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Laser-based non-destructive

testing techniques for the


ultrasonic characterization
of subsurface flaws
A.M. Aindow, R.J. Dewhurst, S.B. Palmer and C.B. Scruby

Laser generation and detection of ultrasound has been used for remote
characterization of flat-bottomed holes, acting as subsurface flaws, drilled into an
aluminium test sample. A pulsed Nd:YAG laser system was used to generate the
ultrasonic source whilst a He-Ne laser interferometer detected the subsequent
surface displacements. The technique allows both the width and depth of flaws
to be assessed. Moreover, an analysis of the data shows that the method is
particularly suited to detection of flaws < 4 mm below the surface of the
sample, a region which is difficult to inspect by conventional contact ultrasonic
techniques.

Keywords: ultrasonic testing, lasers, flaw characterization

It is already well known that acoustic pulses may be used earliest applications was described by Bondarenko et allT1
to characterize subsurface flaws. For the detection of who used a Q-switched ruby laser emitting single pulses of
small flaws in metals, say < 1 m m in size, it is desirable about 2 J with widths of 30-50 ns. They employed a
that the acoustic pulses should have frequency com- Michelson interferometer for the measurement of acoustic
ponents in excess of 10 MHz. This broadband frequency pulses. The detector measured the normal component of
range has already been achieved using a pulsed laserl~-21, elastic displacement, and had a sensitivity of 1 nm in the
- an ultrasonic generator that has the advantage of being
-
frequency range 5 kHz to 150 MHz. By observing in
remote from the test sample under investigation. The transmission, they detected the presence of an artificial
nature of the acoustic waveforms so generated depends on planar defect by the absorption of the direct elastic pulse
many factors, relating to the nature of the acoustic propagating through parts of the test sample. Calder and
sourcel3-61. Acoustic propagation in solids is complex. In WilcoxlSl have used a similar arrangement to detect an
the bulk material, both longitudinal (L) and shear (S) artificial flaw consisting of a 1.5 m m diameter hole
waves may be propagated, and on the surface Rayleigh midway across a 25 m m aluminium plate. With 15 J from a
waves dominate. However, because of the nature of the Q-switched Nd:glass laser, they observed strong ultrasonic
laser acoustic source, these wave arrivals at a point are echoes, but found that the laser pulse caused appreciable
recognized not by an oscillatory displacement but instead local surface damage. Finally, Wellmanlgl has used a
by a step or pulse function. Q-switched ruby laser, with pulse energies from 0.9 to 1.4 J,
to detect simulated flaws in a polished stainless-steel disc.
On the surface of a sample, such acoustic events can be In this case both laser generator and laser detector were
recorded with the use of broadband detectors. Most located on the same side of the disc.
detectors of acoustic pulses are of a contacting nature,
thereby necessarily perturbing the original characteristics This previous work has shown that laser-based ultrasonic
of the acoustic pulse. If instead a laser interferometer is techniques are capable of flaw detection, but has made no
used, the detection system can be made remote, and where attempt to evaluate flaw characteristics from return
convenient some of the output optics can be made integral signals. Consequently, partly because interpretation has
with the laser generator. In addition, a laser interferometer never been demonstrated, and partly because laser
can be made to function as a broadband detector capable equipment is expensive, laser-based techniques have not
of I00 M H z frequency bandwidth. This high frequency been adopted by industry. However, they offer a truly
response may reduce its sensitivity, but we shall show in remote diagnostic technique and are of potential use in
this paper that its sensitivity is sufficient for the detection hostile industrial environments. For example, they have a
and characterization of certain types of subsurface flaw. role to play in the quality control of hot steel produced
from a rolling mill. Other techniques which could be
The use of two complementary laser systems for remote employed include acoustic transducers (EMATS),but these
flaw detection has been described previously. One of the need stringent cooling because of their proximity to the

