Académique Documents
Professionnel Documents
Culture Documents
Abstract
In this study, a microstructural investigation was conducted on the side cracking phenomenon occurring in thick low-carbon steel plates
during hot rolling. Particular emphasis was placed on the role of iron oxides and ferrite–pearlite band structure in the side cracking. Detailed
microstructural analyses of the cracked region showed that the ferrite–pearlite band structure in the side region was considerably slanted to
the surface, while that in the central region was parallel to the surface. Small cracks were often observed when the iron oxide layer formed
by inhomogeneous oxidization along the slanted ferrite–pearlite band structure in the side region within 30 mm from the plate edge was
intruded into the interior after hot rolling. In addition to these small cracks, a few large cracks were also found when some protrusions formed
on the plate surface were decarburized, folded and then intruded into the interior. Based on these findings, the parallel arrangement of the
ferrite–pearlite band structure in the side region by the appropriate control of the hot rolling process and the minimization of the iron oxide
formation by the minimized time exposed to high temperatures were suggested in order to prevent or minimize the side cracking.
© 2005 Elsevier B.V. All rights reserved.
Keywords: Side cracking; Low-carbon steel plate; Hot rolling; Iron oxide layer; Pearlite band structure
1. Introduction However, since the scarfing treatment itself affects the pro-
ductivity, it is better to be omitted. In some mill plants, this
When classifying rolled steel products, those thicker than side cracking phenomenon is not only minimized, but mill
6 mm are generally called “plates”, which are then clas- edge plates are mass produced by applying manufacturing
sified in many types, depending on strength, condition of technology of trimming free plates (TFP), leading to reduced
side cutting, alloy composition, surface treatment, processing production costs.
method, application and so on [1]. Depending on the condi- It is also known that the side cracking considerably varies
tion of side cutting, there are two kinds of plates, i.e., mill edge with the kind of slabs. For instance, low-quality slabs expe-
plate (no-trimming plate) in which only the top and tail parts rience serious cracking problems, whereas the problem is
are cut, but not the side parts and slit edge plate (trimming much less frequent in the high-quality slabs. The reasons
plate) whose side parts are cut by gas or a machine. The side for the side cracking can be largely divided into one due to
cracking often occurring on the surface of the side parts along materials themselves or the other case from processing con-
the rolling direction after hot rolling significantly decreases ditions. With respect to materials, cracks can initiate when
the productivity of plates. Presently, when side cracks occur microvoids formed along grain boundaries due to volume
on the plate surface, side trimming is applied, or the cracked change at the time of phase transformation from austenite to
region is removed by whole-wide cutting. The side cracking ferrite during hot rolling are coalesced [2,3]. Side or corner
problem is also alleviated by scarfing slabs before hot rolling. cracks can also occur when microcracks formed on slabs are
corroded by oxidization during reheating and are grown large
during hot rolling. In terms of processing conditions, when
∗ Corresponding author. Tel.: +82 54 279 2140; fax: +82 54 279 2399. reheating or hot rolling conditions are not appropriate for the
E-mail address: shlee@postech.ac.kr (S. Lee). steel plates, cracking problems arise. Previous studies on the
0921-5093/$ – see front matter © 2005 Elsevier B.V. All rights reserved.
doi:10.1016/j.msea.2005.04.045
178 B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187
Table 1
Chemical composition and dimensions of the slabs and steel plates used in this study
Hot rolling Slab T Slab W Chemical composition (wt.%) Plate T Plate W Plate L
process (mm) (mm) (mm) (mm) (mm)
C Mn Si P S Al V Ti Cu
A 248 1580 0.15 1.40 0.26 0.019 0.001 0.04 0.003 0.001 0.029 18.94 2645 16816
B 250 1580 0.15 1.37 0.29 0.012 0.001 0.05 0.001 0.002 0.013 17.50 2692 20383
side cracking phenomenon which significantly reduces the and both sides of four parts out of the eight were scarfed.
productivity of steel plates are scarce. Particularly, the rea- This was to eliminate any possible defects that might not be
son for the cracking of 1–2% frequency in high-quality slabs visible from the surface but present inside the slabs. For con-
is poorly understood. Therefore, the formation mechanism venience, those scarfed are referred to as specimens ‘1–4’
of side cracks and the need for presenting ways to prevent following the alphabet of ‘A’ or ‘B’ indicating the process,
them require imminent attention in view of the productivity while those non-scarfed are referred to as specimens ‘5–8’.
