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Data File C:\CHEM32\1\DATA\ARAMIS\AJP-2-5.

D
Sample Name: AJP-2-5

=====================================================================
Acq. Operator : SYSTEM
Sample Operator : SYSTEM
Acq. Instrument : Agilent 218 HPLC Location : Vial 1
Injection Date : 5/6/2020 3:21:42 PM
Inj Volume : Manually
Method : C:\CHEM32\1\METHODS\ARAMIS.M
Last changed : 5/6/2020 2:49:50 PM by SYSTEM
(modified after loading)
MWD1 A, Channel 1 (mAU) at 220 nm (ARAMIS\AJP-2-5.D)
mAU
5.465

21.252
21.341
21.666
7000
6000
5000
1

1- 02
3

14.560 1-0 4
05

R - 006
1 7
1- 8
R 009
1 0
25.565 1-011
26.205R1- 12
27.112 1-013
14
4000
00

00

13.990 R 00

1 0

R - 00

R - 01
24.160
R 1- 0

R 1- 0

R -0

R 0
1-

13.635 1-

1
3000
R

20.490 R
5.950

25.805
14.978
2000
12.814

29.090
15.520
15.798

17.055
17.428
18.195

28.577
16.153

18.027
18.561
18.728
18.884
19.184
19.328
20.109

29.541
10.767
11.627

16.454

19.583
19.822

30.832

34.654
3.235

31.689
32.195
32.349
32.909
33.422
34.137

35.652

39.858
4.866

9.874
8.435
8.922
7.654
2.454

1000
0

0 5 10 15 20 25 30 35 min
MWD1 B, Channel 2 (mAU) at 254 nm (ARAMIS\AJP-2-5.D)
mAU
5.511

400
21.054

300
1

1- 02
3

14.540 1- 4
14.976 005

22.024 R1 0067

23.277 1-0 8
23.742 R 09
1 10
25.700 1-0 1
26.187 R1- 12
-0 3
14
00

00

13.990 R 00

21.389R1--00

R - 00

25.150 R -01

26.779 R1 01
R 1- 0

24.218 R1-0
1-

13.659 1-

200
R

20.526 R
18.199
17.430

19.331
15.528

19.179
17.060

18.561
18.698

20.089
15.739
16.158
15.944

25.512
16.455
12.813

24.403
24.499

27.911

30.817
29.586
29.852

39.821
5.960

33.412
10.758
10.235
3.286

5.049

100

0
0 5 10 15 20 25 30 35 min
MWD1 C, Ratio channel (ARAMIS\AJP-2-5.D)
0.008
0.138
0.335
0.354
0.372
0.835
0.976
1.112
1.135
1.355
1.428
1.495
1.538
1.591
1.688
1.795
1.842
2.024
2.092
2.451
2.766
2.866
3.127
4.2924.278
4.338
5.362

-10000

-20000
1

1- 02
3

R 004
5

R - 006
1 7
1- 8
R 009
1 0
1 1
R - 012
1- 3
4
00

00

00

1 0

R - 00

R - 01
R - 01
R - 01

01
R 1- 0

R 1- 0
1-

1-
1-

1
R

-30000

-40000

0 5 10 15 20 25 30 35 min

==================================================================================
Fraction Information
==================================================================================
==================================================================================
Frac Well Location Volume BeginTime EndTime Reason Mass
# # [µl] [min] [min]
-----|-----|----------|----------|----------|----------|-------------|------------
1 1 R1-001 0.00 3.1267 3.5467 MWD1
2 1 R1-002 0.00 5.3600 5.9167 MWD1
3 1 R1-003 0.00 5.9267 6.2433 MWD1
4 1 R1-004 0.00 13.4800 13.7700 MWD1
5 1 R1-005 0.00 14.4433 14.7533 MWD1
6 1 R1-006 0.00 20.8933 21.4300 MWD1
7 1 R1-007 0.00 21.4333 22.2333 MWD1
7 2 R1-008 0.00 22.2333 23.0333 MWD1