0308-9126/84/060329-07 $3.00 © 1984 Butterworth Et Co (Publishers) Ltd


NDT INTERNATIONAL. VOL 17. NO 6. DECEMBER 1984 329
Beamsplitter Interference
Prisms /filter
He-Ne laser
/ ~ / iinterferometer
ntHe~
Nd ; YAG
laser ~
Output
J~ ~ I Convexlens, ]
,=,m . I
X/" i,,;;;;- /I I Storag
Stora II H Mini J
Photodiode ~.~ [ oscilloscope
oscillosc ] ] digitizer computer

h a 11
I I Testsample
T-:
/ / / / / / / / / / / / / / / / / / /
x-y table

Fig.1 Experimentalarrangement

hot steel and also have limited spatial resolution. We have He-Ne laser light, frequency-shifted at 10 MHz, was
therefore proceeded with a set of experiments to show that divided by a beam splitter to travel along different optical
quantifiable parameters can be extracted from ultrasonic paths before being recombined. Their mutual interference
flawdetection using laser-based techniques. was observed as intensity fluctuations which can be
In the present investigation, we have used two lasers related to small movements, typically < 50 nm. In our case
probing from the same surface of a polished flat a 10 m W He-Ne laser was used, with most of the light
aluminium sample, using flat-bottomed holes as sub- going into the main beam which was focussed onto the test
surface flaws. The laser source, used to generate the sample. About 5% was split off to form the reference beam,
acoustic pulses, had more than an order of magnitude less and travelled a fixed path before recombining with the back-
energy than in previous published work on flaw detection, scattered light from the test sample. Subsequent inter-
leading to situations in which the target remained ference between reference and scattered beams was
undamaged. From an analysis of signals received by the monitored by two photodetectors in an optical arrange-
interferometer, it has been possible to not only detect flaws ment which produced antiphase outputs, thereby sup-
remotely, but also to characterize features of the flaw. pressing spurious noise variations. Voltage signals, in the
100 mV range, were directly proportional to absolute
Experimental procedure displacement of the test sample's surface. Movements of
frequencies < 10 kHz were electronically filtered out. so
The experimental arrangement used is shown in Figure 1.
that the system's frequency response extended from
A Q-switched Nd:YAG laser operating at a wavelength of
10 kHz to 100 MHz.
1.06/~m was used as the system generating the acoustic
source. Operating parameters were set such that the laser To maximize signal-to-noise ratio, the He-Ne probe beam
provided output energies of 33 __+ 2 mJ in 30 ns, wi~h a was set normal to the test sample so that backscattered
multimode transverse mode structure. The unfocussed light was also a m a x i m u m on the same axis. Additionally,
beam diameter was 3.5 m m full-width-half-height, so that to prevent any significant pulsed Nd:YAG radiation
the average power density produced by the laser was travelling into the interferometer system, the high power
10 MW cm -~. After propagating through optical com- laser beam was misaligned to the surface normal by 5°,
ponents and b e a m deflectors, the power density on the and a transmission filter at the He-Ne wavelength was
surface of the metal sample wasN4 MW cm -2, insufficient introduced in the interferometer probe beam.
to cause significant change to the surface. In most experiments, the sample consisted of an
The laser was directed onto a polished face of an aluminium plate 177 × 100 × 12.5 mm in which flat-
aluminium test sample, and monitoring of the subsequent bottomed holes of diametera = 6.35 m m had been drilled
surface response was carried out with a visible He-Ne to various depths, normal to the plate. As viewed from the
laser probe b e a m which, in the first set of experiments, was opposite surface, such holes appeared as subsurface flaws
coincident on the surface with the infra-red laser pulse. A at measured depths ofh = 1.22 mm, 2.21 mm, 3.45 m m and
long focal length lens o f f = 1 m was used in the probe 4.80 mm. The surface was polished flat to N3/zm, and the
beam to produce a spot on the surface of "-0.5 m m sample mounted on a n x - y table for translation from one
diameter. The b e a m formed part of a phase-locked flawed region to the next.
interferometer which has been described else- Signal capture from the laser interferometer was either
where, ll01 being based on a Michelson arrangement. through an oscilloscope or a Tektronix 7612D digitizer

330 NDT INTERNATIONAL. DECEMBER 1984


linked to a H P 1000 minicomputer. Each waveform, t

representing the surface displacement, consisted of 2048


data points, and could be stored in the computer for later
signal processing, Synchronous external triggering was
obtained from a photodiode, type HP 5082 - 4220,
monitoring the Q-switched laser pulse. The pretrigger
facility allowed captured waveforms to show the earliest
event of each signal.
Results and discussion
For a sample with no defects the incident Nd:YAG laser E
pulse caused the surface of the sample to rise. Figure 2a
shows this surface motion when a laser pulse of 2 m m .

diameter with 13 mJ energy was incident on the metal.


