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Construction and Building Materials 147 (2017) 194–202

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Construction and Building Materials


journal homepage: www.elsevier.com/locate/conbuildmat

Experimental study on dynamic mechanical properties of the basalt fiber


reinforced concrete after the freeze-thaw based on the digital image
correlation method
Yan-Ru Zhao a, Lei Wang a, Zhen-Kun Lei b, Xiao-Feng Han a, Yong-Ming Xing c,⇑
a
School of Civil Engineering, Inner Mongolia University of Technology, Hohhot 010051, China
b
State Key Laboratory of Structural Analysis for Industrial Equipment, Dalian University of Technology, Dalian 116024, China
c
Department of Applied Mechanics, Inner Mongolia University of Technology, Hohhot 010051, China

h i g h l i g h t s

 This paper studies the effect of basalt fibers and FTCs on the concrete impact resistance.
 Adding fibers could significantly improve the impact resistance of the concrete.
 The FTCs made the basalt fibers lose its enhancement effect.

a r t i c l e i n f o a b s t r a c t

Article history: This paper studies the effect of the basalt fibers and the freeze thaw cycles on the concrete impact failure
Received 19 September 2016 mechanism through the concrete beam fall ball impact test. The experiment used the digital image cor-
Received in revised form 23 December 2016 relation method to measure the full field strains and then make a real-time analysis of them. Based on the
Accepted 23 February 2017
number of impacts and the strain curves of the starting crack points, the impact times respectively for
initial cracking and eventual damaging were determined. The test results show that with the basalt fiber
content increasing, the impact times for the concrete specimens’ initial cracking and final failure were
Keywords:
also raised because adding fibers formed a three-dimensional system which could enlarge the transmis-
Dynamic impact
Freeze-thaw cycles
sion range of the impact stress waves and thus improved the concrete’s elastic deformation performance,
Fiber concrete that is, improved the concrete’s initial cracking capability to impact resistance. On the other hand, as the
Full-field strain number of freeze-thaw cycles increased, the impact times for the initial crack and the final failure
Digital image correlation (DIC) declined in that the freeze-thaw damage reduced the elastic deformation performance of the concrete
specimens. The impact energy in the early freeze-thaw period lost the fastest and the most, indicating
that the freeze-thaw cycles would produce damage and defect in the fiber/matrix interface and therefore
made the fiber’s three-dimensional system gradually lose its enhancement effect. The experimental study
provides a new approach to understanding the effect of the fibers and the freeze-thaw cycles on the
impact resistance performance of the concrete.
Ó 2017 Published by Elsevier Ltd.

1. Introduction frost resistance. Fiber reinforced materials include steel fibers, syn-
thetic fibers, basalt fibers, carbon fibers, hybrid fibers, etc.
The fiber reinforced concrete (FRC) has been developing rapidly Researchers have conducted some tests to study the dynamic
in recent years as a new type of cement base composite and has mechanical properties of various FRC materials under room tem-
been successfully applied in the field of military works, water con- perature [1–6] and have found that fibers can effectively improve
servancies, construction of buildings, airports, and high ways the brittleness of the concrete and thus improve its resistance to
owing to its excellent tensile an bending strength, crack and the impact load. However, in cold regions the concrete members
shrinkage resistance, impact resistance, anti-permeability, and are not only affected by such dynamic loadings as impact, vibration
and collision, but also affected by the loading of freeze-thaw cycles
⇑ Corresponding author. [7], which may lead to the change of the internal structure of the
E-mail addresses: zhaoyanru710523@126.com (Y.-R. Zhao), xym@imut.edu.cn material and the decline of its mechanical performance index
(Y.-M. Xing). [8–9]. Therefore, when calculating the structure design and

http://dx.doi.org/10.1016/j.conbuildmat.2017.02.133
0950-0618/Ó 2017 Published by Elsevier Ltd.
Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202 195

