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Rock Characterisation, Modelling and Engineering Design Methods – Feng, Hudson & Tan (Eds)

© 2013 Taylor & Francis Group, London, ISBN 978-1-138-00057-5

Experimental study on creep behavior of sandstone with pore water


pressure and its constitutive modeling

Y.J. Cao, W. Wang, J. Lü, T.G. Liu & Z. Zheng


Key Laboratory of Ministry of Education for Geomechanics and Embankment Engineering, Hohai University,
Nanjing, China
Geotechnical Research Institute, Hohai University, Nanjing, China

ABSTRACT: An experimental study is conducted on sandstone under different confining and pore pressures
through triaxial creep tests The creep properties of sandstone under different conditions are compared and
analyzed The test results show that: in the case of same confining pressure, pore pressure can increase the
instantaneous elastic deformation and creep deformation but reduce the strength of sandstone. Furthermore,
confining pressure has an impact on creep deformation while maintaining a constant pore pressure. Based on
the classical creep model and the application of effective stress theory, a new nonlinear viscoelasto-plastic
rheological model for sandstone is established, which can reflect the effect of pore pressure on creep properties
and induced damage in the process of creep. The comparison between the results obtained from the modeling and
those from the experiments shows that this model can describe well primary attenuation creep, steady creep and
accelerated creep, and a good accord is obtained.

1 INTRODUCTION a rock-fluid interaction resulting in a negative influ-


ence on the long-term stabilities of engineering. How-
Rheology is the inherent nature of rock material; espe- ever, the coupled effect of creep and pore pressure is
cially most of the engineering rock masses are in rarely considered for studying the rheological proper-
the generalized rheological deformation (Wang & Li ties of rock.Yan et al. (2010) compared the rheological
2008). Engineering practices show that rock defor- properties of porous limestone through triaxial creep
mation increases with time under a long-termed load experiment conducted under different water pressures
leading to cracks or even failure on structures. Jun and deviatoric stresses. She et al. (2010) designed three
(2007) has systematically summarized the progress types of load modes in which a high pore pressure
in rheological mechanics and its engineering applica- is applied to study the influence of pore pressure on
tion in recent years. However, most of these researches creep properties of marble. However, few experimen-
focused on the effect of stress field on the rheological tal studies on rock creep are carried out under different
properties. In fact, the mechanical properties become confining pressures and pore pressures.
more and more complicated with the diversification In this study, we investigated the water-weakening
of structure form and the expansion of construction effect on the rheological properties of rock as a func-
scale in rock engineering. At the same time, engi- tion of both confining pressure and pore pressure by
neering activities, geological effect and the change comparing the experimental data with those obtained
of environment have a direct or indirect effect on the from the tests without pore pressure. Furthermore, a
long-term stability of rock engineering. Experiments new nonlinear viscoelasto-plastic rheological model
and engineering researches have shown that water has based on the concept of effective stress is presented
important effect on rock rheological properties. in order to describe the effect of pore water pressure
Recently, a large number of experimental results on porous rock and the damage caused by water in
reported in the literature were obtained from the tests the process of rock creep. Experiments results will be
carried out under different water contents. (Li & Zhu compared with the results predicted by the new model
et al. 2003, Zhu & Ye 2002, Yang & Xu et al. 2006). introduced in this study.
As have been pointed out by these experiments, rock
creep properties with certain water content are more
significant than those in air-dry state, and tend to
reduce the strength of rock through the physical and 2 EXPERIMENTAL STUDY AND RESULTS
chemical effects. Actually, the properties of rock mass
in engineering such as tunnels and underground oil 2.1 Tested material and equipment
storage are not only affected by the surrounding rock This study is performed on sandstone taken from
stress, but also related to pore pressure which allows a hydropower dam foundation, and the material is

