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Assessment of brittle fracture for PUR materials using local strain energy
density and theory of critical distances
R. Negru, L. Marsavina ⇑, H. Filipescu, C. Căplescu, T. Voiconi
University Politehnica Timisoara, Romania
a r t i c l e i n f o a b s t r a c t
Article history: Local strain energy density and theory of critical distances represent two recent approaches in assessing
Available online 11 August 2015 the brittle fracture of cracked and notched components. Experimental validation of these methods was
mainly conducted on materials with brittle behaviour (ceramics and PMMA). In this paper the applicabil-
Keywords: ity of these methods to another class of plastic materials, i.e. rigid polyurethanes of different densities,
Local strain energy density was investigated. For this, two types of specimens, single edge U-notched and asymmetric semi-
Theory of critical distances circular bend cracked specimens, were experimentally investigated at room temperature and considered
Polyurethane materials
for theoretical predictions. Both criteria provide reasonable predictions for the fracture load.
Ó 2015 Elsevier Ltd. All rights reserved.
http://dx.doi.org/10.1016/j.tafmec.2015.07.011
0167-8442/Ó 2015 Elsevier Ltd. All rights reserved.
R. Negru et al. / Theoretical and Applied Fracture Mechanics 79 (2015) 62–69 63
V-notched specimens made of PMMA and Duralluminium under – specimens with vertical (x = 90°) notch for predominantly
mode I and mixed-mode static loading, and fatigue tests on welded mode I loading, Fig. 1a. Distance S1 was kept constant at
joints and notched components in structural steel. The ‘‘local strain 60 mm and the distances S2 and m were varied to produce dif-
energy approach” was analytically developed to blunt V- and U- ferent mixed mode configurations, see Table 2;
notches under mode I loading by Lazzarin and Berto [23]. This – specimens with tilted U-notches (x = 135°) for predominantly
approach was extended to mixed mode I–II conditions based on mode II loading, Fig. 1b.
a numerical procedure by Gόmez et al. [24] and Berto et al. [25],
and to mode III loading conditions by Berto et al. [26] and The thickness of all SENB specimens was 10 mm and four differ-
Lazzarin et al. [27]. Validation of these developments of local SED ent notch tip radius q were considered: 0.5, 0.75, 1 and 2 mm.
was carried out on both static and fatigue multiaxial conditions SENB specimens were tested using a Zwick/Roell Z005 testing
(Lazzarin et al. [28–30], Berto and Lazzarin [31]). Recently, special machine with a maximum force of 5 kN, under displacement con-
issues of the local SED concept were investigated: semi-circular trol with a loading rate of 1 mm/min at room temperature. The
and other shapes of the control volume, micro-rounded notches recorded load–displacement curves were linear, without any sig-
with application to fatigue strength evaluation of thin sheet nificant non-linearity, and the fracture occurred suddenly, indicat-
welded joints, and slit-parallel loading of a keyhole notch (Radaj ing a brittle behaviour.
et al. [32,33]). The generalized notch stress intensity factors (NSIFs – K uI and
In the present paper brittle fracture of two different K uII ) were determined along the notch bisector, according to
Polyurethane materials is investigated under mixed mode I + II Lazzarin and Filippi [39], Zappalorto and Lazzarin [40]:
loading. Two types of specimens were considered single edge
notched bend specimens with different notch radius and asymmet- pffiffiffiffiffiffiffiffiffi ðrh Þ pffiffiffiffiffiffiffiffiffi ðsrh Þ
K uI ¼ 2pr h¼0
; K uII ¼ 2pr h¼0
ð1Þ
ric semi-circular bend specimens. The predictions of the fracture 1 þ q=2r 1 q=2r
load were based on two engineering approaches: local Strain
where rh and srh are the stresses and (r, h) are the polar coordinates
Energy Density (SED) and Theory of Critical Distances (TCD), and
(see Fig. 1a and b). Stress distributions rh and srh were obtained per-
were compared with the experimental data.
forming a linear elastic finite element analyses under plain strain
conditions using ABAQUS 6.13 software. Bi-quadratic finite ele-
2. Materials ments with reduced integration CPS8R 8-node were considered,
with a refined mesh around the U-notch tip. The mean values K uI
Polyurethane (PUR) materials Necuron 651 (density 708 kg/m3 and K uII were computed over the distance 0.4q starting from the
with a porous microstructure) and Necuron 1020 (density notch tip, as it is recommended in [41]. The mixed mode ratio
1218 kg/m3 with a solid microstructure), produced by Necumer was quantified using the mode mixity through the dimensionless
GmbH Germany [34], were tested in the experimental program parameter Me:
(Marsavina et al. [35]). !
The Young’s modulus and Poisson’s ratio of the considered 2 K uI
e 1
materials were determined by Impulse Excitation Technique [36] M ¼ tan ð2Þ
p K uII
and are presented in Table 1.
