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GRADUATE SCHOOL
Cebu city
FINAL EXAMINATION
equipment.
Always a clean graduated cylinder should be used for measurement because dirt may
chemically contaminate the substance being measured and it may deter accurate
determination of volume. Dirty glassware does not drain properly and the volume delivered may
not be equal to that indicated by calibration mark. Measuring cylinders of 5mL, 10mL, 25mL,
100mL, 250mL, 500mL, 1000mL and 2000mL capacity are available. Measuring cylinders used
for delivering the volume actually contain slightly more than the volume read. This compensates
for the film of liquid left on the walls when liquid is poured out.
b. Using Burette
A burette is simply a long graduated tube of uniform bore with a stopcock or a pinchcock
at one end (Fig. 2.16). It is used for measuring volume in a quantitative (titrimetric) estimation.
The burette reading is noted before and after delivering the liquid. The difference between these
two readings is the volume of the liquid delivered. The liquid should be delivered dropwise. If the
liquid is allowed to run too fast, the walls of the burette will not drain properly and some liquid
may remain sticking to the surface of the walls. This may lead to faulty reading. Measuring
capacity of the burette usually used in the laboratory is 50 mL. Before filling the solution to be
used, the burette should be rinsed with the solution to be filled. For rinsing the burette, few
millilitres of solution are taken into it and the whole inner surface of burette is wetted with the
solution by rotating it. After rinsing, the solution is drained out of the nozzle of the burette.
c. Using Pipette
Normally pipettes of measuring capacity 1 mL, 2 mL, 5 mL, 10 mL, 20 mL, 25 mL etc.
are used. Graduated pipettes are also used in the laboratory work (Fig. 1.3). Pipette is used for
measuring volumes of liquids, when these are to be transferred to a flask or some other
apparatus. Liquids are sucked into the pipette by applying suction through mouth or by using a
pipette filler bulb or a pipette filler pump. It is always safe to use pipette filler bulb or pipette filler
pump to fill the pipette. When poisonous and corrosive solutions are to be drawn into the
pipette, never suck by mouth. Use a pipette filler bulb to draw the liquid up into the
pipette. Hold the pipette in one hand tightly, dip the jet of the pipette into the solution to be
pipetted out, and squeeze the pipette bulb with the other hand. Now loosen your grip on the
bulb so that the liquid is sucked into the pipette. When the liquid is above the etched mark on
the pipette, remove the bulb, and put the index finger of the hand at its place holding the pipette
as shown in Fig. 2.20 c. Loosen the finger carefully to allow the excess liquid to flow out so that
carefully remove the finger and let the liquid run into the flask (Fig. 2.20 d). After emptying the
pipette do not blow out the remaining liquid. Pipettes are so designed that the little amount of
Experiments is a research method in which conditions are controlled so that one or more
allows evaluation of causal relationships among variables while all other variables are
eliminated or controlled. Experimental designs are essential to all experiments. Careful planning
and best time to do the work necessary to ensure that you will have data of the type and quality
Do not adequately control for the problems associated with loss of external or internal
1.1 One – Shot Design (A.K. A after – only design) – a single measure is recorded after
1.2 One – Group Pretest – Postest Design – subjects in the experimental group are
measured before and after the treatment is administered. It has no control group and
offers comparison of the same individuals before and after the treatment. If time
between 1st and 2nd measurements is extended, may suffer maturation. It can also
1.3 Static Group Design ( A.K.A after – only design with control group) – experimental
group is measured after being exposed to the experimental treatment. Control group
measure is taken and major weakness is lack of assurance that the groups were
The simplest experimental design tests just one treatment that is compared with
a no – treatment condition. Subjects are randomly assigned to either the treatment or control
group and are measured or tested both before and after the experimental treatment is
implemented.
2.1 Pretest – Posttest Control Group Design ( A.K.A before – after with control) –
experimental group tested before and after treatment exposure. Control group tested
2.2 Posttest – Only Control Group Design (A.K.A after – only with control) – experimental
group tested after treatment exposure. Control group tested at same time without
effect of all extraneous variables assumed to be the same on both groups. It do not
run the risk of testing effect. Use in situations when cannot pretest.
2.3 Solomon Four Group Design – combines pretest and posttest with control group
design and the posttest with control group design. Provides means for controlling the
interactive testing effect and other sources of extraneous variation. Dies include
random assignment.
members. It allows over all extraneous treatments while manipulating the treatment
variable. Simple to administer, but should not be used unless test members are
similar, and they are also alike regarding a particular extraneous varialble. Different
2.5 Factorial Design – used to examine the effects that the manipulation of at least 2
variable. The impact that each independent variable has on the dependent variable
Groups or subjects not randomly assigned. May not have a comparison group.
3.1 Control Group design with Pretest and Posttest includes an Intervention
Validity implies the extent to which the research instrument measures, what it is
intended to measure. It is related to accuracy and the assessment is difficult. While, reliability
refers to the degree to which scale produces consistent results, when repeated measurements
To sum up, validity and reliability is two vital test of sound measurement.
determining the degree to which variation in observed scale score indicates actual variation
findings about observations and questions. Accurate findings must begin with a design
that determines the overall approach and techniques that will be used. In order to come
up with a good experiment and to choose the best experimental design the following
should be considered:
1. The Study Base – also known as the source population or study cohort, is the group
or population that are studying. Consider who or what is the focus of your study.
2. The Study Timeline – take into account what period of time you should collect data
qualitative.
4. Reliability and Repetition – experiments is reliable and valid if it can be repeated with
similar results. This means that the outcome of the research was not a random
Short size
Double space
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