1.

-Graficando:

Del gráfico:

CUT 12min
TP 68min
TIEMPO DE ENFRIAMIENTO 26
TIEMPO TOTAL 104

Microorganismos Parámetros Valor

Z 18
Tiempos T ref 250
Fo (requerido) 6
tp (proceso actual) 68
CUT 10
Th 78
tcc= 0.58CUT 5.8
tb= th - tcc 72.2
Temperaturas T1 240.35
T2 70
T0 76.1
Tg = TB 235.76
g = t1 - tg 4.59
log g 0.661812686
t1 - t0 164.25
Ecuacion de la curva de calentamientoLog(T1 - T) =log(T1- Tintercepto) - t/fh 2.215505378
Ecuacion de curva de enfriamiento log(T-T2)=LOG(TBA-T2)-FC^-1t 0.785329835
Analiticas FH=PENDIENTE^-1 26.38 min
log (T1- TA) 1.9654369
T1 - TA 92
TA = 148
T1 - T0 164.25
Jh = (T1 - TA)/(T1-T0) 0.562252664
fc = pendiente^-1 112.36 min
log(TBA - T2) 0.968116212
TBA - T2 9.29215
TB - T2 169.4
Jc = (TBA - T2)/(TB - T2) 0.056057855
TBA 79.29215
t TR T
0 146.66 76.1
2 174.74 79.52
4 194.36 84.56
6 206.96 91.04
8 217.94 98.96
10 239.9 108.68
12 239.9 118.22
14 239.9 127.4
16 240.08 136.4
18 240.08 144.86
20 240.44 152.78
22 240.44 160.16
24 240.26 166.82
26 240.26 173.3
28 240.26 179.24
30 240.44 184.64
32 240.62 189.68
34 240.62 194.36
36 240.62 198.68
38 240.26 202.64
40 240.44 206.06
42 240.44 209.3
44 240.44 212.36
46 240.26 215.06
48 240.26 217.4
50 240.44 219.74
52 240.44 221.72
54 240.44 223.52
56 240.26 225.14
58 240.44 226.58
60 240.44 227.84
62 240.26 229.28
64 240.44 230.18
66 240.62 231.26
68 240.62 232.16
70 240.26 232.88
72 240.44 233.78
74 240.44 234.32
76 240.44 235.04
78 240.26 235.76
80 219.56 235.4
82 135.32 230.72
84 98.6 226.22
86 86.36 219.38
88 83.48 211.1
90 82.22 200.48
92 81.14 190.22
94 78.62 180.14
96 78.26 170.78
98 77.36 162.5
100 77.18 157.1
102 77.18 150.44
104 76.82 144.5
2.- Calculo del Fo (proceso)