The mechanical properties under tensile loading, Table 1, were proposed by Ayatollahi and Torabi [42]. For each loading configura-
determined on two types of specimens: tion, the mode mixity parameter Me slightly depends on the notch
radius, see Table 2.
– dog bone specimens with a gage length of 50 mm and a rectan-
gular cross section with 19 mm 10 mm (EN ISO 527 [37], 3.2. Asymmetric semi-circular bend (ASCB) specimens
Filipescu [38]);
– semicircular edge notched specimens, having a net cross section ASCB specimens with vertical crack were considered for mixed
area of 10 mm 10 mm and a notch radius of 5 mm (the stress mode loading, Fig. 2. The crack tip was introduced using a razor
concentration factor Kt is equal to 1.62), used to determine the blade. Different types of applied mixed mode are easily obtained
notch strength as the maximum normal stress existing at the only by changing one of the supports position (S2) and keeping
edge, at the moment before crack initiates [7,31]. constant the other support (S1). The load is applied on the symme-
try axis of the specimen using three point bending grips. Stress
3. Experimental results intensity factors (SIFs) solution for ASCB specimens is expressed
in the form, [43]:
3.1. Single edge notched bend (SENB) specimens
F pffiffiffiffiffiffi
Km ¼ paY m ða=R; S1 =R; S2 =RÞ; m ¼ I; II ð3Þ
Single edge U-notched specimens loaded in three point bending
2Rt
(SENB) were considered for evaluation of mixed mode brittle frac- where Ym represents the non-dimensional SIFs and were obtained by
ture made of Necuron 1020. According to Berto et al. [25] two types finite element analysis [39] and are plotted in Fig. 3 for a crack length
of specimens were investigated in order to achieve from pure a = 20 mm, specimen radius R = 40 mm, distance to fixed support
mode I to mode II conditions: S1 = 30 mm, thickness t = 10 mm, resulting a/R = 0.5, S1/R = 0.75. It
could be observed that changing the distance S2 from 30 mm to
Table 1 3 mm, the loading conditions change from pure mode I to dominant
Elastic, mechanic and fracture properties of the PUR materials.
mode II conditions. Moreover, using a polynomial interpolation the
PUR density 708 1218 exact position of left support, leading to pure mode II loading condi-
Young’s modulus E (MPa) 1250 ± 15.00a 3340 ± 7.1a tion, was determined at distance S2 = 2.66 mm.
Poisson’s ratio m (–) 0.302 0.343 The tests were carried out on a Zwick/Roell Z005 testing
Ultimate tensile strength ru (MPa) 17.40 ± 0.32a 49.75 ± 0.18a machine with a maximum load of 5 kN, under displacement con-
Tensile notch strength rn (MPa) 34.95 ± 1.85a 79.05 ± 1.46a
trol with a loading rate of 1 mm/min at room temperature. For
a
Standard deviation values. each material and support position, four specimens were tested.
64 R. Negru et al. / Theoretical and Applied Fracture Mechanics 79 (2015) 62–69
Fig. 1. SENB specimen geometries (dimensions are in millimeters) – (a) normal notch, (b) tilted notch.
Table 2
Geometry and average maximum fracture load for tested SENB specimens, Necuron 1020 (density 1218 kg/m3).
q (mm) S2 (mm) m (mm) x (°) Fmax (N) K uI (MPa m0.5) K uII (MPa m0.5) Me (–)
Table 3
Experimental results for mixed mode fracture tests on ASCB specimens.
Necuron S1 (mm) S2 (mm) Fmax (N) K I (MPa m0.5) K II (MPa m0.5) Me (–)
Fig. 4. Critical values of notch stress intensity factors versus notch radius.
radius. Such a dependence is very useful for determining the by ‘‘the maximum normal stress existing at the edge at the moment
apparent notch fracture toughness of notched specimens with dif- preceding the cracking” determined on tensile specimens with
ferent notch radius. Similar relationships were proposed in the lit- semi-circular notches, [31].
erature: by Taylor plotting the notch fracture toughness versus the Firstly, Lazzarin and Zambardi [22] proposed the local SED
square root of notch radius [44], respectively by Gόmez et al. pre- approach for the case of sharp V-notches under mixed mode I–II
senting the normalized notch fracture toughness versus nondi- loading conditions. The analytical development refers to the in-
mensional notch root radius, [45]. plane stress–strain field close to the V-notch tip (Williams [47],
Lazzarin and Tovo [48]) and considers a circular sector centred at
the notch tip as critical volume (area), Fig. 5a. An isotropic and
4. Theoretical framework
linear-elastic material was assumed. The strain energy density
averaged in the circular sector of radius R was given as a function
4.1. The volume-based Strain Energy Density (SED) criterion
of notch stress intensity factors K V1 and K V2 :
Berto and Lazzarin [31], and later Radaj and Vormwald [46],
1 I1 ðcÞ V k1 1 2 1 I2 ðcÞ V k2 1 2
presented a comprehensive overview of the volume-based strain WðRC Þ ¼ K R þ K R ð6Þ
energy density criterion. Below, only a reminder of the main con- E 4k1 c 1 C E 4k2 c 2 C
cepts of the SED regarding brittle fracture of notched components
where
is reviewed.
