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to Gas/Liquid Separators
Logan Grim, Wood
Background This paper provides some guidelines for early stages of projects
Gas/liquid separators are a basic unit operation used to segregate and a method for evaluating the effect of inlet piping and inlet de-
phases, commonly found in process plants (Fig. 1). In many situ- vices on gas/liquid separator performance. The effects on the ve-
ations, high-efficiency segregation of the phases is not required as locity profile due to the piping elements will be reviewed as well
the downstream equipment can tolerate carry-over. In other cases, as the impact on the droplet size distribution. With this informa-
poor removal efficiency results in off-specification products, give- tion, the efficacy of gravity separation, and therefore liquid load/
away of product quality and/or suboptimal operation of equipment, challenge to the mist eliminator, can be evaluated using estab-
and thus is critical. It is therefore important to be able to quantify lished methods, such those described by Bothamley (2013). These
the gas/liquid separation performance. methods give designers useful tools to evaluate the adequacy of a
Most vapour/liquid separators are sized using a gravity-based proposed design.
criterion and assume plug flow of the gas and liquid. In reality, the
phases are not evenly distributed across the cross section, resulting Outline of the Procedure
in a degree of underperformance. In certain situations, the piping The methodology is carried out in several steps, illustrated in Fig. 3.
configuration can result in a coherent rotational motion. Centri
fugal motion forces the liquid to the outside of the pipe forming Flow Pattern
an annulus, even if the flow pattern isn’t annular. If this motion Knowledge of the flow pattern is important to the design of sepa-
persists to the inlet of the separator, liquid will jet to the top of the rators, as this tells the designer if there will be intermittent forces,
drum and this may result in bulk liquid carry-over (Fig. 2). such as those occurring in slug flow or high levels of entrainment
A major factor contributing to these effects is the inlet piping such as in annular/mist flow. The author recommends the Taitel and
configuration. However, few guidelines are available. The Amer- Dukler (1976) model, as this has been proven to be reasonably reli-
ican Petroleum Institute (API) provides guidelines (API 686, 2009) able even at larger pipe sizes (Shoham 2006).
for the inlets to pumps, and numerous vendors have specific re- The Taitel and Dukler model calculates the dimensionless liquid
quirements for instruments; however similar criteria are not widely holdup and tests this against stability parameters to determine the
used for separators. Some company standards mandate 10 pipe di- flow pattern. In the original Taitel and Dukler article, for horizontal
ameters (10D) of straight pipe immediately upstream of the sepa- flow, it is shown that the dimensionless liquid height is a function
rator while others have no requirements at all. of the Martinelli parameter only. This allowed the development of
In many situations, however, 10D of straight length is either a graph with the abscissa of the Martinelli parameter which is very
not followed or becomes impractical, especially for large-diameter convenient for hand calculations.
piping. Heijckers (2012) has shown that bends and other pipe fit- For computer applications, this would require the regression of
tings can lead to velocity maldistribution of more than twice the the transition lines for each of the regions. Therefore, it is more
mean velocity (i.e., the maximum face velocity on the mesh pad is useful to calculate the liquid holdup and directly use the transition
twice the average) or flooding of the mist eliminator by bulk liquid. criteria. Since rigorous solution of the liquid holdup is non-trivial,
Inlet Mist
Inlet flow device Eliminator
Swirl
Gas
Distribution H
Velocity
Distortion
This version of this article was updated on 22 May 2018 and contains a number of corrections. | 2018 • Oil and Gas Facilities 1
the author has fit a curve, Eq. 2, based on the Martinelli param-
eter. For turbulent flow in smooth pipes, the Martinelli parameter Flowrate Physical Properties Inlet Piping
(Chisholm 1983) is:
Shear Droplets
To quantify separation performance of gravity separation or mist
Eq. 4—Dimensionless interface area. eliminators, the distribution of the entrained droplets must be
known. The assumption of droplet entrainment preassumes that the
continuous phase is gas and therefore the flow must be annular. The
author has opted to use a two-parameter model for the droplet dis-
tribution based on the recommendations of Kouba (2014). Many
maximum droplet size correlations are available; the author has
Eq. 5—Dimensionless gas velocity. opted to use the modification of Hinze’s equation (1955) by Calder
bank (1958):
For the purposes of separators, the key flow patterns are annular,
slug, and stratified. Stratified wavy is a subset of stratified and it is
2 Oil and Gas Facilities • 2018 | This version of this article was updated on 22 May 2018 and contains a number of corrections.