t TR T LOG (T1-T) LOG(T-T2) L ((L+(L+1))/2*dt Fo acumulado

0 146.66 76.1 2.24029958 #¡NUM! 2.18217E-10 5.56196E-10 5.56196E-10
2 174.74 79.52 2.23167344 #¡NUM! 3.37978E-10 9.81983E-10 1.53818E-09
4 194.36 84.56 2.21864052 #¡NUM! 6.44004E-10 2.11933E-09 3.65751E-09
6 206.96 91.04 2.20128785 #¡NUM! 1.47533E-09 5.53872E-09 9.19623E-09
8 217.94 98.96 2.17909198 #¡NUM! 4.06339E-09 1.81527E-08 2.73489E-08
10 239.9 108.68 2.15020363 #¡NUM! 1.40893E-08 6.183E-08 8.91789E-08
12 239.9 118.22 2.1198495 #¡NUM! 4.77407E-08 2.02227E-07 2.91406E-07
14 239.9 127.4 2.08849047 #¡NUM! 1.54486E-07 6.43013E-07 9.34419E-07
16 240.08 136.4 2.05537833 #¡NUM! 4.88527E-07 1.93027E-06 2.86469E-06
18 240.08 144.86 2.02176797 #¡NUM! 1.44175E-06 5.41265E-06 8.27734E-06
20 240.44 152.78 1.98775562 #¡NUM! 3.9709E-06 1.41777E-05 2.2455E-05
22 240.44 160.16 1.95346974 0.334453751 1.02068E-05 3.41338E-05 5.65888E-05
24 240.26 166.82 1.92001892 0.945468585 2.3927E-05 7.87407E-05 0.00013533
26 240.26 173.3 1.88479536 1.184691431 5.48137E-05 0.000172003 0.000307333
28 240.26 179.24 1.84978782 1.327154512 0.00011719 0.000351013 0.000658346
30 240.44 184.64 1.81531204 1.42553422 0.000233824 0.000679366 0.001337712
32 240.62 189.68 1.78046133 1.500785173 0.000445542 0.001256296 0.002594008
34 240.62 194.36 1.74538712 1.560623875 0.000810754 0.002219682 0.00481369
36 240.62 198.68 1.71028665 1.609380944 0.001408928 0.003747167 0.008560857
38 240.26 202.64 1.67541169 1.649724186 0.002338239 0.005959742 0.0145206
40 240.44 206.06 1.64286005 1.681783766 0.003621503 0.00910287 0.02362347
42 240.44 209.3 1.60959441 1.710117365 0.005481367 0.013588903 0.037212373
44 240.44 212.36 1.57564961 1.735279448 0.008107536 0.019559735 0.056772108
46 240.26 215.06 1.5433229 1.756331767 0.011452199 0.026900791 0.083672899
48 240.26 217.4 1.5132176 1.773786445 0.015448591 0.036288168 0.119961067
50 240.44 219.74 1.48086892 1.790566625 0.020839576 0.047686152 0.167647218
52 240.44 221.72 1.45147941 1.804275767 0.026846575 0.060644411 0.228291629
54 240.44 223.52 1.42291798 1.816373889 0.033797836 0.075378257 0.303669886
56 240.26 225.14 1.39550112 1.826981337 0.041580422 0.091571084 0.39524097
58 240.44 226.58 1.36958689 1.836197481 0.049990662 0.108724569 0.503965539
60 240.44 227.84 1.34556976 1.844104231 0.058733907 0.129347594 0.633313133
62 240.26 229.28 1.31638975 1.852967691 0.070613687 0.149843547 0.78315668
64 240.44 230.18 1.29710365 1.858416878 0.07922986 0.170197911 0.953354591
66 240.62 231.26 1.27276959 1.864866914 0.090968051 0.193035882 1.146390473
68 240.62 232.16 1.25139485 1.870169721 0.102067832 0.213982984 1.360373457
70 240.26 232.88 1.23350376 1.874365836 0.111915152 0.237486018 1.597859475
72 240.44 233.78 1.21005085 1.879554601 0.125570866 0.260122473 1.857981947
74 240.44 234.32 1.19534606 1.882638362 0.134551607 0.28208451 2.140066458
76 240.44 235.04 1.17493159 1.886716274 0.147532903 0.309299515 2.449365973
78 240.26 235.76 1.15350999 1.890756252 0.161766612 0.316252526 2.765618499
80 219.56 235.4 1.16435286 1.888740961 0.154485915 0.239382239 3.005000738
82 135.32 230.72 1.28510703 1.86165387 0.084896325 0.132637036 3.137637775
84 98.6 226.22 1.37621185 1.833911715 0.047740712 0.067642353 3.205280128
86 86.36 219.38 1.48600519 1.788026884 0.019901641 0.026802273 3.232082401
88 83.48 211.1 1.5899496 1.725094521 0.006900632 0.008674368 3.240756769
90 82.22 200.48 1.69478064 1.628184508 0.001773736 0.002251143 3.243007912
92 81.14 190.22 1.77655591 1.508125536 0.000477407 0.000608896 3.243616808
94 78.62 180.14 1.84422858 1.345177617 0.000131489 0.000171198 3.243788005
96 78.26 170.78 1.89883484 1.106530854 3.9709E-05 5.34776E-05 3.243841483
98 77.36 162.5 1.94200805 0.653212514 1.37686E-05 2.06692E-05 3.243862152
100 77.18 157.1 1.96801571 #¡NUM! 6.90063E-06 9.8443E-06 3.243871996
102 77.18 150.44 1.99808489 #¡NUM! 2.94367E-06 4.32053E-06 3.243876317
104 76.82 144.5 2.02325246 #¡NUM! 1.37686E-06 1.621266629 4.865142946
Escogiendo las velocidades letales superiores a 0,002 y aplicando la relación:

