Académique Documents
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OF GEOPttYSICAL
RESEARCtt VOL. 73, No. 14, 3UL¾15, 1968
JAMES D. BYERLEE
The deformationalcharacteristics
of two limestones,
one gabbro,and one dunirehave been
investigated as a function of confining pressure.It was found that friction of these rocks and
friction of granite and serpentinitestudiedelsewhereare nearly identical and that the brittle-
ductile transitionpressureis simply the pressureat which the stressrequiredto form a fault
is equal to the stressrequiredto causeslidingon the fault. The transitionpressureis higher
in extension than it is in compression.This difference occursbecausethe frictional shear stress
requiredto causeslidingis determinednot by confiningpressurebut by the principalstresses
and the angleof the fault. For the samefrictionalshearstresson a fault surface,the con-
fining pressureis muchhigher in extensionthan it is in compression.
Av. Grain
Diameter,
Rock Density Porosity mm Modal Analysis*
that the effective confining pressure on the cell outside the pressurevessel.Strain rate of
sample becomeszero. The other reason is that 2.4 X 10-•/see was maintained constant
most investigations have been made to deter- throughout the experiments. Axial displace-
mine the stressat faulting, and, when faulting ment of the piston was measuredwith a San-
occurs, the experiments are terminated. born DCDT 500 transducer attached to the
The present investigationdeterminesfriction piston. The confiningpressurewas measured
for a number of rocks to determine whether, with a manganincoil situatedinsidethe pres-
as in granite,the brittle-ductiletransitionpres- sure vessel.To keep the pressureconstantas
sure is simply the pressureat which the stress the piston advancedinto the pressurevessel,
required to form a fault is equal to the stress the volumeof the hydraulicsystemwas kept
required to cause sliding on the fault. constant.This was done by automatic switch-
ing of an electric motor that advancedor with-
EXPERIMENTAL METHOD
drew a pistonfrom an auxiliary pressurevessel
Differential stress was measured as a func- connectedhydraulicallyto the main pressure
tion of strain for four rocks at room tempera- vessel. The direction of the motor was con-
ture and at confining pressuresup to about trolled by a logic discriminator circuit,which
5 kb. Porosity, grain size, and modal analysis
I i I
of the rocks studied are given in Table 1.
Preciselyground cylindersof the rocks, 3.8 cm
long and 1.58 cm in diameter,were jacketed in
a gum rubber tube with a wall thickness of
3.17 mm. The ends were sealed with a wire
4.66
clamped to hardened steel end plugs. It was
found that after deformation the specimens
$,55
fell to pieceson removal of the rubber jacket.
To prevent this, a copper cylinder with a wall
/•2.20
thicknessof 0.13 mm was placedover the speci- -• - •- - --I,59
men before finally jacketing in rubber. This
copper cylinder gave the specimen a slight
mechanical strength, so that the rock stayed
intact and permitted accurate measurementof
the angle of the fault surface after completion
of an experiment. i I I i
_
• •2.o4 sectionalarea and length of the specimen.For
large strains, the true stressin the specimen
is different from the value shown because the
.2 •1,22
• ,81 -
area of the specimen supporting the load
changesduring deformation.The dashedlines
,6 in the figures indicate where deformation oc-
57 curredwith a suddenreleaseof elasticenergy.
In all other cases the deformation occurred
stably.
00 '
5 ,
IO ,
•5 20,
Stroin,(perceni) The differential stressat fracture, or at 5%
strain if the specimenwas ductile, is plotted
Fig. 2. Stress-strain curves for Solenhofen lime-
stone. Uncorrected for change in length or cross-
in Figure 5 for all the experiments.The sig-
sectional area. Numbers at the ends of the curves nificanceof the solid line in Figure 5 will be
are the confining pressures. explainedbelow.There is a changein the cross-
4744 JAMES D. BYERLEE
O0 5
-••,42
I0 15 2
the secondfault was calculated from the angle
of the fault and the axial displacement.This
distancewas found to be equal to the offset of
Strc]in,(percent)
the first fault. The angle that the faults made
Fig. 4. Stress-strain curves for Spruce Pine with the axis of the specimenincreasedwith
dunitc. Uncorrected for change in length or cross- an increasein confiningpressure,and near the
sectional area. Numbers at the end of the curves
brittle-ductile transition pressureit was about
are the confining pressures.