analyzing the damage effect, the freeze-thaw damage degradation and different freeze-thaw cycles, and discussed how the fiber
effect has to be considered apart from the impact damage effect of incorporation and the freeze-thaw damage affected the concrete
the dynamic loadings; otherwise the safety problems may arise by impact damage
overestimating the bearing capacity of the material. In addition, to
get familiar with the dynamic response properties of the FRC under
2. Experiment
freeze-thaw conditions is of great importance for evaluating the
structure damage repair and expanding its application to a much
2.1. Testing method
wider range.
At present, further research needs to be done to represent the
The digital image correlation method employs CCD camera to
real-time mechanical performance and micro-macroscopic failure
record the respective speckle images before and after the displace-
mechanism of the FRC under the freeze-thaw environment. As to
ment or deformation of the tested object to get two digital gray
the mechanical performance test under the freeze-thaw cycles,
level fields by analog digital conversion and then some correlation
the material deformation test is one of the most difficult. The tra-
calculations are operated to find the extreme value points of the
ditional strain gauge method is only able to measure the single
correlation coefficient and obtain the corresponding displacement
direction deformation and the displacement at specific directions,
or deformation [16].
but fails to attain the full-field strain information of the sample
In the correlation computation, the gray level of the pixel con-
surface, and the strain gauge is also easy to fail under freeze-
tains the displacement information, so the correlation method is
thaw cycles. The traditional fall ball impact test defines the initial
based on the gray level matching. Hence, it is necessary to set up
crack impact times as the impact times that make the specimen
a mathematical model to measure the image matching degree
produce microfractures when the strain gauge is placed at the bot-
before and after the deformation. The formula is as follows.
tom of the specimen, namely, the impact times when the concrete
strain mutation occurs at the specimen’s bottom [10]. However, it Rðf i ðx; yÞ  f Þ  ðg i ðx ; y Þ  gÞ
has been found in the experiment that after some specimens are C ¼ qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi ð1Þ
2
subject to impacts, the strain value of the gauge gradually Rðf i ðx; yÞ  f Þ  Rðg i ðx ; y Þ  gÞ2
increases but the mutation does not occur even when the specimen
Here, C is the correlation coefficient; f (x, y) and g (x⁄ y⁄) repre-
is completely damaged. As a consequence, the number of the initial
sent the two gray level image subareas before and after the defor-
crack impact times cannot be measured. This is because, on the one
mation. Due to the random speckle distribution, the spots
hand, the crack position cannot be accurately predicted, so the
distribution in the small area around each point of the object is dif-
crack does not go through from where the strain gauge is placed,
ferent and this small area is usually referred to as the subarea. By
and on the other hand, the freeze-thaw and the impact lead to
searching the peak value of the correlation coefficient C we can
the decline of the strain gauge bonding strength so the deforma-
determine the displacement both in direction X and direction Y
tion cannot be accurately transferred to the gauge.
for the target point and further obtain the strain change by numer-
The digital image correlation method (DICM) uses modern opti-
ical differential operation. In actual operation, the closer the corre-
cal technique to measure the mechanical full-field deformation
lation coefficient is to 1, the more reliable the displacement
with non-contact and high precision. It has been widely applied
computed; otherwise, the closer the correlation coefficient is to
to engineering due to its simple operation, low demand on the
0, the greater the calculation error for the displacement.
specimen surface treatment, automatic and precise measurement
[11–13]. In recent years, some researchers have used the DICM
to study the mechanical properties of concrete and rock and have 2.2. Specimen preparation
gained some achievements. Literature [14] applied the DICM to
test the deformation in the concrete fatigue experiment and The strength of the standard concrete used in the test is C30,
obtained the distribution of the displacement field and the strain whose mix proportion is listed in Table 1. The size of the specimen
field under the fatigue load, and therefore predicted the fatigue is 40 mm  40 mm  160 mm. In order to study the strengthening
cracking up location and made a qualitative judgment of the per- and toughening effects of the basalt fiber on the concrete, with the
formance degradation of the concrete specimen under the fatigue standard concrete mix proportion unchanged, different fiber con-
load. Literature [15] used DICM to study the strain field of the con- tents were added into the concrete, respectively, 0.0 kg/m3,
crete precast crack tip region, observed the crack propagation pro- 1.0 kg/m3, 1.5 kg/m3, 2.0 kg/m3 and 2.5 kg/m3. The physical and
cess and area, and calculated the fracture toughness of the mechanical properties of the basalt fiber are illustrated in Table 2.
material. Literature [16], by means of DICM, measured the crack In the process of specimen preparation, the dry mix of sand,
tip evolution process of the three-point concrete bending beam stone, cement, and basalt fibers was put into the mixer to stir for
and obtained the crack tip displacement field and strain field of 3–5 min so that the fibers could mix well with the cement, sand
the specimen under different loads. Literature [17,18] attempted and stone. Then water was added, stirring again for a while. In
to use DICM to study the deformation of rocks with microscopic order to avoid the continuing increase of the intensity during the
cracks, and found out that the displacement distribution obtained freeze-thaw caused by the short curing time, the experiment
was closely related to the distribution of the microscopic cracks, adopted the standard long time curing, namely, 120 days.
showing the opening up or closing effect of the microscopic cracks
in the rock damage. The above researches reveal that the DICM 2.3. Testing method
provides an effective experimental method for further study on
the material and structure fracture damage. The freeze-thaw cycling test used the ‘‘quick freeze method”
Based on the DICM and the three-point bending drop impact specified by the national standard GB/T 50082-2009 [19] to freeze
test, this paper conducted a real-time observation of the full field and thaw the specimen. The actual time for one freeze-thaw cycle
strain of the concrete beam specimen in the process of impact frac- lasted 3.5 h and the maximum and minimum central temperature
ture, and determined the initial crack impact times through the of the specimen were respectively controlled at 8 ± 2 °C and
changing patterns of the strain at the cracking points. It also stud- 17 ± 2 °C. The fall ball impact test was conducted after the spec-
ied the mechanical impact properties and the damage evolution imens had respectively undergone 15, 30, 45, 60 and 75 freeze-
characteristics of the concrete with different basalt fiber contents thaw cycles.
196 Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202