Fo (proceso) = ∆t. ∑ Li

∑ Li =1.621265252

∆t =2min

Fo(proceso)=3.242530505

GARFICO DE Fo acumulado
3.5

2.5
Fo acumulado

1.5
Series1
1

0.5

0
0 20 40 60 80 100
TIEMPO
t TR T LOG (T1-T) LOG(T-T2) L Fo acumulado
34 240.62 194.36 1.65934564 1.560623875 0.002913697 0.009322382
36 240.62 198.68 1.61616031 1.609380944 0.005063426 0.017299505
38 240.26 202.64 1.57240687 1.649724186 0.008403195 0.030766126
40 240.44 206.06 1.53071184 1.681783766 0.013015008 0.052184329
42 240.44 209.3 1.48713838 1.710117365 0.019699012 0.084898349
44 240.44 212.36 1.44153804 1.735279448 0.029136974 0.133734335
46 240.26 215.06 1.39689645 1.756331767 0.04115707 0.204028379
48 240.26 217.4 1.35410844 1.773786445 0.055519359 0.300704807
50 240.44 219.74 1.30663944 1.790566625 0.074893555 0.431117721
52 240.44 221.72 1.26197619 1.804275767 0.096481588 0.602492864
54 240.44 223.52 1.21695721 1.816373889 0.121463123 0.820437576
56 240.26 225.14 1.17201881 1.826981337 0.149432287 1.091332987
58 240.44 226.58 1.12775252 1.836197481 0.179657125 1.420422399
60 240.44 227.84 1.08493357 1.844104231 0.211078716 1.81115824
62 240.26 229.28 1.03019479 1.852967691 0.253772434 2.27600939
64 240.44 230.18 0.99211149 1.858416878 0.284737354 2.814519177
66 240.62 231.26 0.94151143 1.864866914 0.326922224 3.426178754
68 240.62 232.16 0.89431606 1.870169721 0.366812768 4.119913746
70 240.26 232.88 0.85247999 1.874365836 0.402202202 4.888928717
72 240.44 233.78 0.79379038 1.879554601 0.451278294 5.742409213
74 240.44 234.32 0.75434834 1.882638362 0.483553404 6.67724091
76 240.44 235.04 0.69548168 1.886716274 0.530205764 7.691000077
78 240.26 235.76 0.62736586 1.890756252 0.581359059 8.8025649
80 219.56 235.4 0.66275783 1.888740961 0.555193591 9.939117551
82 135.32 230.72 0.96754798 1.86165387 0.305101571 10.79941271
84 98.6 226.22 1.13924922 1.833911715 0.171571222 11.27608551
86 86.36 219.38 1.31428866 1.788026884 0.07152279 11.51917952
88 83.48 211.1 1.46089784 1.725094521 0.024799587 11.61550189
90 82.22 200.48 1.59681694 1.628184508 0.006374475 11.64667596
5.823320874
11.64664175
t TR T LOG (T1-T) LOG(T-T2) L Fo acumulado
34 240.62 194.36 1.65934564 1.560623875 0.002913697 0.009322382
36 240.62 198.68 1.61616031 1.609380944 0.005063426 0.017299505
38 240.26 202.64 1.57240687 1.649724186 0.008403195 0.030766126
40 240.44 206.06 1.53071184 1.681783766 0.013015008 0.052184329
42 240.44 209.3 1.48713838 1.710117365 0.019699012 0.084898349
44 240.44 212.36 1.44153804 1.735279448 0.029136974 0.133734335
46 240.26 215.06 1.39689645 1.756331767 0.04115707 0.204028379
48 240.26 217.4 1.35410844 1.773786445 0.055519359 0.300704807
50 240.44 219.74 1.30663944 1.790566625 0.074893555 0.431117721
52 240.44 221.72 1.26197619 1.804275767 0.096481588 0.602492864
54 240.44 223.52 1.21695721 1.816373889 0.121463123 0.820437576
56 240.26 225.14 1.17201881 1.826981337 0.149432287 1.091332987
58 240.44 226.58 1.12775252 1.836197481 0.179657125 1.420422399
60 240.44 227.84 1.08493357 1.844104231 0.211078716 1.81115824
62 240.26 229.28 1.03019479 1.852967691 0.253772434 2.27600939
64 240.44 230.18 0.99211149 1.858416878 0.284737354 2.814519177
66 240.62 231.26 0.94151143 1.864866914 0.326922224 3.426178754
68 240.62 232.16 0.89431606 1.870169721 0.366812768 4.119913746
70 240.26 232.88 0.85247999 1.874365836 0.402202202 4.888928717
72 240.44 233.78 0.79379038 1.879554601 0.451278294 5.742409213
74 240.44 234.32 0.75434834 1.882638362 0.483553404 6.67724091
76 240.44 235.04 0.69548168 1.886716274 0.530205764 7.691000077
78 240.26 235.76 0.62736586 1.890756252 0.581359059 8.8025649
80 219.56 235.4 0.66275783 1.888740961 0.555193591 9.939117551
82 135.32 230.72 0.96754798 1.86165387 0.305101571 10.79941271
84 98.6 226.22 1.13924922 1.833911715 0.171571222 11.27608551
86 86.36 219.38 1.31428866 1.788026884 0.07152279 11.51917952
88 83.48 211.1 1.46089784 1.725094521 0.024799587 11.61550189
90 82.22 200.48 1.59681694 1.628184508 0.006374475 11.64667596
∑ Li 5.823320874
∑ Li. ∆t 11.64664175