Agilent 218 HPLC 5/6/2020 4:02:04 PM SYSTEM Page 1 of 5


Data File C:\CHEM32\1\DATA\ARAMIS\AJP-2-5.D
Sample Name: AJP-2-5

7 3 R1-009 0.00 23.0333 23.6733 MWD1


8 1 R1-010 0.00 23.9033 24.7033 MWD1
8 2 R1-011 0.00 24.7033 25.1500 MWD1
9 1 R1-012 0.00 25.4767 26.2767 MWD1
9 2 R1-013 0.00 26.2767 26.7433 MWD1
10 1 R1-014 0.00 26.9767 27.3267 MWD1
==================================================================================
=====================================================================
Area Percent Report
=====================================================================

Sorted By : Signal
Multiplier : 1.0000
Dilution : 1.0000
Use Multiplier & Dilution Factor with ISTDs

Signal 1: MWD1 A, Channel 1 (mAU) at 220 nm

Peak RetTime Type Width Area Height Area


# [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------|
1 2.454 BV 0.2276 574.47620 33.74401 0.0648
2 3.235 VB 0.2405 7752.97900 455.63477 0.8742
3 4.866 BB 0.2871 1359.39368 66.89101 0.1533
4 5.465 BV 0.2040 1.08608e5 8017.95508 12.2460
5 5.950 VB 0.1409 6903.93848 726.41876 0.7784
6 7.654 BV 0.6031 2028.43164 39.83453 0.2287
7 8.435 VV 0.6675 1817.40039 32.79814 0.2049
8 8.922 VV 0.4194 918.54651 28.77750 0.1036
9 9.874 VV 0.8229 2534.85620 40.07969 0.2858
10 10.767 VB 0.3921 396.30389 13.13004 0.0447
11 11.627 BB 0.2448 140.75124 8.51832 0.0159
12 12.814 BB 0.3263 950.61792 37.81178 0.1072
13 13.635 BV 0.3142 3646.77588 172.80113 0.4112
14 13.990 VV 0.2935 2361.03784 121.06068 0.2662
15 14.560 VV 0.3016 2896.64990 148.45518 0.3266
16 14.978 VB 0.2654 1578.11902 94.22317 0.1779
17 15.520 BV 0.2035 436.84470 35.50690 0.0493
18 15.798 VB 0.1948 352.54099 26.06722 0.0398
19 16.153 BB 0.1365 63.52588 7.52554 7.163e-3
20 16.454 BB 0.1479 78.99143 8.95932 8.907e-3
21 17.055 BV 0.2371 678.26538 40.34764 0.0765
22 17.428 VB 0.1983 572.49933 40.39936 0.0646
23 18.027 BV 0.1169 201.27853 26.40863 0.0227
24 18.195 VB 0.1793 600.87170 48.57514 0.0678
25 18.561 BV 0.1248 106.53967 13.39987 0.0120
26 18.728 VV 0.1264 104.14636 12.09709 0.0117
27 18.884 VB 0.1475 87.73412 9.51751 9.892e-3
28 19.184 BV 0.1421 175.39642 19.47905 0.0198
29 19.328 VV 0.1654 251.37035 21.34988 0.0283
30 19.583 VB 0.1063 38.19155 5.54936 4.306e-3
31 19.822 BB 0.1090 16.10786 2.44201 1.816e-3
32 20.109 BV 0.2026 329.44458 23.64346 0.0371
33 20.490 VB 0.2027 228.16243 16.88327 0.0257
34 21.252 BV 0.2175 8.21728e4 6205.54834 9.2653
35 21.341 VV 0.1070 4.69933e4 6227.30225 5.2987

