2a

7.445
7.437
7.262
7.193
7.185
7.170
7.162
7.106
7.094
7.071
4.509
4.501
4.489
4.469
4.449
4.421
4.401
4.391
4.381
4.371
4.361
3.926
2.189

0.071
0.000
Current Data Parameters
NAME 25_ramesh
EXPNO 30
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 19.27
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 203
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300197 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
0.420
0.682
0.662
0.419

2.547
2.581
0.053

0.308

PC 1.00
 2a

7.445
7.437

7.5
1.000 7.262
7.193
0.420 7.185
0.682 7.170
0.662 7.162
0.419

7.0
7.106
7.094
7.071

6.5
6.0
5.5
5.0
4.509
4.501
4.489
4.469
4.449
2.547
4.5
4.421
2.581 4.401
4.391
4.381
4.371
4.0

0.053 4.361
3.926
3.5
3.0
2.5

0.308 2.189
ppm
2b

-0.000
8.264
8.258
8.235
8.218
8.207
8.202
8.189
8.185
8.090
7.671
7.649
7.549
7.541
7.462
7.263
7.156
7.148
7.133
7.125
7.067
7.045
5.504
4.709
4.572
4.517
4.470
4.450
4.430
4.410
4.391
4.371
4.351
4.150
4.066
3.918
2.956
2.883
2.169
1.592
0.072
0.008
Current Data Parameters
NAME 25_ramesh
EXPNO 7
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 17.12
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 203
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300192 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
0.190
1.000
0.125
0.977
0.575
0.158
0.558
0.587
0.035
0.050
1.193
2.408
0.123
0.045
0.028
0.008
0.012
0.012
0.004
0.009
0.049
0.043
0.107
PC 1.00
2c

7.567
7.559
7.264
7.145
7.138
7.123
7.115
7.069
7.046
4.471
4.451
4.430
4.422
4.410
4.402
4.382
4.362
3.917
2.771
2.168
1.628

0.073
0.000
Current Data Parameters
NAME 25_ramesh
EXPNO 24
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 18.53
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 144
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300188 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
1.225
1.348

5.451
0.047

3.527
0.200
1.581
PC 1.00
 2c

7.7
7.6
1.000 7.567
7.559

7.5
7.4
7.3
7.264

7.2

7.145
7.138
1.225
7.123
7.115
7.1

7.069
1.348
7.046
7.0
6.9 ppm
2d

7.543
7.536
7.257
7.239
7.206
7.138
7.115
7.108
7.071
7.049
4.493
4.462
4.442
4.422
4.411
4.401
4.391
4.371
4.351
2.345
2.166
1.610
1.256

0.073
0.000
Current Data Parameters
NAME 25_ramesh
EXPNO 8
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 17.20
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 203
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300213 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
0.305
1.000
1.085

2.368

1.064
0.075
0.466
0.017 PC 1.00
 2d

7.60
7.543

7.55
0.305
7.536

7.50
7.45
7.40
7.35
7.30
7.257

7.25
1.000 7.239

7.206
7.20
7.15

7.138
7.115
1.085 7.108
7.10

7.071
7.049
7.05
7.00
6.95
ppm
2e

7.616
7.611
7.598
7.593
7.534
7.527
7.416
7.412
7.394
7.278
7.273
7.260
7.255
7.242
7.239
7.225
7.222
7.206
7.135
7.127
7.112
7.104
7.070
7.048
4.631
4.465
4.445
4.425
4.407
4.405
4.388
4.368
4.348
3.913
3.791
Current Data Parameters
NAME 25_ramesh
EXPNO 23
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 18.47
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 144
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300203 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
1.031
0.943
2.457
1.223
1.269

2.569
5.207
0.028
0.145

0.031

PC 1.00
 2e

7.7
7.616
7.611
1.000
7.598

7.6
7.593

1.031 7.534
7.527

7.5
7.416
0.943 7.412

7.4
7.394

7.278

7.3
7.273
7.260
7.255
2.457 7.242
7.239
7.225
7.222
7.2

7.206

7.135
1.223 7.127
7.112
7.104
7.1

7.070
1.269
7.048
7.0
ppm
2F

7.567
7.559
7.267
7.143
7.135
7.120
7.112
7.072
7.050
4.475
4.455
4.434
4.422
4.414
4.402
4.382
4.362
3.339
3.321
3.303
3.284
2.167
1.695
1.527
1.509
1.490
1.478
Current Data Parameters
NAME 25_ramesh
EXPNO 3
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 16.38
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 128
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300176 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
0.440
0.850
0.885
0.462

