Académique Documents
Professionnel Documents
Culture Documents
(JANUARY -MAY)
Student Manual
of
B.E.VI Semester
Class Coordinator
Contents
1. Academic Calendar
2. Time Table
3. Scheme
4. Syllabus
5. Lecture Plan
6. Tutorial
7. Question Papers
VI Semester(Chemical Engg.)GROUP B For batches admitted in July 15 & July, 16 (to
be implemented in July, 2017)
** Out of Two courses only one course will be selected by the students
L - T- P— C-
01 Theory Period: 01 credit; 02 Practical Periods: 01 credit 3 1 - 4
Objective:
To integrate the basic concepts of economics with the tools of mathematics and statistics in
order to analyze and make optimal business decisions.
Unit I Management Concepts: Meaning, Characteristics, Process ,Importance ,functions,
levels of Management, Organizing process and structure, Administration, Difference and
relationship between Organization, Management and Administration ,Scientific
Management.
Unit-II Decision Making: Introduction , Definition, types, techniques, decision making under
uncertainty, decision making under risk Project Management, Meaning of a project,
Characteristics, Project planning, Project organization, Project Report, Tools and Techniques.
Unit-III Managerial Economics Introduction, Meaning, Characteristics, Principles of
Economics, Facto Influencing Manager, Micro and Macro- economics, Theory of Firm,.
Unit-IV Theory of Cost and Break Even analysis, Theory of production.
Unit-V Production systems, Input-Output Analysis, Input Output Analysis
Productivity: Factors affecting, Measuring, Productivity, Reasons for low productivity,
Increasing Productivity of resources.
Ethics: Meaning and importance, sources of Ethics, Personal and Professional Ethics.
Suggested Reading:
Course Outcomes:
Suggested Reading:
1. Shreeves Chemical process industries By Austin G.T. (5th edition Mc- Graw Hill.1984)
2. Outlines of chemical technology By Dryden C.E., M. Gopal Rao (3rd Edition
affiliated
East – West Press ,New Dehli)
3. Chemical Technology Vol.-1 By Pandey G.N. (Lion Press .Kanpur)
Course Outcomes:
• After undergoing this course the students will acquire knowledge regarding various
technological aspects of chemical industries.
• After undergoing this course the students will understand about manufacturing process and
technical problems associated with this
Student will learn to develop flow sheets
Students will learn engineering and environmental problems of various chemical
industries.
Students will acquire knowledge of intermediate for fertilizer industry
Students will understand applications of cement technology
L - T- P— C-
BCHL603 ELECTIVE-II POLYMER TECHNOLOGY 3 1 - 4
Course Objective:
To understand mathematical modeling of polymerizations and design batch and continuous
reactors.
Unit II: Polyaddition reactions Kinetics and rates of polymerization of styrene, Methyl
methacrylate, Ethylene, Polycondensation reactions –Characteristics, Homogeneous
and heterogeneous polycondensation reaction kinetics, Maximum degree of
polycondensation, Industrial polycondensation
Unit III: Kinetics of chain chemical reactions Characteristics of chain reactions, Stationary
and non stationary chain reactions, Kinetics of branched chain reactions, Auto
acceleration and inhibition of chain kinetics, Kinetics of inhibition
Unit VI: Reactors for polymerization Batch, PFR, CSTR with residence time, average
molecular weight and control strategies, Programmed operation of Polyaddition reactors,
Low and high conversion reactors, Industrial Polymerization reactors.
Suggested Reading:
1. G.N. Burnett, “Mechanism of polymerization reaction”, Interscience, 1954.
2. Anil Kumar, S.K. Gupta, “Fundamentals of Polymer Science and Engineering”, Wiley, 1978.
3. G.S. Misra, “Introductory Polymer Chemistry”, Wiley Eastern Ltd., New Delhi, 1993.
4. F. Wilkinson, “Chemical Kinetics and Reaction Mechanism”, Van Norstrand Reinhold
Company Ltd, England, 1980.
5. F. Rodrigues, “Principles of Polymers systems”, McGraw Hill, New York 1970
6. George Odian, “Principles of Polymerization”, 2nd Edition John Wiley and Sons, New York
1981.