of plates, labor cost, energy reduction and quality improve- Observation of the scarfed slab surface revealed excel-
ment. lent surface condition without visible defects. To observe
In the present study, microstructural analysis was con- any possible microcracks present inside the slabs, the cor-
ducted on the side cracking phenomenon occurring during ner and center regions of the scarfed slabs were cut, and the
hot rolling of thick low-carbon steel plates to elucidate the interior was observed by an optical microscope. The eight
crack formation mechanism. Based on the analysis results, slab specimens in each process of A and B were cut again
correlation between microstructural factors and hot rolling into two parts, and the parts were put under hot rolling test
conditions was investigated to present ways to prevent or min- twice in each process of A and B. The rolling method used
imize the occurrence of side cracks. The kind of slabs and hot in this study was a conventional rolling composed of both
rolling conditions were varied, and the resulting microstruc- rough rolling and finish rolling [7], and the detailed condi-
tures were investigated in order to discuss the effects of tions of reheating and hot rolling of the A and B processes are
microstructural factors on the side cracking. listed in Tables 2 and 3. Comparison of the preheating condi-
tions of the A and B processes showed that the holding time
in a furnace in the B process (3 h and 55 min) was slightly
2. Experimental shorter than in the A process, since the furnace temperature
was kept relatively high and the preheating furnace temper-
The slabs used in this study were 250 mm thick, and man- ature abruptly increased to 1020 ◦ C. The holding time in the
ufactured at Dillinger Hütte, Dillingen, Germany, by contin- A process was longer (4 h and 27 min), as the slab temper-
uous casting, and the chemical compositions and dimensions ature increased relatively slowly and the preheating furnace
of the slabs and plates for the processes ‘A’ and ‘B’ are temperature was 621 ◦ C. In the both A and B processes, the
shown in Table 1. Generally, the carbon content has no sig- rolling temperature was about the same, but the rolling load
nificant influence on the hot ductility of steels. However, it in the B process was higher than that in the A process at
is well established that susceptibility to cracking occurs in all passes. Since the rolling reduction during the final finish
the carbon range from 0.10 to 0.16% because of the influ- rolling (passes 10, 11 and 12) of the B process was consid-
ence of the peritectic reaction in producing large austenite erably higher than that of the A process, finer grain size and
grains, together with concomitant poor ductility [4–6]. The more excellent mechanical properties were expected.
final thickness of the plates was decided to be 15–20 mm at A sketch of the side cracking spots and the orientation
which the side cracking was reported to occur frequently. In is presented in Fig. 1(a), and a photograph showing typical
hot-rolled strips or thin plates (<16 mm), side cracks result- side cracks are shown in Fig. 1(b). Side cracks are observed
ing from slab cracks are less prevalent as the crack depth in both of the plate sides and in both the top and bottom
becomes shallower with increasing rolling reduction. The of the plate surface, and all the cracks are parallel to the
size and chemical composition of the slabs and plates used rolling direction. Most of them are fine thread-shaped small
in both processes do not show much difference. So as to cracks, but some are large cracks of sub-millimeters in depth.
examine the effects of scarfing before hot rolling on the side Microstructures of the center and side regions of the cracked
cracking, the two slabs were equally divided into eight parts, plates were observed by an optical microscope and a scanning
Table 2
Reheating conditions
Hot rolling Preheating furnace Heating furnace no.1 Heating furnace no.2 Heating furnace no.3 Homogenization Extraction Holding time in
process temperature (◦ C) temperature (◦ C) temperature (◦ C) temperature (◦ C) temperature (◦ C) temperature (◦ C furnace (min)
A 621 944 1211 1223 1153 1149 267
B 1020 1150 1173 – 1170 1109 235
B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187 179
Table 3
Detailed hot rolling conditions
Rolling strand of process 1 2 3 4 5 6 7 8 9 10 11 12 13
Thickness (mm) A 223 195 177 158 138 116 94 70 48 33 26 21 17
B 231 211 190 168 146 122 100 82 65 49 34 25 17
Rolling reduction (%) A 10.8 12.6 9.2 10.7 12.7 15.9 19.0 25.5 31.4 31.3 21.2 19.2 19.0
B 7.6 8.7 10.0 11.6 13.1 16.4 18.0 18.0 20.7 24.6 30.6 26.5 32.0
Temperature (◦ C) A 1156 1151 1144 1141 1138 1134 1123 1118 1111 1096 1068 1040 1003
B 1126 1125 1116 1116 1115 1112 1101 1064 1065 1065 1058 1041 1005
Rolling force (tonnes) A 1364 1417 2038 2091 2206 2420 2764 3352 3644 3690 2932 2671 2524
B 1496 1585 3121 3227 3318 3410 3494 3593 3911 4510 4446 3348 2794
Initial slab thickness: 250 mm.
electron microscope (SEM, model; JSM-6330F, JEOL). The paratively examined to investigate the correlation between
cracked and non-cracked regions were cut perpendicular to microstructure and side cracking.
the rolling direction, and their microstructures were observed.
