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Model 3010BR
Preface 1
Thank you! 1
WARNING! 1
Caution 1
Address 1
Introduction 2
Features: 2
Analyzer description: 3
Sensor Warranty: 4
Instrument Warranty: 4
Hydrogen sulfide toxicity: 4
Important: 6
Installation. 7
Location: 7
Safety Considerations: 8
Installation Procedure 9
Initial Calibration: 12
Output Ranges 15
View Output Range 15
Flow Control 19
Maintenance: 22
Periodic Calibration: 22
Sensor Replacement: 22
Sensor replacement cautions: 22
Sensor replacement procedure: 24
Specifications 25
Disclaimer 25
Thank you!
We would like to thank you for purchasing the most cost-effective hydrogen sulfide analyzer available. We
have gone to great lengths to make this analyzer as simple, user-friendly, and complete, as possible. It
includes our revolutionary cell block design that integrates all sample handling components necessary and a
very sophisticated set of electronics. With the optional liquid rejection probe accessory and demister it
provides a complete system for monitoring natural gas gathering systems and many other hydrogen sulfide
applications.
Please verify that the analyzer was not damaged in transit. If so please contact the shipper as well as AMI.
WARNING!
HYDROGEN SULFIDE IS EXTREMELY TOXIC AND CAN BE LETHAL! Read this
manual carefully before using this instrument.
Caution
Read and understand this manual fully before attempting to use the instrument. In particular understand
the hazards associated with using flammable or poisonous gases, and associated with the contents of the
sensor used.
Address
Advanced Micro Instruments.
Costa Mesa, CA 92626
(714) 848-5533
www.AMIO2.com
Introduction
Using the same advanced engineering perfected in the 2010BR trace oxygen analyzer, AMI has produced an
equally effective hydrogen sulfide analyzer. Instead of having to use clumsy, unreliable lead acetate tape,
or alternatively very expensive and delicate laser diode analyzers, AMI has applied a unique electrochemical
sensor to a modified version of the proven platform of the 2010BR to produce an equally effective
hydrogen sulfide analyzer. It provides all the features that the industry has come to expect – fully
programmable alarms, standard isolated voltage or current outputs, and data logging, and the most user-
friendly controls available, together with a fully integrated sample handling system and optional heating, all
in a small weather-proof package that meets all applicable safety standards for hazardous area operation
with flammable gas samples.
The analyzer is designed to be responsive primarily to hydrogen sulfide, but it will also respond to
mercaptans and sulfur dioxide. It should not be used if percent levels of carbon monoxide or hydrogen are
present.
Features:
The electronics are divided into two sections. All of the user controls, the sensor and the display are
mounted in an easily-accessible NEMA box on the right of the assembly, while the power supply and the
safety components, along with the output circuitry are mounted in the small explosion-proof box to the left.
This allows complete control and maintenance when needed without declassifying the area or having to
open an explosion-proof enclosure. The analytical circuit is an “intrinsically safe” circuit that is absolutely
incapable of igniting an explosive mixture of gases even in the presence of two worst-case faults.
The NEMA 4 enclosure contains:
The measuring circuit board and the cell block.
A keypad that allows the user to perform all the normal adjustments required, such as alarm set
points, span, alarm bypass and output range selection.
A large LCD display that shows the H2S reading.
The circuit that measures the output of the sensor, and also measures the temperature of the
cell block, and calculates the H2S level.
o It sends this information digitally into the explosion-proof section on the left.
o It displays the alarm set points, and allows the user to adjust them.
o It displays the output range, which is also selectable.
o It can also display the cell block temperature.
o It displays the “span factor”. This is a useful number that gives an idea of how the
sensor is aging. You could think of it as the setting of the calibration dial on an old-
fashioned analog analyzer.
o The control panel also includes an “Alarm hold off” button. When calibrating the sensor
you normally do not want alarms to shut down the process or pipeline, and so you can
press this button to hold them off for a programmable delay time.
o In addition, it is possible to set up the analyzer so that casual users are not able to make
any adjustments, even though they can see what the alarm settings and the output
range are – they can be locked out of changing them.
The explosion proof box contains:
The safety barriers.
The output/relay PC board.
Sensor Warranty:
The sensor has an expected life of three years, and it is warranted to operate for a period of one year on a
pro-rated basis. If the sensor ceases to operate correctly before this time has elapsed, contact AMI for a
return authorization for evaluation.