30øø
has been studiedin detail, and the resultswill are steepthan is requiredif they are inclined
be presentedin a later paper. at a lower angle.For a fixed configuration of
Figure 6 showsthat at low pressuresthe the surfaces in contact, the shear stress re-
frictional shear stressincreasesrapidly as nor- quiredto causeslidingin this mannerincreases
mal stressincreases.Beyond2 kb, the frictional linearly as normal stressincreases.A stage is
stressrises less rapidly and there is a nearly reached,however,at which it is easierto slide
linear relationshipbetween shear and normal by breakingthroughthe asperitiesthan by lift-
stress.Byeflee [1967a, b] studied the friction ing over them.In the caseof granite,this point
of granite in detail and gave the followingex- seems to occur at a normal stress of about 2
planation for the relationshipbetween shear kb, and, beyond this point, the increase in
and normal stress for sliding. At low normal frictional shear stress with normal stress repre-
stresses,surfacesmay slide by lifting over the sents the change in strength of the material
irregularities on the surfaces.The shear stress with pressure.At normalstresses •etweenabout
required to do this is determinedby the angle 100 bars and 2 kb, the behavior is transitional.
made by the irregularities with the plane of That is, the most steeply inclined asperities
sliding. A larger shear stressis required to lift break, but the surfacesmay lift over the less
the surfacesover one another i,f the asperities steeply inclined ones. In this region there is
14 i i I I
12
10
•o•'•
•>/
ß ß -ß
• o/•**
o
øoj,,' ' oSolenhofen
Limestone
•./ •Oak Hall Limestone
/ "Nahant Gabbro
/ • SprucePine Dunile
• CabrarnurraSerpen•inite
(Ralel,
ghandPaterson,,
I 2 $ 4 ,5 6 ?
Confining
Pressure,
(kilobars)
Fig. 5. Differential stressversusconfiningpressureat fracture or 5% strain if the specimen
wasductile.Opensymbolsindicatebrittle behavior;closedsymbols,ductile.Solidline is the
boundarybetweenthe brittle and ductileregionsdeterminedfrom frictiondata (Figure6).
4746 JAMES D. BYERLEE
6 i i i i i i i
o Solenhofen Limestone
• Oak Hall Limestone
[] Nahant 6'(]bbro _
72
[o oøoo o// • ß _ the angle is •bout 20ø. With this value the
p: o',•d- 2.75r
The transformationwas made numerically,and
a oo/
.' '
: . .. ß
' - the result is plotted as a solid line in Figure 9.
• •/I • - ß This line shouldmark the boundary between
brittle and ductile behavior in extension. The
open symbols in the figure represent brittle
oo ', k I k behavior; the solid symbols,ductile behavior.
The circles were plotted from the data pub-
Confin;ng Pressure (kilobors)
lishedby Heard [1960']; the triangles,from the
Fig. 8. Differen•i81 s•ressversus confiningpres-
sure for carbonate rocks [from Mos•, 1966]. Solid data publishedby Handin et al. [19'6.7].The
line is the bounds• between •he bri•fie 8rid brittle-ductile transition takes place at a pres-
ductile regions de•e•ined from friction dstmsure slightly below the predicted value, ,but,
Dsshed Hne is •he friction bounds• suggestedby considering the uncertainties in the strength,
Mogi. Open symbols indicste bri•le behavior;
h81f closedsymbols,•rsnsi•ion81; closedsymbols,
friction, and fault angle,the transition pressure
ductile. in extensionis consistentwith the friction hy-
pothesis.
the transition pressurefor both the silicates It may well be argued that the intermediate
and the carbonates falls close to this line. The stressmay have an effecton friction, but Byef-
frictional hypothesisseems,therefore, to be lee (1967a and more recent unpublished re-
generallytrue for mostrocktypes.Moqi [1900] suits) has shownthat, for granite in compres-
found that the transition pressurefor shale is sion, the frictional, shear stress at any given
very much higher, but this higher pressure normal stressis the same for sliding surfaces
seems to occur because the frictional shear inclined at 30 ø and 45 ø to the axis of the
stressrequired to causesliding on surfacesof specimen. For example, at a normal stress of
shale at any given normal stressis very much 8 kb, the shear stressrequired to causesliding
lower than it is for other rocks [Maurer, 190.5]. on surfaces of granite is 5.3 kb for both 30ø
For the weaker silicatesin Figure 7, the transi- and 45 ø. In both cases the intermediate stress
tion pressureseemsto be slightly higher than is the confiningpressureP. If the angle is 45ø,
the value predicted. The transition pressureis P is 2.7 kb, but it is 4.94 kb if the angle is 30ø.