Course Outcomes:
• Understand mechanism and mathematical modeling of different types of polymerizations
• Quantitative determination of degree of polymerization and molecular weight distribution
• Design of batch and continuous reactors for these polymerizations
Understand classification of polymerization technique
Understand rates of polymerization
Understand maximum degree of polymerization and kinetic analysis
BCHL604 PROCESS MODELING AND
SIMULATION
L - T- P— C-
3 1 2 5
Unit I The role of analysis: Chemical Engineering Problems, basic concepts of analysis: The
analysis process, A simple example of estimating an order. Source of the model equations:
conservation equations, constitutive equations, control volumes, Dimensional analysis, System
of units, Dimensional consistency in mathematical descriptions, Dimensional analysis and
constitutive relationships, Final observations.
Unit III Treatment of experimental data: Introduction, criteria for Best Fit, Best Slope-I, Best
Slope-II, Best straight line, Physical property correlations, Fitting a quadratic. Simulation
examples of gravity fluid flow, heat and mass transfer, monte-carto simulation.
Suggested Reading:
Russell T. W.F. - INTRODUCTION TO CHEMICAL ENGINEERING ANAL YSIS - John Wiley & Sons
New-York.
Luyben W.L. - PROCESS MODELING, SIMULATION AND CONTROL FOR CHEMICAL ENGINEERS -
II Ed.
Mc. Graw Hill Publishing Co. New York - 1990.
A. K. Jana – Chemical Process Modeling & Computer Simulation, 2 nd Edn., P.H.I.
Course Outcomes
• Understand the important physical phenomena from the problem statement
• Develop model equations for the given system
• Demonstrate the model solving ability for various processes/unit operations
• Demonstrate the ability to use a process simulation
Understand computer programming and convergence
Understand partitioning and tearing
L - T- P— C-
BCHL 605 PROCESS EQUIPMENT DESIGN 3 1 2 5
Course Objectives: The objective of this course is to acquire basic understanding of design
parameter, complete knowledge of design procedures for commonly used process
equipment and their attachments (e.g. evaporator, flash drum, cooling tower, etc.), and
different types of equipment testing methods.
Unit I Scale up criteria and scale up of process equipment. Process design calculations for
heat exchanges equipment shell and take heat exchangers general description, heat transfer
coefficients and pressure drop by Kerm’s & Bells methods rating on existing unit.
Unit II Design of a new system having one or more units in series: single effect evaporation,
Multiple effect evaporator with boiling point elevation.
Unit III Process design calculations for mass exchange equipment plate and packed column
for distribution hand adsorption including column diameter and height.
Unit IV Detailed process and mechanical design, Flash drum, Kettle reboiler, Condenser,
cooling tower rotary drier.
List of Experiment:
Each student should design a complete chemical process plant with mechanical design
details of at least three major equipments.
Suggested Reading:
1. Perry’s Chemical Engg. Hand Book By Perry, Robert H. , Green
Donw (7th Mc Graw Hill New Delhi)
2. Applied Process Design in Chemical Petrochemical plants By E.E. Ludwig (Gulf
Publishing Co. 1964 Vol. – 2)
3. Design of Equilibrium stages By B. D. Smith
4. Chemical Engg. Vol-6 By Coulson J. M.
Richardson J.F (Pergaman Process)
Course outcomes
• Knowledge of basics of process equipment design and important parameters of equipment
design
• Ability to scale up
• Ability a new system having one or more unit in series
Understand various supports and closures
Understand concept of internal and external pressure conditions
Understand scale up criteria
BCHL606 ENERGY TECHNOLOGY
L - T- P— C-
3 1 2 5
Course Objectives:
To understand processing and limitations of fossil fuels (coal, petroleum and natural gas) and
necessasity of harnessing alternate energy resources such as solar, wind, nuclear,
geothermal, tidal and biomass. Also, to understand and practice various characterization
techniques for fuels.
Unit-I Solid Fuels: Coal and lignite reserves in India, Classification of coal, Washing of coal,
analysis of coal, proximate and ultimate analysis.
Unit-II Coal Carbonization, Mechanism of low temperature carbonization and high
temperature carbonization, by- product recovery from coke oven, properties og coke, coal,
grinding, pulverization, briquetting of solid fuels.
Unit-III Liquid Fuels: Origin of Petroleum production, Indian petroleum resources and their
nature, Petroleum processing, distillation, cracking- thermal and catalytic, coking, reforming,
Isomerization, crude Oil Classification, Reserves of Hydrocarbon in India, Introduction to
petroleum refining and processing, atmospheric and vacuum crystallization.