With signal delays introduced into waveform capture by ~l i i i i t i i i
O,
the digitizer, the step rise occurs simultaneously with Time (8/J$ div -1 ) Time (8/,¢sdiv- I )
firing of the Q-switch laser, and represents relief of
internal stress close to the sample's surface as its Fig. 3 Elastic response on the surface of an aluminium sample for
temperature rises. Once heat has been delivered to the laminar type flaws of differing aspect ratios (a/h). A series of flat-
target the displacement remains essentially constant until bottomed holes were used with a diameter a of 6.35 mm, and the time of
the first rising edge of the waveform corresponds to the time when the
significant lateral diffusion takes place. This occurred laser was pulsed
over timescales longer than those seen in Figure 2a~ In
contrast, when the surface movement was examined over
a flawed region with h -- 1.22 mm, this waveform changed
showing significantly different features (Figure 2b). A
100 small, high frequency oscillation was superimposed on a
larger amplitude, low frequency oscillation. The
amplitude of the latter depended on the depth of flaw h
80 (Figure 3) such that the depth of modulation decreased as
h increased. The amplitude of this resonance, as viewed
on the oscilloscope trace, was found to be dependent on
60 the aspect ratio a/h of the flaw, and in our case could not

<E
40 /F be detected for flaw depths greater than 4 mm, where
a/h --<1.5.
Both the high and low frequency oscillations can be
understood in terms of elastic behaviour. We first consider
the low frequency oscillations, as shown in Figure 3. I fit is
20 assumed that a shallow flat-bottomed subsurface flaw is a
thin, clamped, circular plate vibratin~ normal to its
surface, then calculations by MorsePq show that the
I i ! I
fundamental resonance frequency is expected to be given
2.5 5.0 7.5 10 by
a
Time ~us)
Pf = 1.868 ~ - 1 )

50
where Yis Young's modulus, P the density and ~rPoisson's
ratio for the metal concerned. For aluminium
4O
Y = 70.3 G N m -s, (r = 2.7 X 10a kg m -3 and ~ = 0.345.
A comparison of calculated and experimental values is
i shown in Table 1. Experimental evaluation was easy for
cases where the aspect ratio was in excess of about three.
The table shows that agreement is poor, but progressively
improves as the aspect ratio increases. This is to be expec-
'< 20 ted, since for larger a/h the flaw resembles a "plate'
with its physical dimension a more clearly defining the
spatial region over which vibration takes place. It should
lo be noted that the 'plates' investigated in the present work
are only clamped, by the surrounding bulk of the material,
on one face. The diameter of the flaw is not defined on the
o i top face. One would therefore expect that the vibrations
0 2.5 5.0 7.5 10 normal to the surface increase in extent as one moves
b from the 'clamped' to the unclamped face. This results in
Time (/.~s) an overall increase in a for a given h.
Fig. 2 Initial elastic response on the surface of an aluminium sample If a cone angle, for the vibrational volume, of 46 ° is
when the laser spots were coincident above: a--an unflawed region; I~--a
flawed region (h = 1.22 ram. a = 6.35 mm). The time of the first rising
assumed and the plate diameter is taken as the resultant
edge of the waveform corresponds to the time when the laser was pulsed diameter produced on the top, unclamped, face, then the

NDT INTERNATIONAL. DECEMBER 1 9 8 4 331


Table 1. M e a s u r e d resonance frequencies of a flaxural m o d e of vibration above a subsurface f l a w in
aluminium, and comparison w i t h a theoretical model. In all cases, the w i d t h of f l a w a = ( 6 . 3 5 ± 0.1 ) m m

Depth of flaw, Measured (kHz) Calculated from Calculated (kHz) a/h


h (mm) Equation (1) (kHz) O N46° (see text)
(± 0.02 mm)