Table 1
Mix proportion of the concrete.

Cement (kg/m3) Coarse aggregate (kg/m3) Sand (kg/m3) Water (kg/m3) Water/cement W/C
385.42 1134.34 695.24 185 0.48

Table 2
Physical and mechanical properties of the basalt fiber.

Material Single fiber length (mm) Fiber diameter (lm) Density (kg/m3) Fracture ductility rate (%) Elasticity modulus (GPa) Tensile strength (MPa)
Basalt fiber 18 15 2650 2.4–3.0 95–115 3300–4500

The fall ball impact test used the self-designed three-point 3. Results of the test
bending device, with reference to the weight drop method [20]
put forth by the 544 committee of the American Concrete Institute 3.1. Full-field strain
(ACI). The drop hammer was a solid steel ball which weighs 63 g
and whose impact height was 500 mm. The two ends of the beam 3.1.1. Specimen without basalt fibers
were supported plainly with the clear span of 130 mm. A Fig. 2 demonstrated the full field cloud image of the horizontal
40 mm  40 mm steel plate was place on the impacted surface of strain exx acquired by the DIC method which changed with the
the specimen. The fall ball dropped freely from the stipulated number of impact times. At the beginning period of the loading,
height to hammer the specimen, thus completing an impact cycle. the full field strain was small, and the specimen’s bottom edge dis-
At the same time, the test also used the DIC method, that is, after played a strain concentration area which was larger than the other
every fall ball impact, when the specimen became stable, the areas, as is shown in Fig. 2(a) and (b); When the number of impact
CCD camera would take a record of it with manual control until times gradually rose to 47, apparent strain clusters appeared at the
it was damaged. The whole system block diagram is shown in bottom of the specimen (Fig. 2(c)); subsequently, cracks occurred
Fig. 1. and then extended upward because of instability (Fig. 2
The DIC test used 2 CCD cameras (supplement model) with 2 (d) and (e)) until the specimen fractured completely (Fig. 2(f)).
million pixels and the incandescent lamp was used as the fill light In the process of the impact failure, the maximum strain con-
to avoid the influence that may be caused by the frequent blinking centration appeared at the crack tip, whose movement trace (the
of the alternating lamp. In order to make the DIC results more red area) was almost identical with the direction of the main crack.
accurate, before the test, the surface of the specimen that faced The area subject to the strain concentration was reduced radiantly
the camera lens needs speckle spraying. After adjusting the focal from the crack tip to the surrounding area and became larger with
length and the needed light, the size and location of the specimen the increase of the impact times. Hence, the impact failure process
was calibrated by the calibration target whose size and shape had for the specimen with no basalt fibers can be described as follows.
been recorded in the computer. Then the image acquisition system An increased area of the horizontal tensile strain occurred on the
collected the images of the impact failure process. The speckle bottom part of the specimen and then it extended upward and
images were then put in the vic-3D software to compute the dis- cracks came up which extended because of instability, and finally
placement and the strain. the specimen got fractured.

Preparing concrete specimens


with different basalt fiber
contents and then having them
undergo the freeze-thaw cycle
test
DIC testing system
Light

Fall ball

Image card
Computer
DIC testing area
Light CCD camera
Fall ball impact test

Fig. 1. Scheme of setup.


Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202 197

fall ball impact points


‰ ‰ ‰ ‰ ‰ ‰
(a) 5.850
(b) 7.063
(c) 3.520
(d) 5.230
(e) 38.40
(f) 35.00

4.325 5.600 2.415 3.075 28.70 25.40

2.800 3.650 1.450 2.500 19.00 5.400

1.275 1.700 0.175 1.125 9.300 4.300

-0.250 -0.250 -0.140 -0.250 -0.400 -3.400

strain concentration area on the bottom cracking points cracks

Fig. 2. The full field strain ex of the impact failure Impact times: (a) 23, (b) 37, (c) 47, (d) 54, (e) 58, (f) 60.