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2.2 Experimental methodology
Prior to performing creep tests, the rock specimens
were saturated. A series of conventional triaxial com-
pression tests for saturated sandstone samples were
carried out to determine the short-term strength and
deformation behavior under different confining pres-
sures (σ3 = 2 MPa and 6 MPa) and pore pressures
(p = 0 MPa, and 0.5 MPa). After, a series of multiple-
step triaxial creep tests were performed under the same
stress (σ3 and p) conditions at a constant temperature
and humidity so that we can investigated the coupled
effect of confining and pore pressures on creep prop-
erties of sandstone. The creep experiment procedures
were described as follows:
1. The saturated sample in the test chamber with two
linear variable displacement transducer sensors was
installed.
2. When the sample was installed, confining pressure
Figure 1. Samples of sandstone. was increased to a predefined value and then kept
constant for about 24 hours.
3. After that, pore pressure was applied to a prede-
fined pressure, then deviatoric stress was applied
at a rate of 0.1 cm3 /min in a stepwise manner to a
predefined pressure. When the rock samples were
loaded to the first stress level, the axial devia-
toric stress was kept constant for 48 hours while
recording the deformation of rock samples, the con-
fining pressure and stress as functions of time by
an automatic data collection system.
4. After the first stress level for the creep test, the rock
samples were gradually tested under the second,
third. . . . according to previous method until the
accelerated creep damage occurred at the last stress.

2.3 Experimental results and analysis


Figure 2. Rock servo-controlled triaxial rheology system Typical triaxial experimental creep results of sandstone
developed by Laboratory of Mechanics in Lille in France, are shown in Fig. 3. In this section, variation of axial
University of Sciences and Technology of Lille in France and strains in the samples under various stress levels is
Hohai University in China.
analyzed as function of time.
As shown in Fig. 3, when σ3 = 2 MPa and p =
0 MPa, the experiment was conducted at different
a relatively homogeneous quartz-sandstone which is stress levels: 11.4 MPa, 15.2 MPa and 19 MPa, result-
considered as an isotropic rock. The density of sand- ing in instantaneous elastic deformation of 3.8 µε,
stone is 2200 kg/m3 with an average porosity of 0.83 µε and 0.87 µε. The data shows that the instan-
17.34%. Thus it has a good permeability. The sand- taneous elastic deformation depended strongly and
stone was cored from the situ rock mass and re- nonlinearly on deviatoric stress, and the deformation
machined along the direction of stratification in the increased with the increase of stress. Further, when the
laboratory. All tested samples were cylindrical with a pore pressure reached to 0.5 MPa, the elastic defor-
length of 100 mm and a diameter of 50 mm (Fig. 1). mation in the primary creep phase was much higher
Creep tests were conducted on the equipment than the deformation performed without the pore pres-
named Rock servo-controlled triaxial rheological sys- sure under the same confining pressure (σ3 = 2 MPa).
tem (RCT) developed by Laboratory of Mechanics It was clear to notice that pore pressure has an obvi-
in Lille (LML, CNRS), University of Sciences and ous effect on the instantaneous elastic deformation and
Technology of Lille in France and Hohai University in can reduce the elastic modulus of sandstone. More-
China. The equipment is made up of loading system, over, creep experiments were conducted at a fixed
constant-stability pressure equipment, hydraulic pres- confining pressure of 2 MPa, but with deviatoric stress
sure transfer system, pressure chamber equipment, of 11.4 MPa and 15.2 MPa. The corresponding creep
water pressure system and automatic data collec- deformation conducted by the tests at a p of 0.5 MPa is
tion system (Fig. 2). And test data can be collected 158% and 183% more than that at a p of 0 MPa. This
automatically. suggests that the existence of the pore water pressure

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Figure 4. Primary deformation and structural deformation
of porous media.