4.80 Below detection _ _ 1.32


threshold
3.45 188 + 10 869 193 1,84
2,21 170 + 6 557 188 2.87
1.22 152 + 6 307 155 5.20

frequencies shown in column four of Table 1 are


produced. These are seen to be in fair accord with the
experimental value. At presenL however, there is no
80 theoretical modelling available for this behaviour.
Although abetter fit to theory, and larger signals, could be
A
E obtained with larger a/h, values of a and h were chosen to
c 60 represent more typical subsurface defects in metals.
Figure 4a shows a typical experimental result when the
E aspect ratio was 5.2. It was found that the depth of
modulation depended on where the coincident laser spots
4o were positioned. As expected, this depth of modulation
was a maximum when the beams were centrally positioned
above the flaw, and decreased towards the flaw edges. The
20 resonance frequency could also be evaluated using a fast
Fourier transform procedure on the computer to generate
a waveform in the frequency domain (Figure 4b). The
1 I I 1 fundamental resonance frequency was clearly visible,
0 5O 100 150 200 together with some evidence of higher-order components.
When the diagnostic laser system was moved around the
a Time (/as) flawed region, the value of the fundamental resonance
frequency remained constant as expected - - only the
depth of modulation changed.
Hence, in a preliminary flaw investigation, the technique
described above may be used to estimate the area of the
flaw in situations involving thin plates or shallow laminar
flaws - - an area where conventional ultrasonic pulse-
¢.. echo techniques become difficult. In applications such as
the testing of bonded skins, h may be well known. If this is
so, the above technique can be used to monitor any 'plate'
oscillations, from which an estimate of the flaw area can
t~
be made using Equation (1), with the assumption of
v circular flaw symmetry. Using this method, values
"O
-n determined for the diameter a will always represent an
overestimate of their real extent.
"5
E Without some prior knowledge of the flaw depth h the
< technique is not sufficient to characterize the flaws fully,
only to obtain a2/h values. However, there was additional
_.) intbrmation within the laser-generated ultrasonic wave-
~ - - I. . . . . It- - --_i forms which could allow h to be evaluated indepen-
0 dently.
0.25 0.5 0.75 1
This information was obtained by considering the high
b Frequency (MHz) frequency oscillation, referred to previously and shown in
Figure 2b. A FFT of this waveform (Figure 5) indicated an
oscillation of small amplitude at 2.65 MHz, and was found
Fig. 4 Elastic waveform recorded over a 1.22 m m deep flat-bottomed to be reproducible on a shot-to-shot basis. Sucli a
hole, together with its fast Fourier transform. Figure 4a is the same periodicity can be interpreted as due to longitudinal
waveform as in Figure 2b, but shows the long timescale behaviour.
Incident laser energy was 3 6 mJ in a laser spot diameter of ~ 3 ram.
elastic waves propagating repetitively across the flawed
Firing.of the laser occurred at the same time as the initial rising edge of region. Pao et a/112I have previously shown that in the case
the waveform of an elastic plate, the epicentral surface response due to a

332 NDT INTERNATIONAL. DECEMBER 1984


the two alternative ways in which this was achieved. In the
first method, using a coincident laser generator and
detector, the surface was scanned in a raster fashion. On
each x-direction scan, ultrasonic waveforms changed
significantly whenever the laser spots were above any part
A
of the subsurface flaw. If the line of scan was centred
above the flaw as shown in Figure 6, a sequence of elastic
C
waveforms was recorded, examples of which are shown in
Figure 7 where the x-origin is arbitrarily defined. With
successive laser shots separated spatially by a nominal
1 mm, significant modulation, as discussed earlier, was
seen in the rangex = 0,96 mm tox = 5.76 mm. It was easy
2.65 MHz to conclude that the diameter of the subsurface flaw was
between 4.8 mm and 6.7 mm, in good agreement with the
actual length of 6.35 mm.