3.1.2. Specimens with basalt fibers


For the specimens with 2.0 kg/m3 basalt fibers (without freez- 60
ing and thawing), the evolution of the cloud images for the hori-
zontal strain exx, which varied with the number of impact times, 50
is presented in Fig. 3. Like the specimen without fibers, the basalt

Impact times ni
fiber specimens (Fig. 3) experienced a similar impact failure pro- 40 60

cess: the strain concentration area at the bottom of the specimen 50

Impact times ni
became larger with the increase of the number of impacted times 30 40
(Fig. 3(b) and (c)), and then the crack occurred and extended 30 47 times
upward due to instability until the specimen fractured completely 20 20
(Fig. 3(d)–(f)). 10
10
However, there were also some differences. For the fiber speci- 0
men, the strain concentration area not only appeared at the bottom 0.0 0.5 1.0
0
part but also appeared around the impact point at the top. The two Strain (%)
areas approached to each other with the increase of the impact 0.0 0.5 1.0
times and then became connected to form a damage zone (Fig. 3 Strain (%)
(b) and (c)), and eventually, cracking appeared at the bottom of
the specimen and then extended upward (Fig. 3(d)–(f)). Fig. 4. Relationship of the impact times ni and the strain exx for the specimen with
no fibers.

3.2. The critical impact times and the impact times for final failure
the elastic deformation zone, where the strain value changed little
Using the DIC method the strain of any point within the range of and was on a linear rise with the increase of the impact times; the
observation could be computed, so the initiation and development second stage was the fracture transition zone, and with the num-
of the cracks could be studied through the full-field cloud image ber of impact times increasing to a critical value, the strain
where the horizontal strain exx changed under different loadings. increased dramatically, indicating that the cracks extended after
During the course of the impact damage of the specimens with crack initiation until the material was completely fractured.
no fibers, the developing relationship between the maximum hor- In order to accurately determine the number of impact times for
izontal strain exx at the bottom (i.e., the initial cracking point) and the initial cracking, we could observe and analyze the changing
the impact times ni was illustrated in Fig. 4. It can be seen that the pattern of the horizontal strain field at the maximum strain point
strain curve could be divided into two stages: the first stage was (the initial cracking point) on the bottom edge of the specimen

fall ball impact point impact point strain concentration area impact damage zone impact fracture zone
‰ ‰ ‰ ‰ ‰ ‰
(a) 1.899 (b) 0.416 (c) 1.138 (d) 2.520 (e) 23.368 (f) 30.80

1.505 0.010 0.470 0.565 18.550 22.70

0.980 -0.620 -0.420 0.410 12.100 14.60

0.455 -1.250 -1.321 0.356 5.450 6.50

0.061 -1.723 -2.577 -0.156 0.013 -1.60

crack
strain concentration area on cracking point
the specimen bottom
Fig. 3. The full field strain ex of the impact failure with 2.0 kg/m3 of fiber content Impact times: (a) 40, (b) 76, (c) 150, (d) 156, (e) 182, (f) 188.
198 Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202

by using DIC method. As is shown in Fig. 4, piecewise linear fitting 200


was conducted to the two stages of the elastic deformation zone n0
and the fracture transition zone to make the angular average line
W
intersect with the curves, and the coordinate value of the intersec-
tion point in each phase was taken as the initial crack strain and 150

