Method: 862 M1 – DET pH using «Dipping in special»

General

After every titration the electrode equipment is rinsed for 5 seconds in the rinsing
beaker (Position 12) filled with distilled water. At the end of a series the electrode is
also stored in this beaker. Whenever the titration head moves out of the sample
beaker or the rinsing beaker it waits 3 seconds for dripping before it continues.

Parameter

DET pH 862 M1
Start conditions
Activation pulse off
Start delay time 0s
Start volume 0.00000 mL
Dosing rate max. mL/min
Pause 0s
Request sample ID off
Request sample size off
Request sample unit off
Hold during request off
Titration Parameters
Titration rate optimal
Temperature 25.0 °C
Sensor pH electrode
Solution not defined
Stirrer on
Stirring rate 8
Stop conditions
Stop volume 20 mL
Stop meas. value off
Stop EP 9
Volume after EP off
Stop time off
Filling rate max. mL/min
Evaluation
Window off
EP criterion 5
EP recognition all
Fixed EP1 at off
Fixed EP2 at off

862 M1 - 1/2 -
Calculation
Result name EP
R1= EP1
Decimal places 3
Result unit mL
Save as titer off
Save as CV off
Statistics
Statistics off
Reports
Results on
Curve on
Calculation/Statistics off
List of meas. points off
Parameters off
PC/LIMS off
Automation
Automation Dipping in special
Dripping time 3s
Rinsing time 5s
Stirring rate 8

Remarks

Dripping time:
Waiting time after the titration head moves out of the sample or rinsing beaker.
Rinsing time:
Waiting time during which the electrode remains immersed in the rinsing beaker.
Stirring rate:
Stirring rate during the immersion of the electrode in the rinsing beaker.

862 M1 - 2/2 -