Fig. 5
0 5 10

Frequency (MHz)

Fast Fourier transform of waveform in Figure 2b, showing the


15

frequency at which longitudinal elastic pulses repetitively travel across the


flawed region
20

~ nm x = 0

I i ~ n m
x = 0.96 mm

Coincident laser
• ,± generator and
, ~ ' detector of I 1 cm I
I elastic pulses / =: -- I /

"[ I Le.rgeneroro'l / "'/ I


I ""'v'' x = 1.92 mm
Direction of scan,x ~ I Direction of scan,x I
a b

Fig. 6 Two experimental arrangements for scanning a subsurface flaw: ~5


a - - coincident laser source and detector; b - - laser source and receiver a
fixed distance apart

x = 4.80 mm
transient force consists of step motions at time intervals
corresponding to the round-trip transit time of a long-
itudinal pulse. Likewise, the flawed region can be
considered to be a plate with elastic behaviour. Hence
Ill
h = ATCl _ Cl (2)
2 2Vs
x = 5.76 rnm
where AT is the time interval between successive long-
itudinal pulse arrivals on the top surface, cl is the
longitudinal velocity and v s = 1~AT. From Figure 5, nm

Vs = (2.65 +-- 0.1) MHz x = 6.72 mrn

from which h was evaluated as


h = 0.20 --+ 0.04) mm
~ ~ I lOnrn
This was in excellent agreement with measurements using x = 7.68 mm
calipers of
I I I I
h = (1.22 ___ 0.02) mm 0 50 100 150 200
These results show that it is possible using laser-based
Time (/zs)
remote flaw detection systems to collect quantifiable
information about the flaw from single shot measure- Fig. 7 Displacement waveforms obtained from a line scan across a
ments taken above the flawed region. flawed region having a physical diameter of 6.35 mm (lying 1.22 mrn
below the surface). Incident laser energy was 36 mJ in a diameter of
More detailed information about the extent of the flaw has ~ 3 rnm. Firing of the laser occurred at the same time as the initial rising
been obtained from scanning techniques. Figure 6 shows edge of the waveforrn

NDT I N T E R N A T I O N A L . DECEMBER 1 9 8 4 333


approached, the Rayleigh pulse became distorted due to
interaction with the flaw, which again was 1.22 m m below
20 nm
the surface. The physics of the interaction leading to pulse
distortion is not well understood. When the scan had
passed beyond the flawed region, the typical Rayleigh
pulse returned. Other experiments showed that distortion
of the Rayleigh pulse can occur even for cases where the
depth of the sublaminar flaw was 4.8 mm. The ex-
perimental trace observed over the centre of the defect
(x = 5.76 mm, Figure 8), showed evidence of a low
I 20 nm
frequency oscillatory phenomenon at "-200 kHz. This may
well be related to the flexural resonance mode of the plate
defect discussed earlier (Figure 4b).
We may therefore conclude that laser-generated Rayleigh
pulses offer an alternative way of detecting subsurface
flaws. However, without a well developed theoretical
model, it is not possible to analyse experimental
I waveforms to deduce flaw characteristics. This is in
contrast to the first technique involving a coincident laser
source and laser detector, which offers a determination of
the depth of the fl~w below the surface, as well as its spatial
extent.

Conclusion
E = ~ I 20 nm
8 We have shown that a two-laser system can be used for
remote characterization of flat-bottomed holes, acting as
subsurface flaws within an aluminium test sample. A
pulsed Nd:YAG laser system was used to generate the
ultrasonic source whilst a He-Ne laser interferometer
detected subsequent surface displacements.
With both lasers coincident on the metal's surface, the
I depth of flaw was determined by measuring the round-trip
transit time of a compressional wave travelling repetitively
between the metal surface and the subsurface flaw. The
flaw also produced a characteristic resonant frequency
related to a flexural mode of vibration. Its area was
estimated using a formula based on circular symmetry.
For better definition of its spatial extent, the sample's
surface was scanned. Spatial resolution better than
20 nm ___ 1 m m was recorded for a flaw 1.22 m m deep, having an
aspect ratio o f " 5 .
Another technique used separated laser beams on the
sample. Distortion of any Rayleigh pulse formed by the
pulsed laser determined the presence of a subsurface flaw.
I I I I However, it was not possible from these measurements to
2.5 5.0 7.5 10 describe any features of the flaw, since the physics of such
ultrasonic interaction has not yet been developed.
Time (/as)
These results show that quantitative information about a
Fig. 8 Ultrasonic waveforms obtained from a line scan across a flawed
region which has a diameter of 6 . 3 5 mm (lying 1.22 mm below the
subsurface flaw can be obtained from a laser-ultrasonic
surface). Incident laser energy was 1 3 mJ with the receiver placed 1 cm source. Unfortunately, laser detection has required the use
away from the source. The laser was fired at time t -- 0 s of a polished metal surface to reflect sufficient light. This
is normally impractical in an industrial implementation,
and further work is required to improve the sensitivity of
An alternative method for scanning the surface is shown the laser detector, which is presently known to be less
in Figure 6b. Instead of detection immediately above the sensitive than most other types of detector.
laser source, the source and receiver were separated so
that, with a fixed separation, they scanned on either side of Acknowledgements
the sublaminar flaw. A thin layer of oil was used at the
laser source position to enhance the Rayleigh wave We should like to thank B. Moss for his technical support
amplitude. With the x-axis set at an arbitrary origin, the during these collaborative experiments. The work was
flaw was scanned with the target moving over nominal supported by the Metrology and Standards Requirement
2 m m spatial intervals between successive laser shots. Board of the Department of Trade and Industry.
Without any flaw in direct line between laser source and
laser receiver, the surface pulse was that shown at the top References
of Figure 8. It consisted of a fast pulse of a longitudinal I Hutchins,D.A., Dewhurst,R.J., Palmer,S.B. and Scrub),,C.B.
nature followed by a larger Rayleigh pulse. This waveform 'Laser generationas a standard acousticsourcein metals'Appl
has been described in detail elsewhere["l. As the flaw was Phys Lett 38 (1981) pp 677-679

