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Abstract
Due to the increasingly serious environmental problems presented by waste tires, the feasibility of using elastic and flexible tire–rubber
particles as aggregate in concrete is investigated in this study. Tire–rubber particles composed of tire chips, crumb rubber, and a com-
bination of tire chips and crumb rubber, were used to replace mineral aggregates in concrete. These particles were used to replace 12.5%,
25%, 37.5%, and 50% of the total mineral aggregate’s volume in concrete. Cylindrical shape concrete specimens 15 cm in diameter and
30 cm in height were fabricated and cured. The fresh rubberized concrete exhibited lower unit weight and acceptable workability com-
pared to plain concrete. The results of a uniaxial compressive strain control test conducted on hardened concrete specimens indicate large
reductions in the strength and tangential modulus of elasticity. A significant decrease in the brittle behavior of concrete with increasing
rubber content is also demonstrated using nonlinearity indices. The maximum toughness index, indicating the post failure strength of
concrete, occurs in concretes with 25% rubber content. Unlike plain concrete, the failure state in rubberized concrete occurs gently
and uniformly, and does not cause any separation in the specimen. Crack width and its propagation velocity in rubberized concrete
are lower than those of plain concrete. Ultrasonic analysis reveals large reductions in the ultrasonic modulus and high sound absorption
for tire–rubber concrete.
Ó 2008 Elsevier Ltd. All rights reserved.
0956-053X/$ - see front matter Ó 2008 Elsevier Ltd. All rights reserved.
doi:10.1016/j.wasman.2008.01.015
A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482 2473
2. Experimental design
groups are shown in Fig. 1. Particles of tire finer than
In order to investigate the mechanical properties of tire– 0.15 mm may disturb the cement paste reaction (Neville,
rubber concrete, specimens of a cylindrical shape 15 cm in 1995); thus these particles were removed from the tire
diameter 30 cm in height were fabricated. These speci- aggregate source using a sieve # 100 based on the ASTM
mens were different in the content and type of tire particles C136 method. Tire particles were not pretreated before
as a portion of total aggregates in concrete. their incorporation into the concrete mixture. The proper-
ties of fine and coarse aggregates were determined accord-
2.1. Materials ing to ASTM standard test methods C127, C128, C129,
and C136. The grading of tire–rubber materials was deter-
Constituent materials for concrete mixes included a mined based on the ASTM C136 method. The grading
Type I Portland cement meeting ASTM C150 require- curve of rubber materials was determined by using crushed
ments, crushed stone gravel with a maximum size of stones in each sieve in order to provide adequate pressure
20 mm as a coarse aggregate, natural sand with a on tire–rubber particles to pass the sieves. Grading curves
4.75 mm maximum size as fine aggregate, and tire–rubber are presented in Fig. 2. Data regarding the properties of
particles provided by the Yazd Tire Company in Iran. Tire the aggregates and the rubber particles are given in Table
particle specifications are summarized in Tables 1 and 2. 3. The specific gravity of the cement was evaluated to be
These specifications were provided by tire manufacturers 3.15 g/cm3.
according to ANSI (American National Standard Insti-
tute) tests. Two types of scrap tire–rubber particles were
used: crumb rubber, which was a fine material with grading
close to that of the aforementioned sand, and coarse tire
chips produced by mechanical shredding. Tire particle
Table 1
Rubber–tire specification
Rubber powder specification
1 Specific gravity 1.16 g/cm3
2 Ash content 5%
3 Plasticizer 10%
4 Carbon black 29%
5 Polymer 50%
6 Sieve residue on mesh 40 3.36%
7 Sieve residue on mesh 60 80%
Packing: bags of 30 kg
Fig. 1. Type of tire–rubber particles.