SED criterion assumes that failure occurs when the mean value Z þc Z þc
Fig. 5. Control volume for sharp V-notch (a), crack (b) and rounded V-notch under mode I loading (c), Lazzarin and Berto [30].
Fig. 6. Control volume under mode I (a) and mixed I-II mode (b) loading for U-shaped notches, according to Lazzarin et al. [30].
2
ð1 þ mÞð5 8mÞ K IC tables for different notch opening angles 2a, different RC/q ratios
RC ¼ ð8Þ and Poisson’s ratio values in [23]. Substituting the stress rmax by
4p ru
the generalized notch stress intensity factor K V1q , Gómez et al. [24]
For plane stress conditions, Lazzarin and Berto [50] derived the
proposed a compact form for Eq. (10):
corresponding expression:
2 2
5 3m K C K V1q 1
RC ¼ ð9Þ W 1 ¼ Hð2a; RC =qÞ ð11Þ
4p ru E q2ð1k1 Þ
where KC is evaluated under appropriate constraint conditions. For U-notches, when 2a = 0 and r0 = q/2 (Fig. 6a), Gómez et al.
Afterwards Lazzarin and Berto [23] extended the local SED [24] simplified the Eqs. (10) and (11) as follows:
approach from sharp to blunt V- and U-notches. The analytical 2
developments were carried out under tensile loading (mode I) K V1q
pr2max
using the stress distribution ahead of the notch tip proposed by W 1 ¼ HðRC =qÞ ¼ HðRC =qÞ ð12Þ
Filippi et al. [51] and considering an isotropic and linear elastic 4E Eq
material. For rounded V-notches, a crescent-shaped control vol- Under mixed I–II mode conditions (meaning tensile and in-
ume bounded by two radii differently centred was introduced: a plane shear loading) the maximum principal stress rmax occurs
circular notch edge with radius q as the inner boundary and a cir- on a notch edge point determined by the polar angle u, out of
cle arc with radius r0 + RC as the outer boundary, (Fig. 5c). The the bisector plane. Gómez et al. [24] assumed that the crescent-
length r0 represents the distance between the origin of the polar shaped volume is centred at this point, with no change in its shape.
coordinates (used to express the stress field) and the notch tip. This hypothesis involves that the control volume is rotated by the
Following this track, under mode I loading, Lazzarin and Berto polar angle u around the base point of radius q (Radaj and
[23] obtained the elastic average SED in the form: Vormwald [46]). Also, the angle u indicates the crack initiation
point and the crack propagation direction assumed as normal to
r2max
W 1 ¼ Fð2aÞHð2a; RC =qÞ ð10Þ the maximum principal stress on the notch edge. Thus, the proce-
E
dure developed for mode I loading was extended to mixed I–II
where rmax represents the maximum notch stress. Values of the mode conditions being numerically validated.
functions Fð2aÞ and Hð2a; RC =qÞ numerically derived are listed in For the investigated polyurethane materials, the material
parameters calculated using data listed in Tables 1 and 3, and
Eqs. (5) and (8) are presented below side by side with the PMMA
Table 4
(Table 4).
Values of material parameters for local SED criterion.
Fig. 7. Comparison between experimental and predicted values of the critical load for SENB U-notched specimens made from Necuron 1020: (a) Me ¼ 1:0, (b) M e ¼ 0:6,
(c) M e ¼ 0:2.
Fig. 9. Comparison between experimental and predicted values of the critical load for ASCB cracked specimens.
68 R. Negru et al. / Theoretical and Applied Fracture Mechanics 79 (2015) 62–69
a line drawn starting from the hot spot in a direction normal to the Acknowledgments
r1 stress. Usually, this direction is normal to the outer surface of
the notched components. This work was carried out in the framework of the project
Important consequences comes out from these studies: the crit- PN-II-PT-PCCA-2012-3-2-0068, contract number 206/2012
ical strength r0 does not depends on the degree of multiaxiality; financed by the Romanian National Authority for Scientific Research,
whilst the characteristic distance L changes with this parameter. CNCS – UEFISCDI.
Recently, starting from the aforementioned observations, Negru
et al. [54] proposed a similar equation that links L and the dimen-
sionless parameter Me for mixed mode I–II loading conditions:
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