Instrument Warranty:
Any failure of material or workmanship will be repaired free of charge for a period of two years from the
original purchase (shipping date) of the instrument. AMI will also pay for one way ground shipment (back to
the user).
This warranty does not cover the sensor, which is covered by its own warranty (see above).
Any indication of abuse or tampering will void the warranty.
At 150-250 ppm the olfactory nerve is paralyzed after a few inhalations, and the sense of smell
disappears, often together with awareness of danger,
530-1000 ppm causes strong stimulation of the central nervous system and rapid breathing, leading
to loss of breathing;
o 800 ppm is the lethal concentration for 50% of humans for 5 minutes exposure(LC50).
Concentrations over 1000 ppm cause immediate collapse with loss of breathing, even after
inhalation of a single breath.
This section contains important information to do with safety and installation. Please don’t skip it!
Installation.
Location:
The unit is designed to be mounted on a wall or on a 2 inch pipe in a general purpose, Class 1 Division 1 or
Class 1 division 2 Group B,C,D area, with a flammable gas sample allowed. When equipped with the
optional heater it may be mounted outdoors in severe environments, though it should be given a sun shield
if in direct sunlight. It should be mounted at a suitable viewing level. Refer to the drawing (figure 1)
showing the analyzer dimensions. EXPLOSION-PROOF SEALS ARE REQUIRED ON THE POWER AND SIGNAL
CONDULET ENTRIES, whether the area classification is Division 1 or Division 2.
Safety Considerations:
The unit is designed for installation in either a general purpose or a Class 1 Div 1 or Div 2 Group B,C,D area,
but it is also designed so that a hazardous gas may be introduced into its NEMA compartment. This gas may
be any group B,C or D gas.
The unit consists of two enclosures mounted on a back panel. The smaller enclosure on the left is
explosion-proof and contains the electrical connections for the user, and also the power supply and safety
components for the NEMA 4 enclosure.
The NEMA 4 enclosure contains the analytical circuitry, the sample handling components and the hydrogen
sulfide sensor. This circuitry is designed for intrinsic safety and meets requirements for Class 1 Div 1 Group
B,C,D.
There is an RS485 connection running ModBus available from the explosion-proof section. This may be
wired up permanently. There is also a USB port in the explosion-proof section that may be used
occasionally by removing the explosion-proof cap. If so, the area MUST be declassified first.
Installation Procedure
1. Mount analyzer in a shelter if convenient, at a convenient eye level, not too close to the
right wall (so as not to interfere with the gas connections).
2. Make the gas connections
a. Connect the sample line with ¼” ss tubing.
b. Make sure that the sample gas line has a pressure no greater than 150 psig.
c. If so, use a pressure reducing regulator and adjust the inlet pressure to 25 psig.
d. Connect the exhaust to a line that goes outside the building, or to a suitable purge
system. Make sure it runs downhill so no condensation from a wet sample forms
ice or water and blocks it up in it in winter.
e. Turn the sample valve to SAMPLE.
f. Adjust sample flow to 1 SCFH with the flow control valve.
We recommend that you use an “Analyzer Guardian” (a liquid rejection device) on the sample line if there is
any possibility of water or entrained liquids in the sample. Don’t allow liquid water to enter the analyzer!
This may mean that you have to cool the sample and drop out water before it gets into the analyzer.
Exhaust
Sensor
Sample inlet
Flowmeter
Initial Calibration:
The sensor has already been installed, and it is ready for operation. The analyzer has been calibrated at the
factory, but changes in altitude will affect the calibration, so it is best to start off with an initial calibration.
Use this procedure:
1. Connect a stainless steel regulator (with Stainless Steel diaphragm ONLY) to span gas tank.
2. Connect the output of the regulator to the span inlet of the analyzer located on the right
side of the NEMA 4 box.
3. Set the regulator pressure to 10psig.
4. We recommend using the special AMI supplied span gas tubing with O ring sealed fittings
so as to prevent fitting damage to the span port.
5. Confirm all fittings are tight.
6. Press the ALARM HOLD OFF button, and adjust the time displayed suitably (typically 30
minutes). This prevents unintentionally setting off alarms if the gas value is higher than the
alarm set points.
7. Turn the analyzer flow valve on the front of the NEMA 4 box to the SPAN position.
If the span gas reads more than 25% wrong, something is wrong either with the gas, or with the plumbing.