Inclusions of the cracked region were analyzed by energy
dispersion spectroscopy (EDS). The sectioned area of the
cracked region and that of the non-cracked region were com- 3. Results
Fig. 2. Optical micrographs of the (a) corner and (b) center regions of the slab used in the A hot rolling process.
Fig. 3. Optical micrographs of (a) and (d) the center region, (b) and (e) the region of 50 mm far from the side, and (c) and (f) the side region, showing the band
structure of ferrite and pearlite. The upper and lower parts of the figure indicate the surface and interior regions, respectively. Note the slope difference of the
band structure.
B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187 181
Table 4
Number of small side cracks formed on the plate surface
Specimena Number of small side cracks
Top part Tail part
A1 0, 0 0, 0
A2 0, 0 0, 0
A3 1, 0 0, 0
A4 0, 0 0, 0
A5 0, 3 0, 0
A6 0, 1 0, 0
A7 1, 0 0, 0
A8 0, 4 1, 0
B1 – –
B2 1, 0 1, 0
B3 1, 1 3, 1 (1)b
B4 5, 1 (1)b 1, 0
B5 1, 0 0, 0
B6 0, 1 1, 1
B7 0, 1 1, 0
B8 1, 1 1, 1
a Specimen numbers of 1–4 and 5–8 indicate the plate specimens rolled
from non-scarfed and scarfed slabs, respectively.
b Number of large side cracks.
large cracks formed on the side region of the top and tail
parts were counted, and are listed in Table 4. When many
small cracks were aggregated, they were counted as one
small crack. Most side cracks were microcracks which are
tens of millimeters long and 200 m or less deep, but large
cracks having over sub-millimeters depth were also observed
in some plates. The small and fine cracks were mostly formed
within 30 mm from the side, and the large cracks were formed
between 10 and 30 mm from the side.
In the specimens fabricated by the B process, more cracks
Fig. 4. Optical micrographs of the non-cracked side region of the steel plates were formed than in those fabricated by the A process, regard-
rolled by the (a) A and (b) B processes.
less of the scarfing treatment. Locations at the plate did not
show much difference, whether they were the top or the tail.
interior of the center region (Fig. 3a, b, d and e), it is slanted The effect of scarfing on cracking was not readily recogniz-
on the surface and in the interior of the side region (Fig. 3c able in the A specimens as the number of cracks in them was
and f). This slanted pattern is observed down to about 30 mm very few. In the case of the B specimens, the number of small
deep from the side. The slope of the ferrite–pearlite band cracks in the scarfed B5–B8 specimens was slightly reduced
structure decreases as it gets deeper from the surface, and over the number observed in the non-scarfed B1–B4 speci-
becomes almost parallel to the surface near the 1/2 thickness. mens, and no large cracks were formed in the scarfed B5–B8
Such a microstructural arrangement is observed, irrespective specimens at all. These findings indicate that the scarfing and
of hot rolling conditions. Magnified optical micrographs of rolling conditions affect the formation of side cracks.
the non-cracked side region of the plates rolled by the A and
B processes are shown in Fig. 4(a) and (b). Ferrite grains 3.3. Microstructure of small side cracks
of the plate rolled by the B process (Fig. 4b) are finer than
those of the plate rolled by the A process (Fig. 4a), and more Optical micrographs of the cross-sectional area of the
decarburization is observed on the plate surface rolled by the cracked region having fine thread-shaped small cracks are
B process. shown in Fig. 5(a–d). Unlike typical side regions without
cracks (Fig. 4a–d), the surface is rough, and the gray area
3.2. Frequency of side cracking has infiltrated deeply into the plate interior. According to
SEM micrographs of the non-cracked side regions (Fig. 6a
A total of 32 plates were fabricated by varying the condi- and b), the surface seems smooth without cracks, but near
tions of hot rolling and scarfing. The numbers of small and the surface, the gray area inhomogeneously intrudes deep
182 B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187
Fig. 5. Optical micrographs of the cracked region having small side cracks formed in the (a) A8, (b) B3, (c) B4 and (d) B8 specimens.
