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OPTIMASI METODE SPEKTROFOTOMETRI UNTUK PENENTUAN TIOSIANAT

BERDASARKAN PEMBENTUKAN SENYAWA HIDRINDANTIN MENGGUNAKAN
OKSIDATOR HIPOKLORIT
Nadia Mira Kusumaningtyas, Hermin Sulistyarti*, Qonitah Fardiyah
Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Brawijaya
Jl. Veteran Malang 65145
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ABSTRAK
7LRVLDQDW DGDODK VHQ\DZD \DQJ PHPSXQ\DL VLIDW JRLWURJHQLN 6LIDW LQL DNDQ PHQ\HEDENDQ JDQJJXDQ
DNLEDW NHNXUDQJDQ LRGLXP *$., 3HQHQWXDQ WLRVLDQDW GDSDW GLODNXNDQ GHQJDQ PHUHDNVLNDQ QLQKLGULQ GDQ
RNVLGDWRU KLSRNORULW PHPEHQWXN VHQ\DZD KLGULQGDQWLQ ELUX GDODP VXDVDQD EDVD 6HQ\DZD KLGULQGDQWLQ ELUX \DQJ
WHUEHQWXN GLDQDOLVD VHFDUD VSHNWURIRWRPHWUL SDGD SDQMDQJ JHORPEDQJ PDNVLPXP QP 9DULDEHO SHQHOLWLDQ LQL
PHOLSXWL ZDNWX SHQJXNXUDQ GDUL PHQLW S+ ODUXWDQ GDQ NRQVHQWUDVL KLSRNORULW 0 VHEDJDL
RNVLGDWRU GDODP UHDNVL RNVLGDVL WLRVLDQDW PHQMDGL VLDQLGD XQWXN SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ +DVLO
SHQHOLWLDQ PHQXQMXNNDQ ZDNWX RSWLPXP UHDNVL RNVLGDVL WLRVLDQDW PHQMDGL VLDQLGD XQWXN SHPEHQWXNDQ VHQ\DZD
KLGULQGDQWLQ DGDODK PHQLW GDQ VWDELO VDPSDL PHQLW NH 5HDNVL RNVLGDVL WLRVLDQDW PHQMDGL VLDQLGD GDQ
SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ VHFDUD RSWLPXP WHUMDGL SDGD S+ NRQVHQWUDVL RSWLPXP KLSRNORULW \DQJ
GLJXQDNDQ SDGD SURVHV RNVLGDVL WLRVLDQDW DGDODK 0

Kata kunci : *$., JRLWURJHQLN KLGULQGDQWLQ QLQKLGULQ WLRVLDQDW

ABSTRACT
7KLRF\DQDWH LV D VXEVWDQFH ZKLFK KDV JRLWURJHQLF SURSHUWLHV FDXVLQJ LRGLQH GHILFLHQF\ GLVRUGHUV
,'' 7KLRF\DQDWH ZDV R[LGL]HG ZLWK K\SRFKORULWH LQ DONDOLQH FRQGLWLRQ LQ WKH SUHVHQFH RI QLQK\GULQ WR IRUP
EOXH FRORUHG K\GULQGDQWLQ VXEVWDQFH ZKLFK LV DQDO\]HG E\ VSHFWURSKRWRPHWU\ DW ZDYHOHQJWK RI QP ,Q WKLV
UHVHDUFK WKH PHWKRG ZDV RSWLPL]HG WRZDUGV R[LGL]LQJ WLPH IURP PLQXWHV S+ RI VROXWLRQ IURP DQG
K\SRFKORULWH FRQFHQWUDWLRQ IURP 0 7KH UHVXOWV VKRZHG WKDW WKH RSWLPXP WLPH IRU WKLRF\DQDWH R[LGDWLRQ
ZDV PLQXWHV DQG ZDV VWDEOH XS WR PLQXWHV RSWLPXP VROXWLRQ S+ RI DQG RSWLPXP FRQFHQWUDWLRQ RI
K\SRFKORULWH RI 0