also slightly higher for porous tuffs; it would This indicates that within the experimental
be of interest to find out whether this relation error, the intermediate stress has no effect on
friction.
occurs becausethis rock type has lower fric-
tion than other rocks. One question that still remains unanswered
Heard [1900'] has found that the britfie- is what determinesthe stressa rock will sup-
ductile transition pressureis very much higher port at any given confining pressure. There
in extensionthan it is in compression.Before it is at presentno satisfactorytheory to predict
can be determined whether the friction hy- the stress required to form a fault surface in
pothesis is valid for extension, friction must rocks in the brittle region [Brace and Byeflee,
first be convertedinto this new coordinatesys- 1967]. In the ductile region,it is also not clear
tem. In extension just what determinesthe stressthat a rock will
support.In somerocks,particularlylimestones,
plastic deformation of the individual crystals
may occur during deformation; for fully plastic
2c• materials,
theyieldstress-and-strain
hardening
BRITTLE-DUCTILE TRANSITION IN ROCKS 4749
o Heard
"Handin el'. [1967)
i I
o 2 4 6 8 10
Confining
Pressure,
[kilobars}
Fig. 9. Differential stressversusconfiningpressureat fracture or 5% strain for 8olenhofen
limestone in extension. Solid line is the boundary between the brittle and ductile regions
determinedfrom friction data. Open symbolsindicate brittle behavior; closedsymbols,ductile.
rate is almost independentof confiningpres- room temperature and at strain rates of 2.4 X
sure. These effectsare illustratedby the work 10-4/sec.Recent unpublishedresultsfor granite
of Paterson[1964]. I-Ie showedthat, for copper, show that, withim the experimentalerror, fric-
the stress-straincurve at a pressureof 8 kb tion is not different at strain rates of 2.4 X
does not differ by more than a few per cent 10-6/secand 2.4 X 10-4/see.The effectof strain
from the curveat atmosphericpressure.This is rate on the fricti.on of other rock types remains
clearly not true for limestone.Figures '1 and 2 to be determined, however, high temperature
show that the strain strengtheningrate in- and chemical environment may also have an
creasesremarkzbly with confiningpressure. effect on .friction, and this possibility should
Cataclasis(that is crushingof the grains) be investigated.
may be the controllingmechanismof deforma- The present work shows that the 'brittle-
tion at room temperature over the confining ductile transition pressure in rocks at room
pressurerange investigated.At present, how- temperature both in compressionand in exten-
ever, there is no theory that can be used to sion is the pressure at which the stress re-
predict either the stressrequired to deform a quired to form a fault surfaceis equal to the
rock in this manner or the effect confiningpres- stressrequired to causesliding on the fault.
sure should have on the strain strengthening Acknowledgments. The researchfacilities at the
rate. Clearly the problemrequiresfurther work. MassachusettsInstitute of Technology were made
The present experimentswere performed at available through the courtesy of Professor W. F.
4750 JAMES D. BYERLEE
Brace. Professor Brace, Drs. L. Peselnick, C. B. failure of limestone,dolomite, and glassat differ-
Raleigh,and E. C. Robertsonread the manuscript ent temperaturesand strain rates, J. Geophys.
and suggesteda number of improvements. Res., 72(2), 611-640, 1957.
The investigation, which was carried out at the Handin, J., and D. W. Stearns,Sliding friction of
Department of Geology and Geophysics,Massa- rock (abstract) Trans. Am. Geophys. Union,
chusettsInstitute of Technology,was supportedby 45 (1), 103, 1964.
Air Force Cambridge Research Laboratories, Of- Heard, H. C., Transition from brittle fracture to
fice of Aerospace Research, U.S. Air Force, Bed- ductile flow in Solenhofen limestone as a func-
ford, Massachusetts,under contract AF 19(628)- tion of temperature,confiningpressure,and in-
3298.Publication authorizedby the Director, U.S. terstitial fluid pressure,
Rock Deformation,Geol.
Geological Survey. $oc. Am. Mere., 79, 193-226, 1960.
Maurer, W. C., Shear failure of rock under com-
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Byerlee, J. D., Frictional characteristicsof granite Raleigh,C. B., and M. S. Paterson,Experimental
under high confining pressure,J. Geophys.Res., deformation of serpentiniteand its tectonic im-
72(14), 3639-3648, 1967a. plications,J. Geophys.Res. 70(16), 3965-3925,
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Handin, J., H. C. Heard, and J. M. Magouirk,
Effect of the intermediate principal stresson the (Received December 29, 1967.)