Few minimum droplet size correlations are available and Subsequent fittings will result in higher levels of shear and thus
Kouba’s is recommended: smaller droplets.
Droplet coalescence is an ongoing area of research and is not
Eq. 12—Kouba’s dmin. well understood. For very high liquid fractions with significant
mass flux, the flow pattern will be slug flow. For slug flow any
liquid droplets will rapidly collide and coalesce, thus breakup due
to fittings has little effect.
For systems with relatively small liquid fractions, some form of
a collision model is required to give a realistic basis for the coales-
With the minimum and maximum droplet size determined, cence of droplets. The following equation based on the model of
the system can be fitted to an assumed distribution such as a Log Radovcich and Moissis (1962) is used to determine the maximum
Normal Distribution, details of which can be found in Kouba. droplet size after a given length of pipe:
Normally, the gas density is used in the minimum droplet
size equation. However, for systems where droplet shattering is Eq. 15—Droplet diameter due to collisions.
likely, such as with inlet deflectors and halfpipes, the gas den-
sity (ρg) is substituted for the liquid density (ρl) as recommended
by Kouba.
For situations where the flow is not annular, alternative methods
are applied. For stratified flow, the flow is likely to separate in the
pipe, and the assumption of no entrainment is reasonable.
For slug flow, the system is characterized by intermittent gas
and liquid flow which will have differing levels of entrainment.
For flow-induced slugging the slug velocity can be estimated
by Shoham:
Eq. 13—Slug translational velocity. Where P is the collision efficiency and c is the characteristic
velocity
The characteristic velocity is assumed to be the turbulent eddy
velocity given by:
Eq. 14—Effective diameter of fittings. The coalescence model is tentative at best, with both the char-
acteristic velocity and the collision efficiency models having little
empirical data behind them. The model also ignores the influence
of peripheral liquid film mass transfer, which may be significant.
However, this exhibits the correct trends (low collision rates at low
liquid fractions and rapid increase in collision rate at high liquid
With the effective diameter calculated, the new effective ve- fractions) and the main sensitivity of the model is the void fraction.
locity can be determined. Using Eqs. 9 and 12, the droplet size dis- Therefore, the result should be representative of the magnitude of
tribution can be determined. coalescence in the pipe.
In the piping, downstream of the fitting, some of the small drop-
lets will begin to coalesce into larger droplets and, given sufficient
straight length, will return to the equilibrium pipe droplet pattern.
This version of this article was updated on 22 May 2018 and contains a number of corrections. | 2018 • Oil and Gas Facilities 3
High Pressure Region
Secondary Flows
4 Oil and Gas Facilities • 2018 | This version of this article was updated on 22 May 2018 and contains a number of corrections.
Eq. 28—Maximum vertical rise of swirling liquid.
Swirling Liquid Film
Flung to Outside
Eq. 26—Angular velocity of the annular liquid ring and gas core. Eq. 30—Velocity distortion due to the inlet device.
Where E is the number of bends being modeled and ω is the an- The term A is a constant for each type of internal and is given as:
gular velocity. The tangential velocity (Vtan) at the inside edge is
used to estimate the maximum vertical travel of the bulk liquid in
the separator. The maximum tangential velocity is given by:
Device Type Constant A
Eq. 27—Maximum tangential velocity of the liquid annulus.
No device 3
Deflector 2
This version of this article was updated on 22 May 2018 and contains a number of corrections. | 2018 • Oil and Gas Facilities 5
(1) Half Pipe (2) Deflector Plate (Frequent in Vertical Drums)
Smaller droplets
“bouncing” off
of the end plate Smaller droplets
“bouncing” off
High velocity over the of the end plate
Most gas “hits” surface re-entrains liquid
liquid surface
The effect of a poorly established velocity profile upstream • Using Eq. 14, approximately 90% of secondary flows are
of the drum needs to be added to the distortion due to inlet de- likely to be dissipated within 10dp of inlet straight pipe
vice. Since the cumulative effect of the maldistribution upstream °° There should be no bends in the horizontal plane within
of the 30dp of straight pipe (not equivalent length) will be 0.002 10dp of the inlet.