Also, changes in altitude will affect the calibration. See the troubleshooting section for some ideas about
curing this. Alternatively you simply haven’t let the span gas flow long enough. Hydrogen sulfide is “sticky”
– that is, it collects on the walls of the tubing and it can take a long time until the gas being delivered has
the same level of H2S in it as the gas in the bottle.
Do not leave the gas cylinder on when you are not spanning the analyzer, as not only may you drain the
cylinder but any leak will contaminate the area and can be dangerous. Turn the bottle off with the cylinder
valve.
General Description:
This analyzer is designed to be as simple to operate as possible. The analyzer displays the Hydrogen sulfide
level in ppms on the LCD. Meanwhile the analog output and the alarms are set on a single (user selectable)
range.
For example, you can set the analog output to correspond to 0-100ppm, and the alarms to be, for example,
40ppm for Alarm 1 and 50ppm for Alarm 2 (i.e. 40% of range and 50% of range), activating above set point.
Be aware that if you then change the output range to 50ppm, the alarm set points will automatically change
to 20ppm and 25ppm respectively. For this reason, set the output range first and then set the alarm set
points.
Only output ranges of 0-50ppm and 0-100ppm are allowed, since the sensor cannot tolerate higher levels of
hydrogen sulfide.
The unit provides the basic controls through the front panel, and more advanced controls are available
through the user interface program (see below in the Advanced Features and Communications section. If
you are going to set up the analyzer using the advanced computer interface, you can skip this section.
Security:
Through the user interface, three levels of security can be set. These are: No security (all front panel
controls work), Span (only the span control and the alarm hold off button are allowed to operate), and Full
security (only the Alarm hold off button performs a function, though other buttons will show settings but
won’t allow them to be changed). If the front panel controls don’t seem to work, use the AMI User
Interface to change the security settings.
The controls all work the same way. You press the
function you want for a second, and let go, and the
display will show the value corresponding to that
function, for about 3 seconds. For example, if you press
the OUTPUT RANGE button for a second, the display will
show the full scale output range. You can change this
value (if the security setting allows) by then pressing the
UP or DOWN arrow button. You can either press this
once for a small change, or you can hold it down , in
which case the number will change slowly at first, and
then faster. If you overshoot your target, press the
other button to go back, and the display will again start
moving slowly.
Span (Calibration)
When the span gas has been flowing for 25 minutes and the reading is stable, press the SPAN button for
one second until the “SPAN” flag appears, and let go, and then quickly push the Up or DOWN button until
the display reads the same as the label on the span gas cylinder. Release the button, and after three
seconds (if security does not forbid it), the new span factor is stored, the “SPAN” flag disappears and the
analyzer drops back to normal operating mode.
Default Settings
The analyzer is tested and shipped with the following default settings, unless otherwise requested by the
customer at the time of purchase.
Changing the output from 1-5 VDC to 4-20mA (or vice versa)
This unit is equipped with a selectable output. It may be either 1-5V or 4-20mA, selectable via a set of
jumpers on the output PCB (the board directly under the cover plate in the explosion proof housing – see
Fig. 3 above). The positioning of the switch is indicated on the PCB itself – put switch on the left-hand
position for 4-20mA, and put it on the right hand position for 1-5V. The 4-20mA option will increase the
current draw to some degree, if the unit is powered from DC and the heater is not used.
The output 4-20mA circuit is capable of driving a 600 Ohm load, while the voltage output needs at least a
10,000 Ohm load. Either will saturate at more than 125% of the nominal full scale range.
Using AMI software you can set the output to 4mA, 12mA and 20mA(or 1V, 3V and 5V), and adjust the
internal settings to calibrate these values so as to get the most accurate possible transfer of information to
a recording or computing device. If you forget to reset them the unit will automatically return to its normal
operation after ten minutes.
Output Selection:
To change from 4-20mA to 1-5V output, or vice versa, swap around the switch as shown in the figure above.
It is in the left hand position for 4-20mA, and the right hand position for 1-5V. If you switch between the
two options the internal calibration will be fairly close but not perfect, so it may be necessary to use the
AMI User Interface to make the output exact.
