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This Application Note details the photometric determination of zinc sulfate using
the Optrode (610 nm). Complexometric titration of zinc requires an EDTA titrant
and Eriochrome Black T as indicator. The method fully complies with Ph. Eur.
and USP.
Method description
Sample Parameters
Zinc sulfate Titration mode MET U
Measurement drift 50 mV/min
Sample preparation Min. waiting time 0s
Analysis
Weigh approx. 0.150 g sample into a beaker and
dissolve in 100 mL dist. H2O. Add 5 mL buffer solution
and 0.15 mL Eriochrome Black T indicator and titrate
with c(Na2EDTA) = 0.1 mol/L past the first endpoint.
Titration Application Note T–90
Version 1