Unit-IV Petroleum product and their utilization, Blending of petrol for octane number
boosting, Transport fuels: Diesel, Petrol, AVL(Aviation Liquid Fuel), Kerosene, fuel and furnace
oil, Testing of petroleum product: Flash Point, pore point, fire point, Octane number, cetane
number, viscosity and viscosity index, API.
Unit-V Gaseous fuels: Natural gas, synthetic gases, their composition & properties, producer
gas, water gas, coal gas, LPG.
List of Experiments:
1. To carry out the proximate analysis of the given coal sample.
2. To determine the calorific value of the coal by Bomb- Calorimeter method.
3. Crushing, grinding, Pulverizing and screening of solid fuel.
4. To determine the viscosity of the given oil sample by Redwood Viscometer No. 1 and No. 2.
5. To determine the viscosity of a given oil sample by saybolt viscometer.
6. To determine the flash and fire points of the given oil sample by Penskey Martin’s
apparatus.
7. To determine the flash and fire points of the given oil sample by Abel’s apparatus.
8. To determine the flash and fire points of the given oil sample by Cleveland apparatus.
9. To determine the carbon residue of the given oil by Rams bottom method.
10. To determine the carbon residue of the given oil by Conrad son method.
11. To determine the calorific value of a gaseous fuel(LPG by boy’s Gas calorimeter.
12. To determine cloud and pour point of given oil sample(coconut) by cloud and pour .
13. To determine the composition of given gas by Orsat apparatus.
14. To determine the sulphur content of the given fuel oil sample by lamp method.
15. To determine the smoke point of the given Kerosene sample.
Note: Each student should perform at least eight experiments out of the above list.
Suggested Reading:
Sarkar S. – FUEL AND COMBUSTION- 2nd ed. ORIENT Longmen, Mumbai, 1996.
Gupta O.P. FUEL & COMBUSTION-3rd ed. Khanna Publishers, New Delhi, 1996.
Francis W. & Peters M. C. – Fuel & Fuel Technology – 2nd Edn., Pergamon, 1980.
Course Outcomes:
• To know the energy demand of world, nation and available resources to fulfill the demand
• To know about the conventional energy resources and their effective utilization
• To acquire the knowledge of modern energy conversion technologies
• To be able to understand and perform the various characterization techniques of fuels
• To be able to identify available nonconventional (renewable) energy resources and
techniques to utilize them effectively.
Understand importance of energy technology in todays world.
Lecture Plan
(BCHL601) Principles of Management & Economics
Unit-2
1 Hydrochloric acid 2
2 Sulphur and sulphuric compounds 3
3 Phosphoric acid 2
4 Phosphates 1
Unit-3
1 Nitrogenous industries 1
2 Ammonia and nitric acid 2
3 Nitrogen fertilizer 2
4 Mixed fertilizers 1
5 N-P-K fertilizers 2
6 Micronutrients 2
Unit-4
1 Cement 2
2 Ceramic 2
3 Glass industries 2
4 Industrial gases: Nitrogen, oxygen 1
5 Industrial gases: hydrogen, helium and argon 2
Unit-5
1 Inorganic chemicals: bromine, iodine and chlorine 2
2 Alumina and aluminum chloride 2
3 Inorganic pigments 2
Total lectures 40
Suggested Reading:
nd
1. Sarkar S.- FUEL AND COMBUSTION- 2 ed. ORIENT Longmen, Mumbai, 1996
nd
2. Gupta O.P.- FUEL AND COMBUSTION- 3 ed. Khanna Publishers, New Delhi,
1996
3. B.K. Bhaskara Rao, R.K. Jain and V. Kumar Safety in chemical plants/Industry and
management, Khanna Publishers
Tutorial Sheets – I
BCHL605, Principles of Management &Economics
Tutorial - II
Tutorial - III
Q1- Briefly discuss the concept of Break-even analysis with suitable diagram.
Q2- What do you mean by managerial economics? Write about its nature and scope.
Q3- Write the significance of input output analysis?
Q4- Write Economies and Diseconomies of various scale production.
Q5- Distinguish between micro and macro economics.
Tutorial - IV
Q.1 Describe the manufacturing process of potassium chloride with flow chart?
Q.2 Describe the manufacturing of soda ash by solvay’s process with flowchart?