(by Eq. 19), this can be ignored. The cumulative distortion factor °° Bends local to the separator within 20dp must be in the same
(Fi & Ftot) is calculated stepwise for each fitting and subsequent plane to avoid bulk liquid swirl.
straight length: • High-shear fittings, such as globe valves, should be positioned
as far as possible from the separator, at least 30dp.
Eq. 31—Dissipation of the velocity profile distortion. • Liquid droplets in systems with high liquid fractions will rap-
idly coalesce while higher void fractions, often found in gas scrub-
bers, will take much longer to reach equilibrium.
• If the above rules cannot be followed, the effectiveness of gas/
liquid separation of a system can be checked using the method-
ology presented.
Actual Velocity/Plug Flow Velocity
3.5
3
2.5
No Device
2
Deflector Plate
1.5
Halfpipe
Refer to the worked example for better understanding of the ad- 1 Vane Device
dition of the distortion factors. 0.5 Cyclone
0
Conclusions and Recommendations 0 2 4 6 8 10 12
A model is presented that enables a designer to evaluate the impact L/Di
of the inlet piping on gas liquid separators. Based on this model the
following observations and recommendations are made. Fig. 8—Effect of inlet device on gas liquid distribution.
6 Oil and Gas Facilities • 2018 | This version of this article was updated on 22 May 2018 and contains a number of corrections.
Symbology Worked Example
A = Distortion constant for an inlet device, dimensionless Below is a worked example of how to use the methods described
A g̃ = Dimensionless gas area above. (The specifics of the example are taken from a problem pre-
ˉc = Characteristic velocity of a particle, m/s sented by Rhyne). A three-phase mixture is passed to a drum. In
df = Effective diameter of a fitting this example, the properties are:
di = Inner diameter of rotating annulus, m
dini = Initial diameter of a droplet entering a pipe Property Gas Liquid
segment, m Flow (kg/s) 8.829 0.435
dmax = Maximum stable droplet diameter, m
dmin = Minimum droplet diameter due to pipe flow, m Density (kg/m3) 15 630
dp = Pipe internal diameter, m
Viscosity (pa.s) 1.2×10–5 2.5×10–4
E = Number of bends effecting rotational motion,
dimensionless Surface tension (N/m) 0.014
En = Energy lost per fitting
F = Taitel and Dukler stability parameter
The inlet pipe is an 8-in. schedule standard pipe (0.20274m ID)
Fi = Cumulative velocity distortion due to fittings
as per Rhyne’s example.
Ftot = Summation of velocity distortion Rhyne does not indicate the fraction of the liquid that is water,
g = Acceleration due to gravity, (9.80665m/s2) therefore the entire stream is assumed to be hydrocarbon.
H = Maximum liquid jet height due to rotation, m The flow pattern first needs to be determined. The mass quality
hL̃ = Dimensionless liquid holdup is calculated from
K = Resistance coefficient of a fitting, dimensionless
Keff = Effective resistance coefficient of a bend,
dimensionless
L = Length of pipe, m
mg = Mass flow of gas, kg/s Next the Martinelli parameter is computed from Eq. 1:
ml = Mass flow of liquid, kg/s
P = Probability of a successful collision, dimensionless
Qg = Gas volumetric flow, m3/s
Ql = Liquid volumetric flow, m3/s
r = Average radius of a bend, m Using Eq. 2 the dimensionless liquid holdup can be determined:
Rens = No-slip Reynolds number, dimensionless
S = Slip ratio, dimensionless
S̃i = Dimensionless interfacial area gradient
V = Velocity, m/s
Vave = Average plug flow velocity, m/s Using the geometric parameters from the original Taitel and
Dukler paper (Eqs. 3, 4, and 5):
Vm = Two-phase homogenous velocity, m/s
Vmax = Maximum velocity of pipe flow, m/s
VSG = Superficial gas velocity, m/s (gas volume flow over
pipe area)
Vtan = Maximum tangential velocity, m/s
VTB = Taylor bubble velocity, m/s
ṼG = Dimensionless gas velocity
We = Pipe Weber number, dimensionless
Wed = Droplet collision Weber number, dimensionless
x = Two-phase vapor mass quality, dimensionless
Xtt = Martinelli parameter for turbulent liquid, turbulent
gas flow, dimensionless
ε = Void fraction, dimensionless This is checked against the stability parameter for stratified flow
λ = Volumetric quality, dimensionless from the original Taitel and Dukler paper (Eqs. 6 and 7). The super-
μL = Liquid dynamic viscosity, Pa.s ficial gas velocity is calculated by:
μG = Gas dynamic viscosity, Pa.s
μNS = No-slip two-phase dynamic viscosity. Pa.s
ρ = Density, kg/m3
ρg = Gas density, kg/m3
ρNS = Homogenous density, kg/m3
The stability parameters are
ρl = Liquid density, kg/m3
σ = Surface tension, N/m
τ = Shear stress, Pa
ω = Angular velocity, rad/s
ωi = Initial angular velocity, rad/s
ωtot = Total angular velocity, rad/s
This version of this article was updated on 22 May 2018 and contains a number of corrections. | 2018 • Oil and Gas Facilities 7
Therefore, the flow is not stratified. This is then checked against A
Eq. 8, and as hL̃ is less than 0.35, the flow is annular. Thus the stan-
dard correlations for shear droplets can be applied.
