UNIT I ELECTRO CHEMISTRY Introduction to electrochemistry Types of conductors Types of electrolytes Cell terminology Electrochemical cells (or) galvanic

anic cells Daniel cell Representation of a galvanic cell Reversible and irreversible cells EMF of a cell Measurement of emf of a cell Single electrode potential(E) Standard electrode potential(E0) Nernst equation for electrode potential Problems based on nernst equation Reference electrodes(or) standard electrodes Primary reference electrode o Standard hydrogen electrode Secondary reference electrode o Standard calomel electrode Types of electrodes Glass electrode(internal reference electrode) Determination of PH of a solution using glass electrode Ion selective electrodes (ISE) Describtion Types of ion selective electrodes o Glass membrane electrode o Solid state membrane electrode o Liquid membrane electrode o Heterogenous membrane electrode o Enzyme electrode Determination of concentration of a metal ion using ISE Application of ISE Limitations Electro chemical series Definition Significance(or) applications of electrochemical series Potentiometer titrations Redox titration Precipitation titration Conductometric titrations Acid base titrations.

ENGINEERING CHEMISTRY II NOTES ON LESSON

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UNIT II CORROSION AND CORROSION CONTROL Introduction to corrosion and its types Chemical corrosion(dry corrosion) o Pilling -Bedworth rule o Mechanism of chemical corrosion o Corrosion by oxygen o Corrosion by hydrogen o Liquid metal corrosion Electro chemical corrosion (wet corrosion) o Mechanism of electrochemical corrosion o Evolution of hydrogen type o Absorption of oxygen type o Difference between chemical corrosion and electrochemical corrosion types of electrochemical corrosion galvanic corrosion differential aeration(or) concentration cell corrosion factors influencing the rate of corrosion nature of the metal nature of the environment corrosion control control of corrosion by modifying the metal by cathodic protection o sacrificial anodic protection method o impressed current cathodic protection method by modifying the environment corrosion inhibitors anodic inhibitors cathodic inhibitors vapour phase inhibitors protective coatings types of protective coatings paints constituents and their functions of a paint mechanism of drying of drying oil metallic coatings hot dipping electroless plating electro plating anodization

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UNIT III FUELS AND COMBUSTION Introduction, analysis of coal The proximate analysis o Determination of moisture in coal o Determination of volatile matter in coal o Determination of ash in coal o Determination of fixed carbon The ultimate analysis o Determination of carbon and hydrogen in coal o Determination of hydrogen o Determination of nitrogen o Determination of sulphur in coal o Determination of oxygen in coal Metallurgical coke Characteristics of metallurgical coke Manufacture of metallurgical coke by Otto Hoffmanns method Petroleum of gasoline Processing and fractions Cracking catalytic cracking Knocking Octane number Cetane number Synthetic petrol Bergius process (hydrogenation of coal) Fisher- Tropsch process Gaseous fuels Water gas Producer gas Compressed natural gas ( CNG) Liquefied petroleum gas (LPG) Biogas Calorific value Units of calorific value Determination of calorific value Gross calorific value and net calorific value Theoretical calculations of calorific values Flue gas analysis: Orsats apparatus

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UNIT IV PHASE RULE AND ALLOYS Introduction, explanation of terms involved Phase Component Degree of freedom Phase diagram Phase rule One component system Water system Condensed phase rule Two component system Simple eutectic systems (Binary alloys) Lead silver system Construction phase diagram by thermal analysis Copper nickel alloy system Alloys Purpose of making alloys Classification of alloys Ferrous alloys Nichrome Stainless steel Non ferrous alloys Brass Bronze Heat treatment of steel Hardening (quenching) Tempering Annealing

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UNIT V ANALYTICAL TECHNIQUES Explanation of terms used in absorption spectra Beers lamberts law Problems UV and visible spectroscopy Principle Instrumentation (block diagram only) Problems IR spectroscopy Principles Instrumentation (block diagram only) Problems Colorimetric estimation of few metal ions Estimation of iron Flame photometry Principle Instrumentation (block diagram only) Estimation sodium by flame photometry Atomic absorption spectroscopy Principle Instrumentation (block diagram only) Estimation of nickel by atomic absorption spectroscopy.

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