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Method 6.
1.1 Analytes.
determined separately.
stack. The H2SO4 and the SO2 are separated, and both
titration method.
4.0 Interferences.
5.0 Safety.
5.2.
bottles, 500-ml.
be done).
737
sample analysis:
125-ml size.
Section 7.1.3.
Transport.
not be weighed.
739
Section 8.2.
performance of Method 8.
these weights. Weigh also the silica gel (or silica gel
samples as follows:
weights. Also, weigh the spent silica gel (or silica gel
between the filter and silica gel impinger with water, and
Quality Control
Section Measure Effect
7.1.3 Isopropanol check Ensure acceptable level
of peroxide impurities in
isopropanol
8.4, 8.5, Sampling equipment Ensure accurate
10.1 leak-check and measurement of stack gas
calibration flow rate, sample volume
10.2 Barium standard Ensure normality
solution determination
standardization
11.2 Replicate titrations Ensure precision of
titration determinations
11.3 Audit sample Evaluate analyst's
analysis technique and standards
preparation
Section 9.2.
Section 10.0.
Section 10.5.
enforcement authority.
affected facility.
mg/dscm.
mg/dscm.
g/dscm (lb/dscf).
percent
where:
where:
Section 12.11.
750
impingers.
16.0 References.