Fig. 6. (a) and (b) SEM micrographs of the non-cracked side region of the steel plate rolled by the A process. (c) is an EDS spectrum of the iron oxide in (a).
B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187 183
Fig. 7. (a–c) SEM micrographs of the cracked region, showing fine lined-up iron oxides infiltrated to the interior. (b) and (c) are high-magnification SEM
micrographs of the marked rectangular regions in (a) and (b), respectively, and (d) is an EDS spectrum of fine iron oxides in (c).
into the interior, just like in the cracked side region. EDS brittle, they are smashed after hot rolling, and leave grooves
analysis of these gray areas indicates that they are all iron on the surface, which look like microcracks. In some cases,
oxides (Fig. 6c). The iron oxides often form either agglom- they infiltrate into the interior, and form fine oxides sized
erates or pores in the interior (Fig. 6a). When the oxides are smaller than 5 m as shown in Fig. 7(a–c). These fine oxides
Fig. 8. (a–d) Optical micrographs of the surface region containing a large side crack in the B3 specimen. (b)–d) are high-magnification optical micrographs of
the marked ‘A’ through ‘C’ areas, respectively, in (a).
184 B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187
4. Discussion
Fig. 10. Schematic diagram showing the formation process of small side cracks during hot rolling: (a) formation of ferrite–pearlite band structure, (b) formation
of the carbon layer and iron oxide layer on the plate surface and (c) formation of small side cracks in the side regions of the plate under applied exterior loads.
small, thread-shaped cracks on the surface. Also, when the In comparison with small cracks, large cracks occurring in
rolling load continuously applies after the cracking, oxides the side region are less likely to be formed. In this study, two
are broken and infiltrated deeply into the interior in a fine large cracks were found in plates fabricated by the B pro-
particle shape, thereby leading to the formation of the line- cess. Cross-sectional observation of the cracks reveals that
up of Mn–Si-rich iron oxides in the interior (Fig. 7a–d). their direction is parallel to the surface, and that they are
When coarse oxides or oxide layers are in contact or col- about 1 mm deep, unlike in small cracks. Consequently, the
lision against side guide rolls due to the movement of plates, formation mechanism for the large crack should be inter-
they can work as crack initiation sites. Furthermore, when preted differently from the one for the small crack. The
fine oxides are dispersed along grain boundaries, cracks are large crack is formed almost parallel to the direction of the
more readily initiated. The formation process of these small pearlite band, and the hardness in some areas around the
side cracks is schematically presented in Fig. 10(a–c). C–Mn- crack is lower than other areas because of serious decar-
rich areas and C–Mn-depleted areas exist in the slab before burization. The decarburization is a phenomenon in which
hot rolling, but the lined-up ferrite–pearlite band structure is oxygen near the plate intrudes into the interior at high tem-
developed as C–Mn-rich areas are squeezed along the rolling peratures, reacts with carbon, and then is removed in CO or
direction after hot rolling (Fig. 10a). The ferrite–pearlite CO2 . As a result, the carbon concentration inside the plate
banding is generally related to the microsegregation of alloy- decreases, and the surface region consists mainly of soft
ing elements, and it can be eliminated by annealing for several ferrites as the oxidization reaction is accelerated. This decar-
hours at a high austenitization temperature [20–23]. When burization phenomenon primarily arises from oxidizing gas
this band structure aligned parallel to the surface is exposed (e.g., air, vapor and carbonic acid gas), reducing gas (e.g.,
to high temperatures and loads after hot rolling, oxidiza- hydrogen and ammonia), molten salts, or iron oxides, and
tion occurs homogeneously throughout the surface overall, it can simultaneously occur with oxidization when heated
the decarburized layer and iron oxide layer are formed in in an oxidizing atmosphere, thereby forming a black iron
homogeneous thickness on the plate surface (Fig. 10b). How- oxide layer on the surface [24,25]. The decarburization is
ever, when the band structure is slanted or almost vertical a process in which the carbon inside steels is removed
to the surface, oxidization proceeds selectively along the as the exterior oxygen reacts with the carbon diffused to
band structure, and the iron oxide layer is inhomogeneously the surface. The detailed chemical reaction is as follows
infiltrated deep into the interior. As the iron oxide layer is [25,26]:
brittle, it can easily develop into cracks under an applied load
Fe(C) + O2 → Fe + CO2
(Fig. 10c). The final shape of small cracks occurring in the
side region can be identified in Figs. 5(a–d) and 6(a–d). Fe(C) + CO2 → Fe + 2CO
186 B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187
As a result of this decarburization, mechanical proper- detailed microstructural variations of plates, and in investi-
ties deteriorate because of insufficient quenching hardness or gating the difference in the formation mechanism of oxides
decreased carbon concentration in the decarburized region. and in the plastic deformation due to temperature distribution
Deformation or cracking can take place when tensile stress in the plate width and thickness. Furthermore, more funda-
develops on the steel surface since the martensite start point mental understanding of the cracking mechanism is required
of the decarburized region is higher than that of the non- [27–31], as the arrangement and size of grains and oxides
decarburized region in the interior. Consequently, the decar- greatly vary with the location of the side region. In order to
burized microstructure near the large crack may have been clarify the microstructure, oxide shape and cracking mecha-
present near the surface before the crack formation. nism more in depth in the future, efforts are to be made on
In the specimens fabricated by the B process, more side following areas: (1) detailed analysis of oxides using trans-
cracks take place than in those by the A process. This can mission electron microscopy, (2) simulation test of hot rolling
be interpreted by microstructural differences resulting from of slabs, (3) microstructural observation of various slabs and
different hot rolling conditions. According to the final rolling plates and (4) evaluation of the cracking frequency according
reduction at the passes 10, 11 and 12 in Table 3, the B pro- to the plate location and shape.