334 NDT INTERNATIONAL. DECEMBER 1984


2 Tam, A.C. and Coufal, H. 'Photoacoustic generation and 10 Drain, LE., Speake, J.H. and Moss, B.C. 'Displacement and
detection of l0 ns acoustic pulses in solids' Appl Phys Lett 42 vibration measurement by laser interferometry' SPIE Vol 136
(1983) pp 33-35 (1977) pp 52-57
3 Ledbetter, H.M. and Moulder, J.C. "Laser-induced Rayleigh 11 Morse, P.M. "Vibration- and sound' McGraw-Hill (1936) p
waves in aluminium'JAcoust Soc Am 65 (1979) pp 840-842 175
4 Scruby, C.B., Dewhurst, R.J., Hutehins, D.A. and Palmer, S.B. 12 Pao, Y.H., Gajewski, R.I~ and Ceranoglu, A.N. "Acoustic
'Quantitative studies of thermally-generated elastic waves in emission and transient waves in an elastic plate'JAcoustSoc.4m
laser-irradiated metals" JAppl Phys 51 (1980) pp 6210-6216 65 (1979) pp 96-105
5 Aindow,A.M., Dewhurst, R.J., Hutchins, D.A. and Palmer, S.B. 13 Scruby, C.B., Dewhurst, R.J., Hutehius, D.A. and Palmer, S.B.
"An investigation into laser-generated ultrasonic pulses at free 'Research Techniques in ND'V edited by R.S. Sharpe, Academic
metal surfaces"JAcoust Soc Am 69 (1981) pp 449-455 Press Vol 5 (1982) pp 281-327
6 Dewhurst, R.J., Hutchins, D.A., Palmer, S.B. and Scruby, C.B.
'Quantitative measurements of laser-generated acoustic wave-
forms" JAppl Phys 53 (1982) pp 4064-4071
7 Bondarenko, A.N., Drobut, Yu.B. and Kruglov, S.V. 'Optical
excitation and detection of nanosecond acoustic pulses in
nondestructive testing" Soy JNDT 12 (1976) pp 655-658 Authors
8 Calder, C.A. and Wilcox, W.W. 'Non-contact material testing
using laser energy deposition and interferometry'MaterEva138 A.M. Aindow, ILJ. D e w h u r s t a n d S.B. P a l m e r are i n the
(1980) pp 86-91 D e p a r t m e n t o f A p p l i e d Physics, University of H u l l H u l l
9 Wellman, R.L 'Laser system for the detection of flaws in solids" HU6 7RX, UK. C.B. Scruby is i n the Materials Physics a n d
Harry Diamond Laboratories, Report No HDL-TR-1802 (1980) pp Metallurgy Division, A E R E Harwell, O X l l 0RA, UK.
1-30

Paper received 23 July 1984. Revised 28 September 1984

NDT INTERNATIONAL. DECEMBER 1984 335

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