Agilent 218 HPLC 5/6/2020 4:02:04 PM SYSTEM Page 2 of 5


Data File C:\CHEM32\1\DATA\ARAMIS\AJP-2-5.D
Sample Name: AJP-2-5

Peak RetTime Type Width Area Height Area


# [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------|
36 21.666 VB 1.1122 5.55722e5 7307.60254 62.6596
37 24.160 BB 0.7100 2.41376e4 464.69910 2.7216
38 25.565 BV 0.1796 1145.19507 102.33642 0.1291
39 25.805 VV 0.1437 848.51721 89.43600 0.0957
40 26.205 VB 0.4173 1.67267e4 637.19135 1.8860
41 27.112 BB 0.3623 6553.96777 260.72058 0.7390
42 28.577 BV 0.3081 651.82147 30.40194 0.0735
43 29.090 VV 0.2906 1153.84509 63.92537 0.1301
44 29.541 VB 0.2106 322.31912 24.47634 0.0363
45 30.832 BB 0.2786 293.82446 15.26330 0.0331
46 31.689 BV 0.2909 250.94168 13.25410 0.0283
47 32.195 VV 0.1649 44.67699 3.47765 5.037e-3
48 32.349 VB 0.1751 40.97863 3.27241 4.620e-3
49 32.909 BV 0.2605 80.19303 4.81070 9.042e-3
50 33.422 VB 0.2358 53.66199 3.01336 6.051e-3
51 34.137 BV 0.2942 123.04384 6.67200 0.0139
52 34.654 VV 0.2917 315.43362 15.88284 0.0356
53 35.652 VB 0.3941 325.25568 12.23831 0.0367
54 39.858 BB 0.3664 143.85950 5.35583 0.0162

Totals : 8.86891e5 3.18932e4

Signal 2: MWD1 B, Channel 2 (mAU) at 254 nm

Peak RetTime Type Width Area Height Area


# [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------|
1 3.286 BB 0.4069 185.19385 6.35572 1.0425
2 5.049 BV 0.4376 203.23500 6.53912 1.1441
3 5.511 VV 0.2026 6899.33252 530.84631 38.8382
4 5.960 VB 0.2061 642.41949 42.55669 3.6164
5 10.235 BV 0.4582 135.05836 3.66227 0.7603
6 10.758 VB 0.4217 155.54146 4.66805 0.8756
7 12.813 BB 0.4029 195.30432 6.38354 1.0994
8 13.659 BV 0.3046 693.17365 33.60653 3.9021
9 13.990 VV 0.3104 543.87128 26.39920 3.0616
10 14.540 VV 0.2717 619.94452 35.85623 3.4898
11 14.976 VB 0.2694 349.05206 20.94951 1.9649
12 15.528 BV 0.2154 290.90665 22.26865 1.6376
13 15.739 VV 0.0943 41.31743 6.48638 0.2326
14 15.944 VV 0.1315 46.46489 5.18819 0.2616
15 16.158 VB 0.1613 75.43921 6.91424 0.4247
16 16.455 BB 0.1567 50.18825 4.62022 0.2825
17 17.060 BV 0.2153 302.99231 21.00159 1.7056
18 17.430 VB 0.2174 388.66718 27.24851 2.1879
19 18.199 BB 0.2060 462.26761 31.34965 2.6022
20 18.561 BV 0.1307 68.66906 8.28320 0.3866
21 18.698 VB 0.1083 39.43745 5.65970 0.2220
22 19.179 BV 0.1532 151.10947 15.71445 0.8506
23 19.331 VB 0.1685 212.77031 17.66587 1.1977
24 20.089 BV 0.1999 168.60497 11.92645 0.9491
25 20.526 VV 0.2220 183.92444 11.66055 1.0354