Keywords ,'' JRLWURJHQLF K\GULQGDQWLQ QLQK\GULQ WKLRF\DQDWH

PENDAHULUAN
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PHQ\HEDENDQ NHUDFXQDQ VHSHUWL PXDO OHPDK GDQ NHPDWLDQ > @ 7LRVLDQDW PHPSXQ\DL VLIDW
JRLWURJHQLN \DLWX ]DW \DQJ PHQHNDQ VHNUHVL KRUPRQ WLURLG > @ *DQJJXDQ SHPEHQWXNDQ
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*$., PHUXSDNDQ PDVDODK VHULXV \DQJ WHUMDGL GL ,QGRQHVLD 3HQGHULWD DNDQ PHQJDODPL
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6HODLQ LWX WHODK GLNHPEDQJNDQ PHWRGH WHV NLW WLRVLDQDW \DQJ GLGDVDUNDQ SDGD SHPEHQWXNDQ
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GNN > @ WHODK PHQJHPEDQJNDQ PHWRGH SHQHQWXDQ VLDQLGD GHQJDQ SHPEHQWXNDQ VHQ\DZD
KLGULQGDQWLQ \DQJ PHQJKDVLONDQ VHQVLWLILWDV GDQ OLQLHULWDV \DQJ WLQJJL 6HPHQWDUD LWX
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GDODP VXDVDQD EDVD VHKLQJJD PHPEHQWXN VHQ\DZD KLGULQGDQWLQ EHUZDUQD ELUX 0HQJLQJDW
ZDNWX UHDNVL GDQ NRQVHQWUDVL RNVLGDWRU VDQJDW EHUSHQJDUXK WHUKDGDS NHVHPSXUQDDQ UHDNVL
RNVLGDVL WLRVLDQDW PHQMDGL VLDQLGD GDQ MXJD SHPEHQWXNDQ KLGULQGDQWLQ PDND SDGD SHQHOLWLDQ
LQL GLODNXNDQ RSWLPDVL WHUKDGDS GXD SDUDPHWHU WHUVHEXW

METODOLOGI
Alat dan Bahan
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Optimasi waktu terhadap oksidasi tiosianat dan pembentukan senyawa hidrindantin
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GHQJDQ VSHNWURIRWRPHWHU SDGD UDQJH ZDNWX PHQLW VHWLDS PHQLW VHNDOL SDGD SDQMDQJ
JHORPEDQJ PDNVLPXP QP
Optimasi pH terhadap oksidasi tiosianat dan pembentukan senyawa hidrindantin
/DUXWDQ 6&1 SSP GLDPELO P/ GLPDVXNNDQ NH GDODP WDEXQJ UHDNVL
GLWDPEDKNDQ 1D &2 VHEDQ\DN P/ QLQKLGULQ VHEDQ\DN P/ GDQ KLSRNORULW
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NHPXGLDQ GLXNXU DEVRUEDQVLQ\D GHQJDQ VSHNWURIRWRPHWHU SDGD SDQMDQJ JHORPEDQJ
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HASIL DAN PEMBAHASAN

Penentuan waktu optimum dalam proses oksidasi tiosianat dan pembentukan senyawa
hidrindantin
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KLGULQGDQWLQ GLODNXNDQ XQWXN PHQJHWDKXL ZDNWX SURVHV RNVLGDVL WLRVLDQDW GDQ SHPEHQWXNDQ
VHQ\DZD KLGULQGDQWLQ VHFDUD VHPSXUQD GDQ PHQFDSDL NHVHWLPEDQJDQ 2SWLPDVL ZDNWX
NHVWDELODQ VHQ\DZD KLGULQGDWLQ EHUZDUQD ELUX GLODNXNDQ PXODL PHQLW GHQJDQ LQWHUYDO
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1.2
1.0
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0.8
0.6
0.4
0.2
0.0
10 15 20 25 30 35 40
Waktu (menit)
Gambar 1. *UDILN KXEXQJDQ DQWDUD ZDNWX GDQ DEVRUEDQVL WHUKDGDS SHPEHQWXNDQ VHQ\DZD
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ODQMXW \DQJ GLWXQMXNNDQ GHQJDQ ZDUQD ELUX VHQ\DZD KLGULQGDQWLQ VHPDNLQ PHPXGDU