Impact times ni
the critical impact times [21]. It could be seen from Fig. 4 that
the initial crack stain e0 of the concrete specimens with no fibers
and no freeze-thaw was 0.14%, and the critical impact times n0 100
was 47, whereas the impact times for the final failure W was 57.
Therefore, by analyzing the curves of the horizontal strain ex of
the cracking point at the bottom edge which varied with the
impact times, we could analyze the effect of the fiber content 50
and the freeze-thaw cycles on the concrete’s impact deformation
properties. 0.0 0.5 1.0 1.5 2.0 2.5
Fiber density (kg/m3)
3.2.1. The effect of the fiber content
For specimens with different amounts of fiber, the curves of the Fig. 6. The anti-impact property under different fiber density.
horizontal strain exx at the bottom crack point corresponding with
the impact times were shown in Fig. 5(a), which indicated that
adding fibers could significantly improve the impact resistance of 3.2.2. The effect of the freeze-thaw cycles
the concrete. In the elastic deformation stage, increasing the fiber Taking into account the effects of the freeze-thaw cycles on the
content could improve the elastic deformation performance of impact resistance of the concrete, specimens without fibers were
the concrete whereas in the fracture shifting stage, increasing the selected to be frozen and thawed 0, 15, 30, and 60 times respec-
fiber content could improve the anti-impact times. tively. Fig. 7 showed the relationship between the number of
Furthermore, by extracting the critical impact times n0 and the impact times and the strain at the cracking point under the respec-
impact times for final failure W in Fig. 5(a) and then mapping them tive freeze-thaw cycles. It could be seen from Fig. 7 that the freeze-
together, we could obtain the impact resistance of the specimens thaw reduced the elastic deformation capability of the concrete in
with different fiber density, as is shown in Fig. 6. It could be found the first phase. When the specimen was frozen and thawed 60
that both the critical impact times n0 and the impact times for final times, the slope of the strain curve in the first phase was only
failure W increased with the increase of the fiber density from 0 to 20% of that of the specimen with no freeze-thaw. In addition, with
2.0 kg/m3, then decreased for fiber density of 2.5 kg/m3, which the increase of the number of freeze-thaw cycles, the impact times
indicated that a certain amount of fiber content could improve for final failure came to decrease, but the strain limit increased sig-
the impact resistance of the concrete, or more specific, the cracking nificantly; under the same impact energy, the concrete after the
resistance and the damaging resistance, but if the fibers density is freeze-thaw deformed to a much larger degree, which indicated
2.5 kg/m3, it woud reduce the impact resistance of the concrete. It that the freeze-thaw cycles effected much damage to the concrete
was also found that the ratio between the numbers of impact times and therefore reduced its impact resistance.
causing the initial crack and that leading to the final failure did not Fig. 8 showed the relationship of the impact times and the
differentiated much. When the fiber contents were 1.0 kg/m3, strain at the cracking point for the specimen with 2.0 kg/m3 fiber
1.5 kg/m3, 2.0 kg/m3 and 2.5 kg/m3, the ratios of the impact times content after different freeze-thaw cycles. Similar to the specimen
for the initial cracking and that for the ultimate damaging (n0/W) without doped fiber, with the increase of the freeze-thaw cycles,
were respectively 86%, 75%, 85%, and 75%, which suggested that the elastic deformation performance in the first stage was reduced,
adding the basalt fibers mainly improved the impact resistance and the number of impact times causing the ultimate damage also
to the initial crack of the concrete. Once the specimen has cracked, declined, which signified that the freeze-thaw weakened the rein-
the basalt fiber does not have much to do to resist the macroscopic forcement of the basalt fiber and thus degraded the impact resis-
crack propagation. tance of the concrete. In addition, under the same freeze-thaw

60
160
Freeze-thaw times
140 50
0 15
120 30 60
40
Impact times ni
Impact times ni

100
30
80

60 20

40 3 3
0.0kg/m 1.0kg/m 10
20 3 3
1.5kg/m 2.0kg/m
3 0
0 2.5kg/m

0.0 0.5 1.0 1.5 2.0 -0.5 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0
Strain (%) Strain (%)

Fig. 5. Relationship of the impact times ni and the strain ex for the specimens with Fig. 7. Relationship of the impact times ni and the strain ex for the non-fiber
different fiber contents. specimens under different freeze-thaw cycles.
Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202 199

170 2.0-0
160
150
140
130
2.0-15
120
110

Impact times ni
100
90
80
70 2.0-30
60
50
40 0.0-0 2.0-45 2.0-60 2.0-75
30
20
10
0 0.0-15 0.0-30 0.0-60
0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0
Strain (%)

Fig. 8. The full field horizontal strain of the specimens with 0.0 kg/m3 and 2.0 kg/m3 fiber density under different freeze-thaw cycles (the number before‘‘-”refers to the fiber
content and the number after‘‘-”refers to the freeze-thaw cycles).