Agilent 218 HPLC 5/6/2020 4:02:04 PM SYSTEM Page 3 of 5


Data File C:\CHEM32\1\DATA\ARAMIS\AJP-2-5.D
Sample Name: AJP-2-5

Peak RetTime Type Width Area Height Area


# [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------|
26 21.054 VV 0.1980 2070.85742 156.90216 11.6574
27 21.389 VB 0.1923 528.56659 36.63001 2.9754
28 22.024 BB 0.2163 49.66092 3.07657 0.2796
29 23.277 BV 0.2084 480.89740 34.13654 2.7071
30 23.742 VB 0.2320 104.36111 6.72721 0.5875
31 24.218 BV 0.1796 27.50480 2.20436 0.1548
32 24.403 VV 0.0699 10.05020 2.02564 0.0566
33 24.499 VB 0.1716 29.14050 2.27253 0.1640
34 25.150 BV 0.1974 59.22788 4.50330 0.3334
35 25.512 VV 0.1990 112.04134 7.92382 0.6307
36 25.700 VV 0.2204 111.27840 6.78260 0.6264
37 26.187 VB 0.1813 63.42340 5.19947 0.3570
38 26.779 BB 0.4008 541.97076 19.89526 3.0509
39 27.911 BV 0.2454 64.64054 3.53374 0.3639
40 29.586 BV 0.2033 64.26407 4.06801 0.3618
41 29.852 VB 0.2087 63.58718 3.93131 0.3579
42 30.817 VB 0.2697 103.80167 5.09579 0.5843
43 33.412 VV 0.3144 67.00842 2.85929 0.3772
44 39.821 BBA 0.3651 107.12766 3.74031 0.6031

Totals : 1.77643e4 1225.31873

Signal 3: MWD1 C, Ratio channel

Peak RetTime Type Width Area Height Area


# [min] [min] %
----|-------|----|-------|----------|----------|--------|
1 7.81e-3 BV 0.0106 4.40996 6.93703 1.223e-4
2 0.138 VV 0.0765 492.96820 111.75027 0.0137
3 0.335 VB 0.0992 2246.48999 300.93564 0.0623
4 0.354 BV 0.0220 201.94200 154.92711 5.602e-3
5 0.372 VB 0.0170 144.97530 142.10593 4.022e-3
6 0.835 BV 0.0736 108.49255 20.23048 3.010e-3
7 0.976 VV 0.1130 807.15991 93.23120 0.0224
8 1.112 VB 0.0442 666.91345 184.89673 0.0185
9 1.135 BB 0.0305 240.94238 136.05774 6.684e-3
10 1.355 BV 0.0878 725.84637 110.32671 0.0201
11 1.428 VB 0.0271 332.50546 204.64554 9.224e-3
12 1.495 BV 0.0958 897.78845 156.44589 0.0249
13 1.538 VV 0.0283 264.24725 155.81750 7.330e-3
14 1.591 VV 0.0639 620.00134 139.46199 0.0172
15 1.688 VV 0.0796 630.44000 117.55514 0.0175
16 1.795 VB 0.0653 433.16000 104.89515 0.0120
17 1.842 BV 0.1246 684.67468 79.42658 0.0190
18 2.024 VV 0.0839 438.57355 74.30704 0.0122
19 2.092 VV 0.0604 299.47241 73.64774 8.308e-3
20 2.451 VB 0.3426 2021.89221 77.18968 0.0561
21 2.766 BV 0.0848 2.23367e4 3733.76880 0.6196
22 2.866 VV 0.0711 3.40415e4 6504.45166 0.9443
23 3.127 VV 1.8228 2.12325e6 1.37248e4 58.9000
24 4.278 VB 0.0223 6.66673e4 5.11680e4 1.8494
25 4.292 BV 0.0124 2.01115e4 2.74978e4 0.5579

Agilent 218 HPLC 5/6/2020 4:02:04 PM SYSTEM Page 4 of 5


Data File C:\CHEM32\1\DATA\ARAMIS\AJP-2-5.D
Sample Name: AJP-2-5

Peak RetTime Type Width Area Height Area


# [min] [min] %
----|-------|----|-------|----------|----------|--------|
26 4.338 VV 0.0302 1.01349e5 4.20594e4 2.8115
27 5.362 VB 21.8985 1.22481e6 652.76410 33.9770

Totals : 3.60483e6 1.47786e5

=====================================================================
*** End of Report ***

Agilent 218 HPLC 5/6/2020 4:02:04 PM SYSTEM Page 5 of 5

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