cess applies considerably higher rolling reduction than the A
process. Under the higher rolling reduction during final finish
rolling, the final grain size can decrease because the growth 5. Conclusions
of austenite grains is considerably prevented [7]. Thus, the B
specimens having more refined grains than the A specimens Based on microstructural analysis of the side cracking phe-
may have more excellent properties. This difference in grain nomenon occurring during hot rolling of thick low-carbon
size may be related to the formation of cracks. As the fine- steel plates, following conclusions were reached.
grained B specimens have a larger grain boundary area than (1) Observation of the microstructures in the center and side
the A specimens, which works as a good path for oxidization regions of steel plates showed that the ferrite–pearlite
or decarburization reactions at high temperatures, active oxi- band structure was arranged parallel to the surface in
dization or decarburization takes place in the B specimens. As the center region, whereas it was seriously slanted to the
a result, the B specimens undergo more irregular or serious surface in the side region. The slope of the band structure
oxidization on the surface than the A specimens, and have decreased as it got into the center region or the interior
more of small and large cracks in the side region. from the side.
In this study, the formation mechanism of side cracks (2) Small cracks typically occurring in the side region were
occurring during hot rolling in low-carbon steel plates was formed when the brittle iron oxide layer inhomoge-
investigated in terms of microstructures and rolling condi- neously infiltrated into the interior after the ferrite–
tions. It was found that the size, shape and arrangement of pearlite band structure was arranged to be slanted or
iron oxides and other microstructures formed during reheat- vertical to the surface after hot rolling and oxidization
ing and hot rolling significantly affected the side cracking. occurred selectively along the ferrite–pearlite band struc-
Based on these findings, following solutions can be sug- ture.
gested to prevent or minimize the side cracking phenomenon: (3) Large cracks were formed in the case of material inhomo-
(1) minimize the segregation of C and Mn in slabs by suf- geneity or insufficient homogenization during the reheat-
ficiently homogenizing slabs at high temperatures, (2) make ing process. Since the C–Mn-rich region aggregated near
the microstructural arrangement of the ferrite–pearlite struc- the plate surface was harder than the region nearby, the
ture located in the side region as parallel to the surface as large cracking could occur when the surface was decar-
possible through appropriate controlling of the hot rolling burized, folded, and then intruded into the interior during
conditions such as modified materials design to minimize hot rolling.
the broad ratio (final plate width to initial slab width), (3)
prevent or minimize the formation of iron oxides by mini-
mizing the exposure time to high temperatures and (4) even Acknowledgments
in the presence of the oxide layer, prevent the fall-off of
oxides or the adherence of cracks resulting from excessive The work was supported by Technology Innovation Center
edge works such as mechanical friction or impact by prop- for Metals & Materials (TICM) funded by the Ministry of
erly adjusting the spacing between plates and side guide rolls. Commerce, Industry and Energy (MOCIE) of Korea.
The results of this study interpreting the crack formation
behavior in terms of microstructures and fabrication process
conditions are expected to be used as important experimen- References
tal data for studies to prevent the side cracking. However,
[1] J.B. Song, S.Y. Im, I.H. Lee, Steel Knowledges, The Korean Institute
since this study is mainly concerned with comparative inter- of Metals and Materials, 2001 (Chapter 3).
pretation of the qualitative and phenomenal data from the [2] H. Suzuki, S. Nishimura, J. Imamura, Y. Nakamura, Tetsu-to-Hagane
cracked and non-cracked regions, it lacks in analyzing the 67 (1981) 1180.