2474 A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482
Table 4
Experimental program
Specimen Tire content (%) by Fine tire Coarse tire Fine mineral Coarse mineral Replicates in Replicates in
designation total aggregates aggregate (%) aggregate (%) aggregate (%) aggregate (%) compressive test ultrasonic test
P 0 0 0 100 100 3 2
C25 12.5 0 25 100 75 3 2
C50 25 0 50 100 50 3 2
C75 37.5 0 75 100 25 3 2
C100 50 0 100 100 0 3 2
F25 12.5 25 0 75 100 3 2
F50 25 50 0 50 100 3 2
F75 37.5 75 0 25 100 3 2
F100 50 100 0 0 100 3 2
C25F25 25 25 25 75 75 3 2
C50F50 50 50 50 50 50 3 2
Table 5
Concrete mixture proportions
Specimen Water Cement Coarse tire aggregate Fine tire aggregate Gravel Sand Moisture of gravel Moisture of sand
(lit) (kg) (kg) (kg) (kg) (kg) (%) (%)
P 227 350 0 0 900 900 0 0
C25 229 350 152.375 0 675 900 2.6 5.5
C50 299 350 304.18 0 450 900 2 6.4
C75 356 350 456.3 0 225 900 3 8
C100 442 350 609.5 0 0 900 3 7
F25 215 350 0 149.5 900 675 3 7
F50 282 350 0 299 900 450 4 7.5
F75 384 350 0 452.1 900 225 3 2.5
F100 453 350 0 602.8 900 0 3 7
C25F25 298 350 152.375 149.5 675 675 3 6
C50F50 434 350 304.2 301.4 450 450 4 9
A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482 2475
slump (cm)
5.5
2.3. Test methods
4.5
To evaluate the properties of fresh concrete, slump and
3.5
unit weight were measured according to ASTM C143 and
ASTM C138 (ASTM, 1988), respectively. A compressive 2.5
strain-control test was conducted for hardened concrete
1.5
specimens to obtain the stress–strain curves for all of the 0 10 20 30 40 50
specimens. The test was performed by a universal testing Tire content (%) of total aggregates
machine and a sensitive data acquisition system. The
machine yielded a loading value variation due to a constant b 2500
rate of specimen deformation. This rate was chosen to be Coarse
0.005 mm/sec. The ends of the cylinders were capped with Fine
Tire–rubber concretes are able to withstand loads beyond crete specimens. In contrast, the propagation of failure
the peak load, which is referred to as post-failure strength. symptoms were abrupt and concentrated for plain con-
Failure states in plain concrete specimens, as shown in crete. Fig. 4 demonstrates that the failure parameters grow
Fig. 4, are accompanied with the separation of pieces or uniformly from the bottom to the top of a C25 of
slices from the specimen. For concrete containing tire par- specimen.
ticles, the failure state was not accompanied by any detach- The lateral deformations of tire–rubber concrete speci-
ment due to the bridging of cracks by rubber particles. mens are larger than those of plain concrete specimens;
Tire–rubber concrete specimens did not exhibit any detach- however, because of the porosity due to the substitution
ment, despite losing a considerable amount of strength as of tire particles, Poisson’s ratios for tire–rubber concrete
shown by the F25 and C25 specimens in Fig. 4. are slightly more than those for plain concrete. It is impor-
Tire–rubber concrete specimens present large deforma- tant to note that the behavior of rubberized concrete is not
tions compared to plain concrete specimens. During the perfectly elastic, therefore Poisson’s ratio is not constant
unloading process, the flexible behavior of tire particles for the entire loading process. Poisson’s ratio increases
decreases the internal friction among the concrete elements, and approaches 0.5 as the behavior of rubberized concrete
and recovers extra strain. becomes plastic-like. As shown in Fig. 4, considerable lat-
Failure properties, like discontinuities and cracks, eral deformations are observable in tire–rubber concrete
propagated uniformly and gradually in tire–rubber con- specimens after an entire loading process.
Fig. 5. compressive stress–strain response of rubber–tire concrete, (a) responses of concrete types shown all together, response of concrete with (b) 12.5%,
(c) 25%, (d) 37.5% and (e) 50% tire content by total aggregate volume.
2478 A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482
0.4
β
are slightly more than that of F specimens for total rubber
α concentrations lower than 25%; however for total rubber
0.2 40% of Ultimate Stress concentrations greater than 25%, the ultimate strength
results are reversed. Ultimate strengths of combined speci-
Nonlinearity Index= tg β / tgα
mens were nearly between the ultimate strengths of the C
0 and F specimens, but closer to F specimen strengths.