Penentuan pH optimum dalam proses oksidasi tiosianat dan pembentukan senyawa

hidrindantin
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3URVHV SHQHQWXDQ WLRVLDQDW EHUGDVDUNDQ SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ DNDQ RSWLPXP
DSDELOD EHUHDNVL GDODP NRQGLVL EDVD PHQXUXW 1DJDUDMD GNN > @ 6HKLQJJD RSWLPDVL S+
GLODNXNDQ SDGD NLVDUDQ S+ PHODOXL SHQJXNXUDQ DEVRUEDQVL SDGD SDQMDQJ JHORPEDQJ
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1.6 2SWLPXP
1.4
1.2
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1.0
0.8
0.6
0.4
0.2
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9 10 11 12 13 14
pH

Gambar 2. *UDILN KXEXQJDQ S+ GDQ DEVRUEDQVL WHUKDGDS SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ

3DGD S+ WHUMDGL SHQLQJNDWDQ DEVRUEDQVL NDUHQD SDGD S+ WHUVHEXW PXODL WHUMDGL
SURVHV RNVLGDVL WLRVLDQDW PHQMDGL VLDQLGD \DQJ GLWDQGDL GHQJDQ PXQFXOQ\D ZDUQD PHUDK
DNLEDW SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ PHUDK \DQJ NHPXGLDQ WXUXQ SDGD S+ NDUHQD
WHUMDGL SHUJHVHUDQ EDWRNURPLN GDUL QP NH QP 6HGDQJNDQ SDGD S+ WHUMDGL
SHQLQJNDWDQ DEVRUEDQVL NHPEDOL NDUHQD SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ EHUZDUQD ELUX
S+ RSWLPXP XQWXN SHPEHQWXNDQ VHQ\DZD KLGULQGDQWLQ ELUX DGDODK .DUHQD SDGD PHWRGH
LQL KLGULQGDQWLQ \DQJ GLJXQDNDQ VHEDJDL GDVDU SHQJXNXUDQ DGDODK KLGULQGDQWLQ EHUZDUQD ELUX
PDND S+ GLWHQWXNDQ VHEDJDL S+ RSWLPXP SHQJXNXUDQ GDQ GLJXQDNDQ XQWXN SHUFREDDQ
VHODQMXWQ\D 3HQLQJNDWDQ S+ GL DWDV GDSDW PHQ\HEDENDQ QLQKLGULQ \DQJ EHUHDNVL DNDQ
WHUGHNRPSRVLVL VHKLQJJD PHQXUXQNDQ VHQ\DZD KLGULQGDQWLQ \DQJ WHUEHQWXN
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sianida
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VLDQLGD VHEDJDL SURGXN \DQJ DNDQ GLKDVLONDQ 2OHK NDUHQD LWX SHUOX GLODNXNDQ RSWLPDVL
NRQVHQWUDVL RNVLGDWRU DJDU VLDQLGD \DQJ GLKDVLONDQ GDODP MXPODK \DQJ PDNVLPDO 2NVLGDWRU
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\DQJ PDPSX PHQJRNVLGDVL WLRVLDQDW PHQMDGL VLDQLGD VHODLQ LWX KLSRNORULW PHUXSDNDQ ODUXWDQ
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Konsentrasi Hipoklorit (M)

Gambar 3. *UDILN KXEXQJDQ NRQVHQWUDVL KLSRNORULW GDQ DEVRUEDVL WHUKDGDS SHPEHQWXNDQ

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