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1. PROJECT INTRODUCTION
As the title “Analysis of Heat Treatment and effect of Carbon Percentage in Metal Structure”
suggests this project is to understand the effect of heat treatment technique and carbon
content on the metal properties and structure. Here we shall also analyze the process of heat
The heat treatment includes heating and cooling operations or the sequence of two or more
such operations applied to any material in order to modify its metallurgical structure and alter
Heat Treatment is a technique of controlled heating and cooling of metals to alter their
Heat Treatment is often associated with increasing the strength of material, but it can also be
formability, restore ductility after a cold working operation. Steels are heat treated for one of
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Softening: Softening is done jto reduce strength of hardness, remove residual stresses,
improve toughness, restore dutility, refine grain size or change the electromagnetic
Hardening: Hardening of steels is done to increase the strength and wear properties.
A Annealing
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Annealing is performed primarily for homogenization, recrystallization or relief of residual
stress in typical cold worked or welded components.Few important variants of annealing are
followings.
Full annealing process consists of three steps. First step is heating the steel component to
above A3 (upper critical temperature for ferrite) temperature for hypoeutectoid steels and
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above A1 (lower critical temperature) temperature for hypereutectoid steels by 30-50 C.
The second step is holding the steel component at this temperature for a definite holding
complete austenization. Final step is to cool the hot steel component to room temperature
slowly in the furnace. The full annealing is used to relieve the internal stresses, to reduce
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Schematic representation of annealing operation
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Iron-carbon phase equilibrium diagram
b.Spheroidise annealing
holding the steel component at just below the lower critical temperature (A1) transforms the
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A typical heat treatment cycle to produce spheroidised structure.
d.Recrystallization annealing
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temperature i.e. at temperature between 625 C and 675 C (recrystallization temperature
Stress relief annealing process consists of three steps. The first step is heating the cold
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worked steel to a temperature between 500 C and 550 C i.e. below its recrystallization
temperature. The second step involves holding the steel component at this temperature for 1-
2 hours. The final step is to cool the steel component to room temperature in air.
B.Normalizing
Normalizing process consists of three steps. The first step involves heating the steel
component above the A3 cm temperature for hypoeutectoid steels and above A(upper critical
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temperature for cementite) temperature for hypereutectoid steels by 30 C to 50 C. The
second step involves holding the steel component long enough at this temperature for
homogeneous austenization. The final step involves cooling the hot steel component to
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room temperature in still air. Due to air cooling, normalized components show slightly
Normalizing
C. Hardening
Different techniques to improve the hardness of the steels are conventional hardening,
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a. Conventional hardening
Conventional hardening process consists of four steps. The first step involves heating the
steel to above A3 temperature for hypoeutectoid steels and above A1 temperature for
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hypereutectoid steels by 50 C. The second step involves holding the steel components for
sufficient socking time for homogeneous austenization. The third step involves cooling of
hot steel components at a rate just exceeding the critical cooling rate of the steel to room
temperature or below room temperature. The final step involves the tempering of the
martensiteto achieve the desired hardness. In this conventional hardening process, the
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b. Martempering (marquenching)
Martempering process overcomes the limitation of the conventional hardening process. This
process follows interrupted quenching operation. In other words, the cooling is stopped at a point
above the martensite transformation region to allow sufficient time for the center to cool to the
temperature as the surface. Further cooling is continued through the martensite region, followed
by the usual tempering. In this process, the transformation of austenite to martensite takes place
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b. Austempering
This process is also used to overcome the limitation of the conventional hardening process. Here
the quench is interrupted at a higher temperature than for martempering to allow the metal at the
center of the part to reach the same temperature as the surface. By maintaining that temperature,
both the center and surface are allowed to transform to bainite and are then cooled to room
temperature. Austempering causes less distortion and cracking than that in the case of
D.Tempering
Tempering is achieved by heating hardened steel to a temperature below A1, which is in the
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range of 100 C to 680 C, hold the component at this temperature for a soaking period of 1 to 2
hours (can be increases up to 4 hours for large sections and alloy steels), and subsequently
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Following Figuredepicts the influence of tempering temperature on the properties of steel. It is
observed that the increase in the tempering temperature decreases the hardness and internal
E. Flame Hardening:
Flame hardening is used to harden only a portion of a metal. Unlike differential hardening,
where the entire piece is heated and then cooled at different rates, in flame hardening, only a
portion of the metal is heated before quenching. This is usually easier than differential
hardening, but often produces an extremely brittle zone between the heated metal and the
unheated metal, as cooling at the edge of this heat affected zone is extremely rapid.
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F.Induction hardening
Induction hardening is a surface hardening technique in which the surface of the metal is
heated very quickly, using a no-contact method of induction heating. The alloy is then
quenched, producing a martensite transformation at the surface while leaving the underlying
metal unchanged. This creates a very hard, wear resistant surface while maintaining the
proper toughness in the majority of the object. Crankshaft journals are a good example of an
G.Case hardening
commonly carbon or nitrogen, diffuses into the surface of a monolithic metal. The resulting
interstitial solid solution is harder than the base material, which improves wear resistance
A.Crack: When the internal tensile stresses exceed the resistance of the steel to separation
B.Distortion:Distortion occurs due to uneven heating, too fast cooling, part incorrectly
supported in furnace, incorrect dipping in quenching and stresses present before preheating.
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C.Warping: Asymmetrical distortion of the work is often called warping in heat-treating
practice.
A.METHODS OF ANALYSES
The material used for this study is a medium carbon steel with carbon content of 0.30%
carbon.