cycles, the ultimate damaging impact times of the fiber concrete 4. Discussion
were larger than those of the non-fiber concrete, suggesting that
under freezing and thawing, the doped fibers still played their rein- 4.1. The impact energy increase rate of the fiber content
forcement role.
Further, by extracting the critical impact times n0 and the From Fig. 9 it could be seen that when the freeze-thaw cycles
impact times for final failure W in Fig. 8 and then graphing them (45) were identical, the impact times of the fiber concrete for
in Fig. 9, a histogram could be attained to illustrate the specimens’ cracking and damaging were increased, compared with those of
capability for impact resistance with different fiber contents and the non-fiber concrete. In order to further study the influence of
under different freeze-thaw cycles. As was shown, with the same the fiber content on the concrete’s anti-impact mechanical prop-
fiber content, n0 and W decreased as the freeze-thaw cycles erty, the impact energy increase rate of the fiber content could
increased, which meant the freeze-thaw cycles would reduce the be defined as follows, in condition that the freeze-thaw cycles
impact resistance of the concrete. On the other hand, under the remained the same.
same freeze-thaw cycles (<30), n0 and W reached their peak value
Wm
when the fiber density was 2.0 kg/m3, which suggested that a cer- cm ¼  100% ð2Þ
W0
tain number of fibers could improve the concrete’s impact resis-
tance of the cracking resistance and failure resistance; however, In the above formula, cm is the increase rate (%) when the fiber
if the freeze-thaw cycles were beyond 30, the fibers functioned lit- content is m, referring to the improvement of impact resistance of
tle for the improvement of the concrete’s impact resistance. the fiber concrete compared with the non-fiber one. W0 and Wm
correspond to the number of impact times leading to failure when
200 the fiber content is 0 and m (kg/m3).
3
The relationship between the impact energy increase rate and
Initial cracking A--0.0kg/m the fiber content was demonstrated in Fig. 10. When the number
Failure B--1.0kg/m
3
of freezing and thawing cycles is small, the effect of fiber incorpo-
3
150 C--1.5kg/m ration on the impact energy of the concrete is significant, and the
3
D--2.0kg/m value of c first increases and then decreases. When the fiber con-
Impact times

tent reaches 2.0 kg/m3, c reaches its maximum value. With the
3
E-- 2.5kg/m
increase of freezing and thawing cycles, c value does not have
100
much fluctuation, indicating that the effect of the fiber incorpora-
tion on the increase rate of the impact energy is gradually becom-
ing smaller, and the freeze-thaw damage significantly weakens the
50 fiber enhancement.

4.2. The freeze-thaw loss rate and loss speed of the impact energy
A BC DE A BC DE A BC DE A BC DE A BC DE A BC DE
0 In order to further analyze how the freezing and thawing
0 15 30 45 60 75
affected the concrete’s mechanical property for impact resistance,
Freeze-thaw times
when the concrete was doped with the same amount of fibers,
Fig. 9. The impact resistance of the basalt fiber specimen under different freeze- the freeze-thaw loss rate of the impact energy could be defined
thaw cycles. as follows:
200 Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202

2.0 Freeze-thaw times


80
0 15
30 45
1.5 60 75
60

1.0
40

0.5
20 3 3
0.0kg/m 1.0kg/m
3 3
1.5kg/m 2.0kg/m
0.0 3
2.5kg/m
1.0 1.5 2.0 2.5 0
Fiber density (%) 0 15 30 45 60 75
Freeze-thaw times
Fig. 10. The impact energy increase rate of the specimens with different fiber
content.
Fig. 11. The impact energy loss rate under different freeze-thaw cycles.

W0  Wi
ai ¼  100% ð3Þ
W0 5
In the formula, ai refers to the freeze-thaw loss rate of the 0.0kg/m
3

impact energy (%) when the concrete was frozen and thawed i 4 1.0kg/m
3

times, or in other words, it means the impact energy loss degree 1.5kg/m
3

of the frozen-thawed concrete compared with the concrete with- 2.0kg/m


3

3 3
out freezing and thawing. The greater the impact energy lost rate, 2.5kg/m
the more damage the freeze-thaw cycles do to the concrete. W0
and Wi respectively refer to the damaging impact times under 0 2
and i freeze-thaw cycles.
Moreover, with the fiber content unchanging, the freeze-thaw
1
loss (decrease) speed of the impact energy could be described in
the following formula
0
W ði15Þ  W i W ði15Þ  W i
bi ¼ ¼ ; ð4Þ
i  ði  15Þ 15 0 15 30 45 60 75

