do not hesitate to contact me at (323) 262-1101 ext. 276. Sincerely Vianey Mendez Health and Safety Manager

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