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b Heat treating the Medium Carbon Steel
Standard heat treatment procedures were adoptedto heat treat the medium carbon steel. Five
different samples were prepared for each of the operation and the average values were
After the specimens had been heat treated as appropriate, the tensile test were carried out on
them to determine the mechanical properties of the steel and compare it with the non heat
treated specimen which was also subjected to the same tensile test.
a. Hardening process
b. Tempering process
c. Annealing process
d. Normalizing process
C.Material Testing
After the successful heat treatment test was performed on Standard Universal Testing chine.
Figure (b)
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The stress/strain values obtained from the tensile test gave the engineering stress/strain
values. These values were later converted to true stress/strain values using the relationship
given below:
The heat treated specimens were now subjected to tensile test. The resulting engineering
stress - strain curves obtained from the test are shown in Figures 2 to 5 for annealed,
Table 1: The materials property for different heat treated specimens based on true-stress
strain data
The value of yield strength (σy) was observed to be higher for the tempered steel specimen,
possibly as a result of the grain re-arrangement due to the subsequent tempering process. The
yield strength value for the hardened specimen was also observed to be greater than that of
normalized and annealed specimens, while the normalized specimen also has a greater value
than that of annealed specimen, which has the least value. The hardness of the steel increases
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with cooling rate and also with increasing pearlite percentage which increased as the
percentage mertensiteincreases.The increase in the hardness was due to the delay in the
The value of ultimate tensile strength (σu) were observed to be in the order; hardened >
tempered > normalized > annealed, possibly as a result of the refinement of the primary
Beyond the yield point, the stress continuously increases with further plastic strain, while the
slope of the stress-strain curves, representing the strain hardening steadily decreases with
increasing stress.
It was also observed from the graphs that for all the heat treated specimens, except for the
hardened specimen, there were tremendous increase in the toughness of the material which
indicates that hardened material, though have a very high ultimate tensile stress (σu), but at
the expense of its toughness, hence where toughness is a major concern, the material should
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The strain produced for each of the specimen was in the order of annealed > normalized >
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Empirical relationships were also developed to determined various value of stresses at any
given strain and strain rate for each of the specimen. The empirical relationships were given
respectively.
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E.CONCLUSION
From the results obtained, it can be inferred that mechanical properties depends largely upon
the various form of heat treatment operations and cooling rate. Hence depending upon the
properties and the applications that may be required for any design purpose, a suitable form
of heattreatment should be adopted.For high ductile and minimum toughness, annealing the
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6 GENERAL HEAT TREATMENT DATA
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7 EFFECT OF CARBON CONTENT IN METAL STRUCTURE
A Introduction
As an elemental metal, pure iron has only limited engineering usefulnessdespite its allotropy.
Carbon is the main alloying addition that capitalizeson the allotropic phenomenon and lifts
iron from mediocrity intothe position of a unique structural material, broadly known as steel.
To analize the effect of carbon content in iron we would go through the Iron carbon phase
B.Allotropy of Iron
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This diagrame graphically represents the effects of temperature and composition on all the
1) All the alloys in the temperature range above the curve ABCD are in liquid state.
2) Point A on the curve represent the melting point(1539˚C) of pure iron. Point D
lquid along the curve ABC Austenite crystals separate from the liquid metal.
Similarly, the crystal of cementite will separate from the liquid with fall in
temperature of the latter along line CD. The horizontal line HJB represent a pearlite
reaction in which austenite is formed.Crystal of delta (δ) iron separate from the
3) The curve HJECF represents the temperature line along which all carbon always
carbon will solidify at temperatures represented by the solidus line HJE and all
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those containing 2.0 to 6.7% carbon at 1130 ˚C, represented by the solidus line
ECF.Point C corresponds to 4.3% carbon.At this point austenite and cementite are
precipitated from the liquid alloy and form an eutectic alloy called
Eutectoid.
4) Two types of transformation are represented by this diagram, called the Primary
include primary solidification i.e. , the change of alloy phase from liquid to solid
and the secondary transformation include the phase change in solid state.
5) The area of ferrite formation is represented by the region GPQ. Solubility of carbon
in α iron at 723 ˚C is indicated by point p.At this point it is 0.025% carbon and goes
6) Steels having less than 0.8% carbon are called Hypoeutectoide steels and those
having more than 0.8% carbon Hypereutectoid steels.Those steels which contain
the line ES will consist of austenite and cementite. Similarly, cast iron with carbon
below 4.3% will have pearlite and ledeburite, those with exactly 4.3% carbon only
ledeburite having above 4.3% carbon cementite and ledeburite as their phase
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8 FINAL OUTCOME
After analyzing the process of heat treatment it is observed as final outcome that it develops
Relieves the internal stresses set up in the material after hot or cold working
Improves machinability
Increases quality of metal to increase better resistance to heat, corrosion and wear
Improves mechanical properties like tensile strength, ductility and shock resistance etc.
After analyzing the effects of carbon content it is observed as final outcome that with increase
in carbon in steel
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9 SCOPE OF FUTURE STUDY:
Scope for future study regarding heat treatment and carbon percentage in metals is more. I have
learnt a lot from this project by analyzing heat treatment by various method and carbon
percentage.
By changing the percentage of carbon in steel we can control the hardness of steel.
Better optimization of temp. & process can reduce the defects of heat treatment.
Better control of temperature in heat treatment can increase the hardness as well as
toughness.
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10 REFERENCES:
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11 FINAL REMARKS OF PROJECT GUIDE
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