among which, bi is the loss speed of i cycles of freeze-thaw, signify- Freeze-thaw times
ing the degree of the anti-impact energy loss of the fiber reinforced
Fig. 12. The impact energy loss speed under different freeze-thaw cycles.
concrete per freeze-thaw cycle. The impact energy lost speed is
used to indicate how fast the freeze-thaw cycles weaken the impact
resistance energy of the concrete. W(i-15) is the damaging impact 4.3. The microscopic reinforcement mechanism of the fiber
times when the freeze-thaw cycles range from i to 15. The i refers
to the number of freeze-thaw cycles which valued 15, 30, 45, 60 The impact load is transmitted in the form of stress wave in the
and 75 in the experiment. concrete. In the process of impact, if the stress wave keeps trans-
Fig. 11 showed the relationship between the impact rate loss mitting forward without any transference and remains the acute
rate and the freeze-thaw cycles, from which it could be found that crest, only a small volume of the material bears the stress and
with the increase of the freeze-thaw times, the anti-impact energy therefore brittle fracture occurs when the stress wave is strong
loss rate of the concrete, that is, the impact energy loss degree, was enough. When the basalt fibers are mixed into the concrete, a three
on increase. The relationship between the loss speed of the anti- dimensional supporting system would be formed since the fibers
impact energy and the freeze-thaw cycles was illustrated in distribute randomly and disorderly. As a result, under the external
Fig. 12, which revealed that as the freeze-thaw cycles increased, force, the fibers are able to have some loose movement and help
the energy loss speed went up and then fell down, in other words, the surrounding matrix to sustain the stress, and thus the trans-
in the beginning stage of freezing and thawing, the impact energy mission area of the stress wave becomes larger and larger, which
loss speed accelerated whereas in the later stage it slowed down. means only a much stronger stress can make the material fracture,
According to the characteristics revealed in Fig. 12, the process that is, the tenacity of the concrete has been enhanced. In the full
of energy loss of the fiber concrete under freezing and thawing field strain analysis for the fiber concrete specimens (Fig. 3), it
cycles could be divided into three stages, namely, the initial stage, could be observed that there formed the impact damage zone in
the middle stage and the final stage. In the initial stage of freezing the basalt fiber concrete, which indicated that the microscopic
and thawing, the loss speed was the fastest and the loss rate the enhancement mechanism of the fiber in the process of impact
highest. During this stage (the freeze-thaw cycles < 30), the loss could be attributed to the three dimensional system produced by
speed took on a quick rising trend (Fig. 12) and the loss rate was the fibers which made the impact stress transmission extend to a
rapidly raised to 53–64% (Fig. 11). In the middle stage (30< the much larger area, and consequently dispersed the impact strain
freeze-thaw cycles <60), the loss speed came to slow down in a certain range, consumed the impact energy of the fall ball,
(Fig. 12) and the loss rate slowly rose to 62–89% (Fig. 11). In the and improved the anti-impact times of the specimen.
final stage (60< the freeze-thaw cycles <75), the loss speed kept In addition, in the process of concrete making, the three dimen-
low and stable and the loss rate had reached around 90% (Fig. 11). sional supporting system formed by the randomly distributed
Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202 201