3 way Selector Valve – Located right beneath the cell cap on the lower right side of the front panel of
the NEMA 4 enclosure. It selects either sample or span gas to flow past the sensor. It can be turned off, to
prevent gas from flowing past the sensor, useful when replacing the sensor. Rotate the valve until the
groove in one side of the valve corresponds with the position marking, and the detent clicks into place.
Flow Control valve – Located in the center of the 3 way selector valve. This provides flow control of
the sample or span gas flowing past the sensor as indicated in the flowmeter.
Flow meter – Shows the sample or span flow rate in the range of 0 to 2 SCFH. The flow should generally
be set at 1 SCFH.
Communication Program:
The analyzer supports both the industry-standard ModBus protocol running on an RS485 loop, and the AMI
User Interface software connected via a USB port. If the USB connection is detected the ModBus
connection will be disabled.
Details of these protocols can be found in the “AMI Communications Manual” provided upon request or
downloaded from the AMI website at www.amio2.com.
Maintenance:
The model 3010BR is virtually maintenance free other than for periodic calibration and occasional sensor
replacement.
Periodic Calibration:
The analyzer should be calibrated about once every month to obtain the best accuracy. The sensor typically
declines in sensitivity by less than 1% of full scale per month, so a monthly calibration is usually satisfactory.
Use in a particularly aggressive environment may degrade the sensor faster: in this case calibrate more
often.
Sensor Replacement:
This should be done based on the Span Factor feature, rather than as a response to a dead sensor. See the
Front Panel Settings and Adjustments section earlier in this manual.
CAUTION: The sensor contains an acid. If there is any sign of a liquid in the
cell compartment, do not allow it to come into contact with your skin. If it
does, immediately flush the affected area with water for a period of at
least 15 minutes. Refer to the Material Safety Data Sheet provided.
Specifications
4 standard user selectable output ranges to choose Minimum detection: 50ppb of Hydrogen Sulfide
from: 0-10ppm, 0-50ppm, 0-100ppm, 0–200ppm (H2S)
Optional output ranges available: 0-500ppm, Repeatability: +/- 1% of range or +/- 0.2ppm of
0-1000ppm and 2000ppm H2S,whichever is greater
o The selection of an output range Operating temperature range: 25 to 115˚ F non-
simultaneously controls the two alarms, the heated; -20 to 115˚ F heated option
analog output and the data logger so that Diurnal temperature specification:< +/- 2 % of scale
all 4 functions operate on the same range over temperature range
Digital display: High resolution 3 ½ digit LCD. Reads 90% full scale response times for specified range: 0-
full scale from 0.00ppm to 100ppm independently of 100ppm < 120 seconds @ 1.5SCFH0-2000ppm < 120
output range selection and 0.00ppm to 2000ppm seconds @ 1.5SCFH
when using high range sensor. Response to Methyl Mercaptan: 40% of actual
Alarms: 2 fully adjustable Hydrogen Sulfide (H2S) concentration
concentration alarms Dry contacts 5A. Response to Sulfur Dioxide: 18% of actual
@24VDC/115VAC concentration
Alarm delays: Programmable from 0-300 minutes Area Classification: Designed to meet UL-913 and UL-
Alarm hold off: Programmable from 0-120 minutes• 1203 Class 1, Div. 1, Groups B,C,D with a flammable
Isolated analog output signal: 1-5VDC or gas sample
4-20mARepresents the output range selected: Inlet gas pressure: 0.5 to 150psig
0-10ppm, 0-50ppm, 0-100ppm, 0-200ppm Gas connections: ¼" 316 S.S. compression fittings
Data logger: Logs data for 15 days @ 1 minute Wetted parts: 316 S.S. fittings, electroless nickel
intervals, 30 days @ 2 minute intervals, etc. plated cellblock, gold plated contacts, acrylic flow
Represents the output range selected: 0-10ppm, meter and Viton O-rings
0-50ppm,0-100ppm,0-200ppm Recommended flow rate: from 1.0 to 1.5 SCFH
Power requirements: 12-24VDC/ 115VAC<70mA. @ Mounting: Wall mount or 2.0" pipe
12VDC non heated<24W @12VDC with heated Dimensions: 13.0"W x 9.5"H x 5.0"D
option Weight: 16 lbs.
Disclaimer
Although every effort has been made to assure that the AMI analyzers meet all their performance
specifications, AMI takes no responsibility for any losses incurred by reason of the failure of its analyzers or
associated components. AMI’s obligation is expressly limited to the analyzer itself.