the concept of effective stress can be used to consider


the influence of pore water pressure on creep deforma-
tion. The sandstone can roughly be considered as an
assembly of solid grains with different kinds of con-
tact surfaces and a connected macroscopic porosity.
According to the study of Li & Kong et al. (1999), there
Figure 3. Axial strain-time relation curves under differ- are two kinds of deformation mechanism occurred
ent confining pressures and pore pressures at various stress in porous media: firstly, the overall deformation is
levels. only caused by the deformation of framework grains,
known as the primary deformation (Fig. 4a); Secondly,
increases the axial strain of sandstone. It is because the overall deformation is generated by the change of
that water molecules get into the specimen and weaken spatial structure in the particles of medium skeleton
the links between the rock grains and the phenomenon such as the relative displacement produced between
of compaction softening tends to occur. On the other skeletal particles, known as the structural deformation
hand, water molecules play a role in dissolving the min- (Fig. 4b).
eral grains and reducing the friction coefficient, which Porous media will produce instantaneous recov-
is regarded as a potential source of strength reduction erable elastic-strain response (primary deformation
in sandstones where a friction reduction of about 10 and viscous strain response (structural deformation)
percent has been derived by comparing experimen- derived from the adjustment of relative displacement
tal strength data and results from a micromechanical under the action of external force. At this moment,
model (Baud et al. 2000). When maintaining a constant porous medium is considered as a dual medium body,
pore pressure of 0.5 MPa, the primary elastic deforma- and its deformation mechanism presents the couple
tion of the sandstone at a σ3 of 6 MPa were 52% lower effect of primary deformation and structural deforma-
than that at a σ3 of 2 MPa at the same stress level. In tion as the characteristics of double effective stress. As
addition, the higher confining pressure is, the smaller reported by Li & Kong (1999), the primary effective
corresponding creep deformation is. So we can con- stress and structural effective stress can be calculated
clude that confining pressure has a negative effect on by the following formula:
creep deformation at the same stress level. 1) The primary effective stress,

3 RHEOLOGICAL MODEL STUDY


p
where σeff defines as the primary effective stress;
From the strain-time curves shown in Fig. 3, it can be φ is the porosity; p is pore pressure. The primary
seen that the axial strains under the failure deviatoric effective stress depends on the elastic strain of
stress level undergo three stages: attenuation creep, media.
steady-state creep and accelerated creep. In order to
model the creep behavior of rocks, a lot of creep mod-
els have been proposed (Cao et al. 2002, Xu & Yang 2) The structural effective stress,
2006 and She et al. 2009). These models can enrich
rheological theories of rock to some extent while they
are difficult to describe the rheological behavior of s
porous media subjected to pore water pressure. Fur- where σeff represents the structural effective stress;
thermore, the induced damage during the process of φc is connected porosity involved with cement-
creep cannot be taken into account. In this part, consid- ing properties of porous media. And the structural
ering the mechanism of pore deformation, we propose effective stress determines the rate of viscous strain.
a new nonlinear creep model based on the conventional
Nishihara model and the application of effective stress.
A pressurized pore fluid acts to reduce the applied
3.1 The double effective stress normal stresses and thus allows the lower effective
stresses undertaken by internal skeleton. It can be
Rheology of porous media is a very complicated pro- studied from the previous analysis of double effective
cess. For the creep behavior of viscoelastic materials, stress which is able to take the water-weaken effect

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Figure 5. Damage deformation of porous media.

into account during the creep course of sandstone.


Elastic modulus and peak strength will be weakened
by the behavior of damage due to the fact that the
known effects of water on rheological behavior of
rocks are usually decomposed into physical effects of
pore water pressure and chemical effects (Paterson &
Wong 2005). In case of mechanical damage, there are
a lot of tensile microscopic cracks, the “wedge” effect
caused by the pore water pressure will lead to water
access into the progressive crack tips due to damage,
and in this way the development and propagation of
cracks are improved. Therefore, tertiary creep (accel-
erating strain as failure is approached) corresponds to
an increase in crack growth rate due to crack interac-
tions. In case of chemical effects, chemical reaction
with water and hydrophilic minerals will attack crys-
talline matrix of sandstone resulting in the damage
of microstructure. From the above, this behavior of
damage can be expressed as grain rupturing and crack
propagating (Fig. 5). In view of porous media this
behavior can be described by the damage porosity.
Based on the study of Hai et al. (2010), the damage
effective stresses can be expressed as follows: Figure 6. Typical creep curve of sandstone.