fibers in the concrete plays a supporting role which reduces the After the concrete is mixed with the basalt fibers, an interface
sinking of the aggregate and increases the homogeneity of the with some strength between the fiber and the matrix is needed
aggregate distribution, and thus improves the internal quality of to transfer the stress (strain), but the fatigue stress from the joint
the concrete such as its homogeneity. Consequently, the strain action of the ice expansion pressure and the seepage pressure in
concentration is less likely to occur which to a certain extent pre- the freeze-thaw cycles makes not only the concrete matrix but also
vents the occurrence of micro-cracking in the concrete, reduces the the interface crack. As the freeze-thaw cycles increase, the interfa-
sources and sizes of the micro-cracks. Therefore, with the increase cial damage becomes severe and the interfacial strength comes to
of the fiber content, the impact resistance performance of the con- decline, so it cannot transmit the stress any more, making the three
crete is also gradually improved. dimensional system gradually fail to work after 30 times of freez-
In terms of the modulus of elasticity, fibers can be divided into ing and thawing.
rigid and flexible fibers. The rigid fiber has a larger elasticity mod- During freezing and thawing, the fibers’ reinforcement effects
ulus and a stronger stiffness, so it has a high capability for load on the properties of the concrete matrix keeps on declining until
transmission, such as the steel fiber; on the contrary, flexible fibers the number reached 75, when the reinforcement of the fibers
have a smaller elasticity modulus and low stiffness, so they are totally disappeared. The spatial 3-D system produced by mixing
poor in load transmission but their elongation limit and deforma- fibers can expand the transmission range of the impact stress
tion resistance behavior are more advantageous, for example, the waves, but its effect comes to decline and after 30 freeze-thaw
Dura fiber, the nylon fiber and the basalt fiber. When the macro- cycles, it failed to work. In other words, before freeing and thawing
scopic crack propagates, the rigid fiber undergoes pullout failure 30 times, the fibers play two enhancement roles at the same time
in the cracking area which can provide a strong drawing resistance though they gradually decrease, but after that, the fibers only have
or ‘‘bridge” effect to inhibit the macroscopic crack from opening up one role left which continued to decrease. Therefore, in the initial
and extending; as to the flexible fibers in the cracking area, they stage (0–30), the impact energy of the specimen lost the most
experience pullout and broken failure under the instantaneous and the fastest (Fig. 11 and 12) because of the high porosity and
impact, which cannot offer enough drawing resistance to prevent low strength of the interface, so under the freezethaw damage,
the opening up and extending of the macroscopic crack. Therefore, the interface subjected the damage prior to the matrix.
when the basalt fiber content increases, the impact times from the
initial crack to the final failure do not have a significant increase.
In the test, for a particular fiber density, the best performance in
terms of first crack as well as failure impact resistance of the basalt 5. Conclusion
fiber concrete is given by concrete with 2.0 kg/m3 fiber density,
rather than 2.5 kg/m3 fiber density, which can be explained as fol- By combining the DIC method and the fall ball impact test,
lows: if fibers are made to fully play their enhancing and toughen- and by using the real time observation to the characteristics of
ing role in the concrete, it is necessary for each single fiber to be the full field strain and the evolution of the cracking points in
wrapped with a certain thickness of the concrete, for only in this the process of impact fracture of the concrete specimen beam,
way can the fiber and the cement base be made intensively inte- the research studied the effect of the basalt fibers and the
grated (connected), making them jointly bear the force. In other freeze-thaw cycles on the concrete’s mechanical performance
words, an interface with certain strength is needed between the of impact resistance. It was found that the full field strain of
fiber and the concrete matrix. If excessive fibers are added into the specimens with different fiber contents could reflect the
the concrete, it is difficult to mix the concrete homogeneously formation and evolution of the impact damage zone. The spatial
and fiber clusters are likely to occur, leading to insufficient bonding 3-D system formed by the fibers could help to expand the trans-
stress and strength because there is no cement between fibers or mission range of the impact stress wave and therefore could
the cement layers are too thin. In other words, there is not enough improve the impact resistance performance of the concrete.
interface strength, which eventually makes some fibers unable to However, the freeze-thaw cycles would result in damage and
play their role, or ‘‘fail”. These ‘‘failed” fibers not only cannot flaw at the fiber/matrix interface which made the fiber’s 3-D sys-
improve the various performances of the cement matrix but also tem gradually lose its enhancement.
may become the defects of the concrete due to their lack of bond- Meanwhile, the research used the horizontal strain exx at the
ing capacity. Therefore, excessive amounts of fibers will yield maximum strain point (the starting cracking point) at the speci-
adverse effect to the concrete and thus reduce its impact resistance men’s bottom edge to study the initial impact cracking and the
property. crack propagation. It wass found that the impact times and the
To sum up, the mechanism of the basalt fiber’s reinforcement strain exx curves could be divided into two phases, namely, the
effect on the concrete’s impact resistance lies in two aspects. On elastic deformation phase and the ductile fracture phase. The elas-
the one hand, the spatial 3-D system resulted from the mixing of tic deformation phase accounted for about 80% of the total impact
the basalt fibers enables the impact stress waves to transmit to a life span. By adding the basalt fibers, the anti-impact elastic defor-
much wider area; on the other hand, the fibers can improve the ini- mation property of the concrete could be improved, that is, the
tial defects of the concrete matrix. concrete’s crack initiation capacity for impact resistance was
improved. On the other hand, the freeze-thaw cycles weakened
4.4. The microscopic damage mechanism of the freeze-thaw cycle the performance of the concrete in the elastic phase and therefore
reduced the anti-impact property of the concrete.
When the saturated concrete is undergoing the freeze-thaw In addition, the impact energy loss during the freeze-thaw
cycles, the water in the concrete’s micro-pores under the interac- cycles could be divided into three stages: initial, middle and final.
tion of plus and minus temperatures, tends to form the fatigue The loss speed of the impact energy in the initial stage rose very
stress by the joint action of the ice expansion pressure and the fast and the loss rate could amount to 53–64%, which indicated
seepage pressure. When the fatigue stress rises to equal the tensile that in the early freeze-thaw period, the impact energy loss of
strength of the concrete, microscopic cracks take place inside the the concrete specimen is at the fastest speed and highest rate. In
material. With the increase of the freeze-thaw cycles, the cracks the middle stage, the loss speed fell down quickly and the loss rate
will run through with one another, resulting in the decrease of was up to 62–89%. In the final stage, the loss speed kept slow and
the anti-impact property of the basalt fiber concrete. stable and the loss rate reached approximately 90%.
202 Y.-R. Zhao et al. / Construction and Building Materials 147 (2017) 194–202

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