3.- Hallar tp para Fo = 2, 7, 10 y 14 (Método General)

tcv Fo
78 3.23 Fo tcv tp (aprox.)
76 2.87 2 70.6495468 60.6495468
74 2.53 7 100.861027 90.8610272
72 2.24 10 118.987915 108.987915
14 143.1571 133.1571
 A1 A2 A3 A4
T L T L T L T L

0 0 0 0
38 0.00233824 38 0.00233824 38 0.00233824 38 0.00233824
40 0.0036215 40 0.0036215 40 0.0036215 40 0.0036215
42 0.00548137 42 0.00548137 42 0.00548137 42 0.00548137
44 0.00810754 44 0.00810754 44 0.00810754 44 0.00810754
46 0.0114522 46 0.0114522 46 0.0114522 46 0.0114522
48 0.01544859 48 0.01544859 48 0.01544859 48 0.01544859
50 0.02083958 50 0.02083958 50 0.02083958 50 0.02083958
52 0.02684658 52 0.02684658 52 0.02684658 52 0.02684658
54 0.03379784 54 0.03379784 54 0.03379784 54 0.03379784
56 0.04158042 56 0.04158042 56 0.04158042 56 0.04158042
58 0.04999066 58 0.04999066 58 0.04999066 58 0.04999066
60 0.05873391 60 0.05873391 60 0.05873391 60 0.05873391
62 0.07061369 62 0.07061369 62 0.07061369 62 0.07061369
64 0.07922986 64 0.07922986 64 0.07922986 64 0.07922986
66 0.09096805 66 0.09096805 66 0.09096805 66 0.09096805
68 0.10206783 68 0.10206783 68 0.10206783 68 0.10206783
70 0.11191515 70 0.11191515 70 0.11191515 70 0.11191515
72 0.12557087 72 0.12557087 72 0.12557087 72 0.12557087
74 0.13455161 74 0.13455161 74 0.13455161 74 0.12055161
76 0.1475329 76 0.1475329 76 0.1305329 76 0.0805329
78 0.16176661 78 0.14176661 78 0.08166661 78 0.04166661
80 0.15448591 80 0.0848591 80 0.0408591 80 0.0150591
82 0.08489632 82 0.04489632 82 0.01600632 82 0.00489632
84 0.04774071 84 0.01774071 84 0.00474071
86 0.01990164 86 0.00690164
88 0.00690063
∑ 1.616380 1.436853 1.266961 1.121310
Fo (min) 3.232760 2.873706 2.533922 2.242621
 3.50

3.00

2.50 y = 0.1655x - 9.6925

VALOR Fo (min)

R² = 0.9978
2.00

1.50

1.00

0.50

0.00
71 72 73 74 75 76 77 78 79
TIEMPO DE CIERRE DE VAPOR (min)

Areas bajo las curvas de letalidades

0.18
0.16
0.14
0.12
0.1
L

0.08
0.06
0.04
0.02
0
0 4 8 12 16 20 24 28 32 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96
TIEMPO (min)

4.- Datos:

Z vitamina = 12 °C

Fo mo = 15 minutos

METODO DE LA ECUACION LINEALIZADA DE LA CURVA DE RETENCION DE LA VITAMINA

TIEMPO % RETENCIÓN Log (R )

2.6 95 1.977723605
7.4 90 1.954242509
15.0 80 1.903089987
47.0 50 1.698970004
 Log (R ) vs tiempo
2

1.95

1.9 y = -0.0063x + 1.9977

R² = 0.9995
1.85
Log (R)

1.8

1.75

1.7

1.65
0.0 10.0 20.0 30.0 40.0 50.0
tiempo (min)