0 0.04 0.08 0.12 0.16
The systematic reduction of ultimate strength in tire–
Strain (mm/mm)
rubber concrete might restrict the use of tire–rubber con-
b 8 crete, with tire–rubber concentrations exceeding 25%, in
structural applications. Reduction in tire–rubber concen-
7 Coarse
Fine
tration and rubber particle pretreatments are required to
6 enhance the ultimate strength and other mechanical prop-
Nonlinearity Index
Combined
5 erties of rubber-particle concrete. Pretreatment is available,
4
ranging from an inexpensive and easy treatment with
water, to complicated and expensive physical, chemical,
3 and mechanical treatments. A typical treatment for tire–
2 rubber particles is a NaOH solution to improve rubber
1
adhesion with the cement paste (Segre and Joekes, 2000).
Another report, in contrast, states that a NaOH and silone
0
0 15 30 45 60 pretreatment of rubber does not significantly change the
Tire rubber content by total aggregate (%) compressive strength and splitting tensile strength of rub-
ber-concrete composites, when compared to untreated
Fig. 6. (a) Evaluation of nonlinearity index and (b) nonlinearity index for composites (Albano et al., 2005).
various types of rubberized concrete.
3.2.5. Toughness
aggregate concentration, while the shape of the stress– Toughness of tire–rubber concrete was determined by
strain curve is primarily affected by the coarse aggregate calculating the area under the stress–strain curve up to
concentration. These observations imply the stress–strain 80% of the ultimate stress in the post-peak region. The
response for CF tire–rubber concrete is located between toughness value is defined as a ratio between the area under
the corresponding C and F stress–strain curves equaling the stress–strain curve up to 80% of the ultimate stress, to
the total respective tire particles concentration. Hence the area under the stress–strain curve up to the ultimate
any desired stress–strain curve between the C and F curves stress. Fig. 7a illustrates how each of the areas was deter-
can be obtained by tuning coarse and fine tire mined. It should be noted that the 80% factor of ultimate
concentrations. stress was selected to limit further reductions in strength
level. Thus, the toughness index (Ti) is expressed as follows
T 80%
Table 6 Ti ¼ ð4Þ
Ultimate strengths and tangential moduli of elasticity for various concrete T 100%
types containing different tire–rubber contents
The toughness indices for different rubber concentrations
Concrete mixture Total rubber Stressmax (MPa) Et (GPa) and different mixtures are presented in Fig. 7b. Tire–rubber
content (%)
concrete exhibited greater toughness as compared to the
Control P 0 30.77 7.41 plain concrete. Toughness indices maximize as rubber con-
C-type C25 12.5 6.52 2.47 centration approaches 25% of the total aggregate volume.
C50 25 1.49 0.31 Beyond rubber concentrations of 25%, toughness indices
C75 37.5 0.65 0.12 decrease due to the systematic reduction in strength. The
C100 50 0.37 0.03
toughness index for a combined C25F25 mixture is higher
CF-type C25F25 25 1.17 0.42 than that of the F50 and C50 mixtures.
C50F50 50 0.53 0.04
F-type F25 12.5 6.36 1.15 3.2.6. Reduction factors (RF) for hardened concrete
F50 25 1.22 0.31 properties
F75 37.5 0.81 0.11 Mechanical property results of rubberized concrete
F100 50 0.55 0.04
showed that property values were primarily dependent on
2480 A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482
a 7
Ultimate Stress
a 1.0
4 T 100% =A 0.6
SRF
T 80% =A+B
3 Toughness Index=(A+B)/B 0.4
A
2
B
0.2
1
0 0.0
0 0.01 0.02 0.03 0.04 0.05 0 15 30 45 60
Strain (mm/mm) Rubber content by total aggregate volume (%)
b 7 b 1.0
Coarse All Data
6
0.8
Toughness Index
Fine
5 Combined
Poly. (All Data)
4 0.6
ERF
3
0.4
2
1 0.2
0
0 10 20 30 40 50 60 0.0
Rubber content by total aggregate volume (%) 0 15 30 45 60
Rubber content by total aggregate volume (%)
Fig. 7. (a) Evaluation of toughness index and (b) toughness index values
for various amounts of rubber contents. Fig. 8. (a) Strength reduction factor and (b) elastic modulus’ reduction
factor of all types of rubberized concrete containing different rubber
the total rubber concentration. Therefore, it is convenient content.
to establish a function to investigate the influence total rub-
ber concentration has on the mechanical properties of con-
crete. Hence, the reduction factor (RF) is defined for a and the tangential modulus of elasticity. A regression anal-
mechanical property as the ratio of the compressive ysis was utilized to determine the functional parameters.