Figure 7. The modified Nishihara model.

b generalized Kelvin component is useful to describe


where σeff represents the damage effective stress; φ is
the original porosity and φb is the damage porosity, h the structural deformation of rocks. But the classical
is defined as a parameter reflecting crack closure. If Nishihara model is difficult to describe the acceler-
σ > 0, we have h = 1; if σ < 0, we have 0 ≤ h < 1. D is ated creep of rocks. Therefore, a nonlinear viscoplastic
the damage variable between 0 and 1. The parameter εb component can be introduced to describe the strain rate
controls the plastic strain caused by damage depending change of accelerated creep. The viscoplastic compo-
on the damaging effective stress. nent only works as the accelerated creep happens. The
strain-time relation under constant stress is expressed
3.2 Formation of the constitutive model by Eq. 9. The modified Nishihara model is illustrated
in Fig. 7.
Fig. 6 is a typical creep curve of sandstone revealing
an obvious three-stage creep. The primary creep stage
AB is characterized by a rapidly attenuated creep strain
rate to reach a steady creep stage BC, then the ter-
tiary creep stage CD is characterized by an accelerated
strain for a period of time until failure of rock. where σ is the stress, σs is the long-term strength. A
By considering the deformation mechanism of and η3 are the material coefficients, tc is the starting
rock, a Hook elastic component can be introduced time of accelerated creep, ch(t) is the hyperbolic cosine
to describe the primary deformation of rocks, and a function.

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During the accelerated creep, damage deforma-
tion caused by water-rock interaction accumulates
rapidly. According to M.L. Kachanov (1986), damage
evolution law can be defined as:

In the formula, α and r are the material coefficients;


t is creep time; tc is the starting time of accelerating
creep. In this case, only the damage deformation in the
accelerated creep stage is considered. Therefore dam-
age deformation is zero before the accelerated stage.
Taking into account the influence of pore pressure and
damage, by use of equation (6) together with substitu-
tion of equation (9) into equation (5), the final effective
stress can be expressed in the form:

According to the previous analysis, the total creep


strain can be written by:

The strain εe , εve and εb are determined respectively


by corresponding effective stress. Only the primary
and structural deformation occurs during the primary
and steady creep stages. It is assumed that a negligible
porosity caused by the primary and structural deforma-
tion varies a little due to the close-grained structure.
However, the damage porosity varies a lot when the
accelerated creep occurred because of progressive
damage caused by the water-weaken effect. The for-
mula (6) and (9) can reflect this change. Besides,
elastic modulus and viscosity coefficient vary with the
pore pressure and porosity (Wei et al., 2011), that is:

The constitutive relationship of the modified


Nishihara model is deduced as follows:

Figure 8. Comparison between results of modified damage


Nishihara model and experimental results.

creep phase occurs, the creep curve will be divided


into two parts based on the starting time of acceler-
ated creep. The first part (t < tc ) is the curve before
3.3 Parameter identification and verification
the accelerated creep stage; and the second part is the
According to the study, when the stress level is less than one (t ≥ tc ) that the rock steps into its accelerated creep
the long-term strength, the accelerated creep phase stage. First, we can use the data when t < tc to fit the
will never occur, so the modified Nishihara model material parameters E0 , E1 , E2 , η1 and η2 which con-
will degenerate into the generalized Kelvin model. The trol the attenuating and steady creep. Then the values
formula (10) when t < tc can be applied directly. The for E0 , E1 , E2 , η1 and η2 are fixed, and the data (when
fitting result is given in Fig. 8(a). When the accelerated t ≥ tc ) will be used to fit the parameters A, r, α and

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Table 1. Parameters of modified damage Nishihara model.