B. Hwang et al. / Materials Science and Engineering A 402 (2005) 177–187 187
[3] Y. Maehara, K. Yasumoto, Y. Ohmoni, High Temp. Tech. 4 (1986) [19] Y.H. Kim, S.C. Lee, Y.J. Choi, J.H. Lee, Y.D. Lee, in: S.M.
13. Hwang, J.J. Lee (Eds.), Proceedings of the Fourth Rolling
[4] R.J. Gray, A. Perkins, B. Walker, Proceedings of the International Symposium—Rolling 2001, Korean Institute of Metals and Mate-
Conference on Solidification, 1979, p. 300. rials, Jeju, Korea, 2001, p. 500.
[5] E. Takeuchi, J.K. Brimacombe, Metall. Trans. B 16B (1985) 605. [20] M. Matsuda, H. Miura, Met. Mater. Int. 9 (2003) 537.
[6] Y. Maehara, K. Yasumoto, Y. Sugitati, K. Gunji, Trans. ISIJ 25 [21] S.E. Offerman, N.H. van Dijk, M.Th. Rekveldt, J. Sietsma, S. van
(1985) 1045. der Zwaag, Mater. Sci. Tech. 18 (2002) 297.
[7] I. Tamura, H. Sekine, T. Tanaka, C. Ouchi, Thermomechanical Pro- [22] B.-S. Kim, B.-G. Kim, H.-W. Lee, W.-S. Chung, Met. Mater. Int. 8
cessing of High-strength Low-alloy Steels, Butterworth & Co., Ltd., (2002) 367.
1988. [23] P.E.J. Rivera-dı́az-del-castillo, J. Sietsma, S. van der Zwaag, Metall.
[8] E. Ervasti, U. Stahlberg, J. Mater. Process Tech. 94 (1999) 141. Mater. Trans. A 35A (2004) 425.
[9] S.-I. Kim, Y.-C. Yoo, Met. Mater. Int. 8 (2002) 7. [24] G. Bandel, Stahl Eisen 58 (1938) 1317.
[10] M.H. Han, S. Lee, N.J. Kim, K.J. Lee, T. Chung, G. Byun, Mater. [25] E.T. Turkdogan, Physical Chemistry of High Temperature Technol-
Sci. Eng. A A264 (1999) 47. ogy, Academic Press, 1980 (Chapter 7).
[11] H. Fujii, T. Ohashi, T. Hiromoto, Tetsu-to-Hagane 62 (1976) 1813. [26] D.R. Gaskell, Introduction to the Thermodynamics of Materials, Tay-
[12] K. Brimacombe, K. Surimachi, Metall. Trans. B 8B (1977) 489. lor & Francis, 1995.
[13] S. Lee, J.W. Rhyu, K.M. Cho, J. Duffy, Metall. Trans. A 24A (1993) [27] A.J. McEvily, Metal Failures—Mechanism, Analysis, Prevention,
901. John Wiley & Sons Inc., 2002.
[14] J.H. Kwak, J.H. Chung, K.M. Cho, Mechanical Working and Steel [28] H.N. Han, C.-S. Oh, D.W. Suh, C.G. Lee, T.-H. Lee, S.-J. Kim, Met.
Processing Conference Proceedings, vol. 38, 2000, p. 311. Mater. Int. 10 (2004) 221.
[15] Y.-J. Seok, J.-K. Yoon, Met. Mater. Int. 8 (2002) 543. [29] C.-S. Oh, H.N. Han, C.G. Lee, T.-H. Lee, S.-J. Kim, Met. Mater.
[16] G.E. Dieter, Mechanical Metallurgy, third ed., McGraw-Hill, 1986 Int. 9 (2004) 399.
(Chapter 7). [30] B. Hwang, Y.G. Kim, S. Lee, N.J. Kim, J.Y. Yoo, Metall. Mater.
[17] W.F. Hosford, R.M. Caddell, Metal Forming, second ed., Prentice- Trans. A 36A (2005) 371.
Hall International, 1993 (Chapter 7). [31] M. Thompson, M. Ferry, P.A. Manohar, ISIJ Int. 41 (2001)
[18] A. Gittins, J. Aust. Int. Met. 20 (1975) 184. 891.