strength or tangential modulus of elasticity in rubber-con- Eqs. (7) and (8) yield the ultimate SRF and tangential elas-
cretes containing a rubber concentration, R, to the value of tic modulus reduction factor (ERF) in terms of rubber con-
the control plain concrete. The variation of the RF-deter- centration in a volumetric ratio of total aggregate volume.
mined compressive strength and tangential modulus of The R-square values were determined to evaluate the accu-
elasticity corresponding to rubber concentration are pre- racy of the equations
sented in Fig. 8a and b, respectively. The RF was unity 12
for a 0% of rubber concentration (control specimen), and SRF ¼ 0:02 þ 0:98ð1 RÞ R square ¼ 0:99 ð7Þ
gradually decreased with increasing rubber concentration 11
ERF ¼ 0:01 þ 0:99ð1 RÞ R square ¼ 0:98 ð8Þ
from 0% to 50% by total aggregate volume. Khatib and
Bayomy (1999), in a similar study, examined several math- A comparison with results reported in literature demon-
ematical functions, including various degrees of polyno- strates that the strength obtained in this study is lower than
mial functions, and proposed the following equation to those reported by the others. For example, for a 7.5% total
quantify the reduction in the compressive strength rubber concentration, the SRF attained by Khatib and
m
Bayomy (1999) was 0.6 after 28 days; Li et al. (2004) ob-
SRF ¼ a þ bð1 RÞ ð5Þ tained a SRF of 0.55 from a 7.5% total rubber concentra-
Since the strength reduction factor (SRF) equals unity for tion. Eq. (7) from this study gives the SRF a value of 0.4
0% of R, the following condition can be satisfied from a concentration of 7.5% of total rubber. This anomaly
can be attributed to a lack of pretreatment of the tire–rub-
aþb¼1 ð6Þ
ber particles, improper calibration of equations based on
In Eqs. (5) and (6), the SRF varies from 1 to 0; R is the rub- concretes with higher tire–rubber contents, and tire type.
ber content in a volumetric ratio of total aggregate volume,
and a, b, and m are the functional parameters. Khatib and 3.2.7. Sound absorption
Bayomy (1999) found the functional parameters a, b, and The ultrasonic echo technique is a valuable tool for test-
m to be 0.1, 0.9, and 7 in concrete aged 28 days, respec- ing concrete elements. The ultrasonic test is performed by
tively. A similar procedure was conducted in the present an instrument composed of a transducer and a receiver.
study to examine the reduction factors for ultimate stress Acoustic waves were sent by the transducer and propagate
A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482 2481
ð1 þ tÞð1 2tÞ
EU ¼ qv2 ð10Þ
ð1 tÞ
Fine concrete.
4500 Combined
4. Conclusions and recommendations
3500
1. Fresh rubberized concrete mixtures with increasing rub-
ber concentrations present lower unit weights compared
2500 to plain concrete. Workability of rubberized concrete
with coarse rubber particles is reduced with increasing
1500 rubber concentration; however, rubberized concrete
0 10 20 30 40 50 with fine rubber particles exhibits an acceptable work-
Tire content (%) of total aggregates ability with respect to plain concrete.
2. The substitution of mineral aggregates with tire–rubber
c 60 particles in concrete results in large reductions in ulti-
Coarse mate strength and the tangential modulus of elasticity.
50
Due to the considerable decrease in ultimate strength,
Ultrasonic Modulus (GPa)
Fine
rubber concentrations exceeding 25% are not recom-
40 Combined
mended. Pretreatment of tire particle surfaces should
30
be considered for possible improvement of tire–rubber
concrete mechanical properties. An investigation is
20 needed to identify the influence of rubber’s mechanical
properties on the ultimate strength of rubberized
10 concrete.
3. More ductile behavior is observed for rubberized con-
0 crete compared to plain concrete specimens under com-
0 10 20 30 40 50
Tire content (%) of total aggregates pression testing. Unlike plain concrete, the failure state
in rubberized concrete does not occur quickly and does
Fig. 9. Results of the ultrasonic test: (a) hardened concrete unit weight,
(b) influence of rubber–tire on ultrasonic pulse velocity in concrete and (c)
not cause any detachment in the specimen’s elements.
values of the ultrasonic moduli for different concrete types. Crack width in rubberized concrete is smaller than that
2482 A.R. Khaloo et al. / Waste Management 28 (2008) 2472–2482