σ1 –σ3 σ3 ρ E0 E1 E2 η1 η2 η3
/MPa /MPa /MPa /GPa /GPa /GPa /GP · h /GP · h /GP · h A α r

11.4 2 0 2.91 74.25 68.34 1216.8 307.8 – – – –


11.4 2 0.5 2.35 70 50 1229.5 1040.5 – – – –
11.4 6 0.5 4.72 74.41 129.3 749 31.49 – – – –
19 2 0.5 2.29 184 5.6 5.4 4.4 24.4 0.0058 12 49
33.6 6 0.5 3.94 188.5 5.4 1.43 50 113 0.0014 1.2 25.24

η3 which control the accelerated creep. All the param- Hai L., Liang B. & Shui, S.M. 2010. Damaging effec-
eters will be identified from the fitting results shown tive stresses of porous media. Mechanics in Engineering,
in Fig. 8(b) and Fig.8(c), and the Tab. 1 presents the 32(1):29–32.
values of parameters. It is noted that the elastic param- Kachanov, M.L. 1986. Introduction to continuum damage
mechanics. Russia: Martinus Nijhoff publishers, 22–36.
eters E0 , E1 , E2 decrease with pore pressure under Li, C.L., Kong, X.Y. & Xu, X.Z. et al., 1999. Double effective
the same stress. The simulation results by using the stresses of porous media. Nature Magazine, 21(5):288–
modified Nishihara model agrees well with the test 292.
results. The proposed model can show the influence of Li,Y., Zhu, W.S. & Bai, S.W. et al. 2003. Uniaxial experimen-
pore pressure on rock creep deformation and describe tal study on rheological properties of granite in air-dried
accurately the accelerated creep. and saturated states. Chinese Journal of Rock Mechanics
and Engineering, 22(10):1673–1677.
Paterson, M.S. & Wong, T.-F. 2005. Experimental Rock
4 CONCLUSIONS Deformation—The Brittle Field, Springer Verlag, Berlin.
She, C.X. 2009. Research on nonlinear viscoelasto-plastic
creep model of rock. Chinese Journal of Rock Mechanics
In this study, the results of triaxial creep tests on sand- and Engineering, 28(10):2006–2011.
stone are presented in order to investigate the creep She, C.X., Cui, X., 2010. Influence of High Pore Water
behavior and its sensitivity to pore pressure as well Pressure on Creep Properties of Rock. Chinese Journal
as confining pressure and deviatoric stress. The anal- of Rock Mechanics and Engineering, 29(8):1603–1609.
ysis show that the existence of the creep deformation Sun, J., 2007. Rock rheological mechanics and its advance
of sandstone increases with pore water pressure while in engineering applications. Chinese Journal of Rock
limited by a high confining pressure. It is also shown in Mechanics and Engineering, 26(6):1081–1106.
the proposed model that the damage caused by water- Tang, L.S., Zhang, P.C. & Wang,Y., 2004. On fracture of rocks
weaken effect has influence on the creep deformation. with cracks under water action. Chinese Journal of Rock
Mechanics and Engineering, 2004, 23(19): 3337–3341.
The comparison between the results obtained from the Wang, Z.Y & Li, Y. P., 2008. Rock rheological theory and
modeling and the experiments shows that this model numerical simulation. Beijing: Science Press.
can well describe the primary attenuation creep, the Wei, J. & Wang Y.Y. et al., 2011. Mathematical model of
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ACKNOWLEDGEMENTS Xu, W.Y.,Yang, S.Q & Chu, W.J. 2006. Nonlinear viscoelasto-
plastic rheological model (Hohai model) of rock and
The work was supported by the National Sci- its engineering application. Chinese Journal of Rock
Mechanics and Engineering, 25(3):433–447.
ence Foundation of China (Grant no. 51109069, Yan, Y., Wang S.J. & Wang E.Z. 2010. Creep equation of
11272114, 11172090) and National Program on Key variable parameters based on Nishihara model. Rock and
Basic Research Project (973 Program) (Grant no. Soil Mechanics, 31(10): 3025–3035.
2011CB013504). Yang, S.Q., Xu, W.Y. & Xie, S.Y. et al. 2006. Studies on triax-
ial rheological deformation and failure mechanism of hard
rock in saturated state. Chinese Journal of Geotechnical
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