5.551

2.399

0.041
0.721
3.569
PC 1.00
 2F

7.6
7.567
1.000
7.559

7.5
7.4
7.3
7.267

7.2

7.143
0.440 7.135
7.120
0.850
7.112
7.1

0.885 7.072

0.462 7.050
7.0
6.9
ppm
2G

7.539
7.532
7.456
7.439
7.365
7.360
7.356
7.343
7.325
7.318
7.314
7.304
7.297
7.288
7.279
7.258
7.136
7.129
7.114
7.106
7.067
7.044
4.523
4.461
4.440
4.420
4.408
4.400
4.388
4.368
4.348
2.164
1.629
Current Data Parameters
NAME 25_ramesh
EXPNO 20
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 18.30
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 203
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300212 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
1.833
3.028
1.204
1.213

2.437
5.159

0.059
1.077
PC 1.00
 7.325
2G

7.318
1.000
7.314

7.5
1.833
7.304
3.028 7.297
1.204 7.288
1.213 7.279

7.0
7.258
7.136
7.129
7.114
7.106

6.5
7.067
7.044

6.0
5.5
5.0
4.523
4.461
4.440
2.437 4.420

4.5
5.159 4.408
4.400
4.388
4.368
4.0
3.5
3.0
2.5 4.348

0.059 2.164
2.0

1.077 1.629
ppm
 2G

7.60
7.55
1.000 7.539
7.532

7.50
1.833 7.456

7.45
7.439

7.40
7.365
7.360
7.356
7.343

7.35
7.325
3.028 7.318
7.314
7.304

7.30
7.297
7.288
7.279
7.258

7.25
7.20
7.15

7.136
1.204 7.129
7.114
7.106
7.10

7.067
1.213
7.044
7.05
7.00
6.95
ppm
2h

7.568
7.561
7.265
7.148
7.140
7.125
7.118
7.074
7.051
6.067
6.049
6.042
6.032
6.025
6.007
6.000
5.990
5.982
5.965
5.412
5.409
5.370
5.367
5.239
5.214
4.525
4.477
4.457
4.437
4.420
4.417
4.400
4.380
4.360
3.932
Current Data Parameters
NAME 25_ramesh
EXPNO 9
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 17.25
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 203
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300183 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
1.179
1.276

0.805
0.991
0.978
5.107
2.386

0.246
1.404
0.333 PC 1.00
 2h

7.60
1.000 7.568
7.561

7.55
7.50
7.45
7.40
7.35
7.30
7.265
7.25
7.20

7.148
7.15

1.179 7.140
7.125
7.118
7.10

7.074
1.276
7.051
7.05
ppm
 2h

6.067

6.2
6.049
6.042
6.032
0.805 6.025
6.007

6.0
6.000
5.990
5.982
5.965

5.8
5.6
5.412
5.409
0.991

5.4
5.370
5.367

0.978 5.239
5.214

5.2
5.0
4.8

4.525
4.6

4.477
4.457
4.437
5.107 4.420
4.4

4.417
4.400
4.380
4.360
4.2
4.0

2.386 3.932
3.915
ppm
 2i

7.900

7.9
1.000
7.878

7.8
1.000 7.718

7.7
0.994 7.670

7.6
7.555
7.531
2.285 7.524

7.5
7.495

7.4
7.3

7.260
0.634 7.239
7.2

7.154
7.147
1.224 7.132
7.125
7.1

7.060
1.263
7.037
ppm
2i

7.900
7.878
7.718
7.670
7.555
7.531
7.524
7.495
7.260
7.239
7.154
7.147
7.132
7.125
7.060
7.037
4.888
4.847
4.445
4.425
4.417
4.405
4.397
4.384
4.377
4.357
4.025
3.898
3.854
2.168
1.581
1.255
Current Data Parameters
NAME 25_ramesh
EXPNO 2
PROCNO 1

F2 - Acquisition Parameters
Date_ 20180425
Time 16.32
INSTRUM spect
PROBHD 5 mm PABBO BB-
PULPROG zg
TD 32050
SOLVENT CDCl3
NS 32
DS 0
SWH 6410.256 Hz
FIDRES 0.200008 Hz
AQ 2.4999001 sec
RG 203
DW 78.000 usec
DE 6.50 usec
TE 298.0 K
D1 2.00000000 sec
TD0 1

======== CHANNEL f1 ========

NUC1 1H
P1 13.50 usec
PL1 -3.00 dB
PL1W 13.42244530 W
SFO1 400.2330017 MHz

F2 - Processing parameters
SI 131072
SF 400.2300205 MHz
WDW EM
15 14 13 12 11 10 9 8 7 6 5 4 3 2 1 ppm SSB 0
LB 0.30 Hz
GB 0
1.000
1.000
0.994
2.285
0.634
1.224
1.263

2.401
4.975
0.135
2.816

0.253

0.171 PC 1.00