Q.4 Describe the manufacturing of sulphuric acid by contact process with flow chart?
Q.5 Describe the manufacturing of ammonium nitrate with flow chart? Write down the major
engineering problem involved in the process?
Q.6 Explain the ammonia oxidation process for nitric acid production with neat flowchart?
Q.7 Explain the process for manufacturing of Portland cement with flow chart?
Q.8 Explain the types and manufacturing of pigments? What are the major engineering
problems in their manufacturing?
Tutorial of Process Modeling and Simulation
1. Explain non reacting liquid system and derive the equations for mass balance and
component mass balance of non reacting liquid system?
2. Study the steady state and unsteady state behavior of modeled equations of non reacting
liquid systems?
3. What are reacting liquid systems?
4. Derive the basic model equations for tank type reactor?
5. Derive the model equations of batch type reactor for first order reaction?
Tutorials
Describe the role of various parts of shell and tube heat exchangers and draw a schematic
diagram of 1,2 shell and tube heat exchanger.
Fuel oil tank is to be heated from 15.5 0C to 43 0C by means of steam coil. The oil has a
pour point below 15.5 0C. This oil stands in the tank and circulates only by natural
convection. Exhaust steam is used and it leaves the coil at atmospheric pressure but not
cooled below 100 0C. The film heat transfer coefficient for fuel oil is 15.7 and the heat
transfer coefficient for condensing steam is 3500. The fouling factors for the oily steam is
4.0 and for fuel oil 7.0 (in terms of heat transfer coefficients). The coil is required to heat
2250 kg/hr of fuel oil of specific heat 0.8 Kcal/kg 0C. The inside diameter of pipe is 4.1
cm and the outside diameter 4.83 cm. calculate the overall heat transfer coefficient and the
heat transfer surface area.
Design an exchanger to sub-cool condensate from a methanol condenser from 95 °C
to40°C. Flow-rate of methanol 100,000 kg/h. Brackish water will be used as the
coolant,with a temperature rise from 25° to 40°C
Gas oil at 200 °C is to be cooled to 40 °C. The oil flow rate is 22,500 kg/h. Cooling water
is available at 30 °C and the temperature rise is to be limited to 20 °C. The pressure drop
allowance on tube side is 25 kN/m2 and shell side is 150 kN/m2. Design a suitable
exchanger for this duty.
Design a shell-and-tube exchanger for the following duty.
20,000 kg/h of kerosene (42° API) leaves the base of a kerosene side-stripping column
at 200°C and is to be cooled to 90°C by exchange with 70,000 kg/h light crude oil(34°
API) coming from storage at 40°C. The kerosene enters the exchanger at a pressureof 5
bar and the crude oil at 6.5 bar. A pressure drop of 0.8 bar is permissible onboth streams.
Allowance should be made for fouling by including a fouling factor of 0.0003 (W/m2°C) -
1
on the crude stream and 0.0002 (W/rn°C)-1 on the kerosene stream.
A 5% aqueous solution of a high molecular weight solute has to be concentrated to 30% in
a forward-feed double effect evaporator at the rate of 8000 kg.h-1. The feed temperature is
40°C.The steam chest is fed with saturated steam at 148°C. A vacuum of 600 mm Hg is
maintained in the second effect. The overall heat transfer coefficients are 550 and 370
kcal.h-1m-2 °C-1 in the first and the last effect respectively. The specific heat of the
concentrated liquor is 0.87 kcal.kg-1 °C-1. Consider vertical short tube evaporator. Latent
heat of vapor generated from effect I and effect II are 531 kcal/kg and 563 kcal/kg
respectively and latent heat of steam is 506 kcal/kg.
a. Calculate the heat transfer area required (assume equal areas in all three
effects).
b. Estimate the steam economy and the steam consumption.
A distillation column for separation of methanol from water receives two feeds 100
kmol/h saturated liquid having 30 mol% methanol, and 100 kmol/h 20% vaporized feed
having 60 mol% methanol. The top product should have 96 mol% methanol, and the
bottom must not contain more than 3 mol% of it. If an external reflux ratio of 1.45 is used,
calculate the amounts of the top and bottom products, and determine the number of ideal
trays required for the separation. The vapor-liquid equilibrium data are given below:
Tutorial
Energy Technology (BCHL606)
4. Write down the importance of washing of coal and different washing techniques.