The pipe routing in Fig. 9 has been followed between the con-
denser and the reflux drum. 4D
The initial conditions, upstream of the first elbow (A), are as-
sumed to be at equilibrium. To solve the Eq. 26 we need the ef-
fective velocity heads contribution to the swirl, the void fraction,
and the velocity and density of the mixed phase. There are three 6D
elbows in the system, each on alternate planes, and since they are B
4D
at right angles a swirl will be induced into the flow. The elbows in
this example are assumed to be long radius (r/D=1.5) therefore
(Eq. 21):
C
Using the Chisholm slip correlation Eq. 24: Now the energy from the first bend is added (Point A); first cal-
culate the swirl of the bend from Eq. 26:
8 Oil and Gas Facilities • 2018 | This version of this article was updated on 22 May 2018 and contains a number of corrections.
Next, calculate the Reynolds number and the Weber number: Weber number is given by Eq. 18:
Adding the second elbow (B) and calculating the net to the third
Pipe Bend Globe Valve elbow (C) (L/dp=4):
d min 22 19 2
This version of this article was updated on 22 May 2018 and contains a number of corrections. | 2018 • Oil and Gas Facilities 9
Now the total residual distortion can be calculated from Eq. 30,
considering the effect of the inlet deflector:
0.15 m
0.15 m
Repeating this for the half pipe and inlet vane device results in
the following, which are compared to Rhyne’s data:
Calculated Rhyne
Device
Distortion Distortion
1.001 m
Deflector 2.19 2.55 1.032 m
Half pipe 1.86 1.86
Inlet Vane 1.62 1. 78
Note that Rhyne presented the distortion for most cases with ideal
pipework. It is assuming that the additive effect for the simple de-
flector is applicable to other cases. 0.203 m
Acknowledgments
I would like to express my appreciation to Wood for assistance
The right-hand term is the contribution of the inlet piping, and in publishing this article. Special thanks to Chris Jones, Cam-
the left-hand is that resulting from the inlet device and the change eron McCormack, and Steve Harrow for their criticism and edito-
in direction in the separator. rial assistance.
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Bubble Flow to Slug Flow. Massachusetts Institute of Technology. Logan Grim is a senior process engineer at Wood, based in Reading,
Rhyne, L.D. 2015. CFD Optimization of Scrubber Inlet Design. SPE Web UK. During his 9 years with Foster Wheeler, now Wood, he has worked
Event. on the process design of refining, LNG, and upstream facilities. He
Shoham, O. 2006. Mechanistic Modeling of Gas-Liquid Two-Phase Flow in has designed several applications for physical property prediction and
Pipes. Richardson, Texas: Society of Petroleum Engineers. equipment sizing and rating. Grim holds an MEng in chemical engi-
Souders, M. and Brown, G.G. 1934. Design of Fractionating Columns, En- neering from Imperial College London and is a chartered member of the
trainment and Capacity. Industrial & Engineering Chemistry, pp. 98–103. IChemE. He may be contacted at logan.grim@woodplc.com.
This version of this article was updated on 22 May 2018 and contains a number of corrections. | 2018 • Oil and Gas Facilities 11