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Journal of Materials Processing Technology 132 (2003) 49–57

Effect of hybridisation on crushing behaviour of carbon/glass


fibre/epoxy circular–cylindrical shells
E. Mahdia, A.M.S. Hamoudab,*, B.B. Saharib, Y.A. Khalidb
a
Aerospace Engineering Department, Faculty of Engineering, University Putra Malaysia, 43400 UPM, Serdang, Selangor, Malaysia
b
Mechanical and Manufacturing Engineering Department, Faculty of Engineering, University Putra Malaysia,
43400 UPM, Serdang, Selangor, Malaysia
Received 17 October 2000; received in revised form 6 March 2002; accepted 1 May 2002

Abstract

This study concentrates on the effect of hybridisation on the crushing behaviour, energy absorption and failure mechanism and mode for
composite cylinders. The static crushing behaviour of filament wound laminated (FWL) circular–cylindrical composite shell under uniform
axial load has been investigated experimentally. Five different hybrids and non-hybrid FWL circular–cylindrical composite shell containing
carbon and glass fibres were fabricated. Five types of composites were tested, namely, carbon fibre/epoxy, glass fibre/epoxy, carbon–glass–
glass/epoxy, glass–carbon–glass/epoxy and glass–glass–carbon/epoxy. Failure modes were examined using the photographs taken during the
different crushing stages for each specimen. Failure modes were highly dominated by the effect of hybridisation. The results also showed that
the structure with material sequence of glass–carbon–glass/epoxy exhibited good energy absorption capability.
# 2002 Published by Elsevier Science B.V.

Keywords: Circular–cylindrical composite shell; Hybridisation; Material sequence; Specific crushing energy; Filament wound laminated; Crushing
behaviour; Splaying mode

1. Introduction viour of hybrid circular shell made of at least two types of


fibre reinforced polymeric matrix (i.e. hybridisation). The
The automotive industry is one of the four largest markets main reason for using hybridisation is the ability to combine
for composite materials. Rigorous confirmations are arising the two or more types of reinforcement in such a way as to
from extensive experimental and theoretical investigations tailor the material to exact needs of structural applications
that high performance composites have a capability to [8]. Based on the fact that advantages found with one type
absorb high energy in fracture mechanism [1]. Most of fibre can be used to complement the poor performance
research in the past has focused the attention to the crushing of other type for particular property, the crushing behaviour
behaviour of non-hybrid shell composites [2–5]. An exten- of structure made of carbon fibre reinforced polymer com-
sive study on crushing behaviour of fibre reinforced com- posite can be optimised by hybridisation with glass fibre
posite material has been carried out by Hull [6]. From that reinforced polymer composite. Chiu et al. [9] studied
work, it was found that the composite materials absorb high experimentally the crush failure modes of two-dimensional
energy, despite that the failure mechanism was fracture at triaxially braided hybrid composite tubes. They employed
the surface rather than plastic deformation. Christoforou the quasi-static axial compression to investigate the effect of
and Swanson [7] studied the problem of strength loss in hybridisation. They observed that the crush failure modes
composite structures due to impact. It appears that the value and energy absorption of the braided composite tubes were
of load is highly affected by the crushing distance. Their strongly influenced by the fibre types used and their hybrid
model is based on Fourier series expansion to calculate ply kind. Generally, all the energy absorption data generated up
stress and strains. However, the practical requirements to date have been developed for axial collapse of non-hybrid
claim for additional and essential work on crushing beha- circular–cylindrical composite shells. On the other hand,
research work to generate energy absorption data for axial
*
Corresponding author. Tel.: þ603-948-6101-2083; collapse of hybrid circular–cylindrical composite shells is
fax: þ603-8948839. still young and few. This is main reason for carrying out this
E-mail address: hamouda@eng.upm.edu.my (A.M.S. Hamouda). work.

0924-0136/02/$ – see front matter # 2002 Published by Elsevier Science B.V.


PII: S 0 9 2 4 - 0 1 3 6 ( 0 2 ) 0 0 2 6 0 - 1
50 E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57

Fig. 1. Schematic diagram for filament winding process.

This paper describes the investigation carried out on cured FWL cylindrical composite shells were then extracted
carbon/glass hybrid composite circular–cylindrical shells. from the wooden mandrel using the Instron digital-testing
The main aim of this paper is to evaluate the effect of machine model 8500. The maximum extraction force was
hybridisation and reinforcement sequence on the crushing found to be 0.01% of the initial failure load.
behaviour as well as on the energy absorption of circular–
cylindrical shells.
3. Geometry and material

2. Fabrication process of FWL composite cylinder A total of 15 specimens of FWL glass/carbon hybrid
cylindrical shells were tested in uniaxial compression.
The wet filament winding process was used to fabricate The description and material sequence of FWL carbon/
the specimens of the filament wound laminated (FWL) glass/epoxy hybrid cylinder are shown in Table 1 and
cylinder and cone composite shell. The fibre is passed Fig. 2, respectively. The average volume fraction of glass
through a resin bath, causing resin impregnation. This is fibres and carbon fibres is 0.52 and 0.56, respectively. All the
followed by the application of wet fibre to the wooden specimens were of 110 mm height, 100 mm outer diameter
mandrel to form the FWL composite shells. The schematic and 3 mm wall thickness (see Fig. 3).
process is shown in Fig. 1. The winding parameters (e.g.
winding tension, winding speed, resin content, resin mixing
time and winding time between layers) are maintained at 4. Test procedure
constant level during the fabrication period of the 15
cylindrical composite shells. The fabricated FWL cylindri- Static crushing tests were carried out using an Instron
cal composite shells were cured at room temperature (32 8C) 8500 digital-testing machine with a full-scale load range of
for 24 h to provide optimum hardness and shrinkage. The 250 kN. Load platens were set parallel to each other prior to

Table 1
Description of FWL carbon/glass/epoxy hybrid cylinder

Inner (908) Middle (558) Outer (908) Base diameter (D1) (mm) Height (HTOT) (mm) Wall thickness (mm)

C C C 100 110 3
G G G 100 110 3
G G C 100 110 3
G C G 100 110 3
C G G 100 110 3
E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57 51

Fig. 2. Material sequence of FWL carbon/glass hybrid circular–cylindrical shell.

Fig. 3. Notation used for the FWL carbon/glass hybrid circular–cylindrical shell.

the initiation of the test. The entire FWL glass/carbon hybrid the material condensation process takes place and the load
cylinder shell specimens were compressed 0.95% at a strain increases sharply to the final crushed stage.
rate of 1.524 s. The load and displacement were recorded by
an automatic data acquisition system. Three tests were
performed on each type of specimens. 6. Crushing process

All the specimens were crushed progressively from one


5. Load–displacement of G/C hybrid end by splaying mode. In the crushing process, the axial load
circular–cylindrical shells increased linearly up to the initial failure, where micro-
fragmentation was observed at the top portion of the CGG
The typical load–displacement curves are presented to and GGC (see Figs. 5 and 6), while the micro-fragmentation
exemplify the effect of reinforcement sequence on the was observed at the bottom portion of the GCG (see Fig. 7).
crushing behaviour of C/G hybrid circular–cylindrical com- This mainly attributed to the reinforcement sequence. In
posite shell as shown in Fig. 4. Load–displacement curve general, the crushing process, of FWL glass/carbon hybrid
shows a linear relation up to the initial failure stage. After composite circular–cylindrical shell, is dominated by the
that, the load falls sharply, where a micro-fragmentation was interlaminar cracks propagating between the layers in the
observed at the two end parts of the cylinders. After the first crushed zone forming lamina bundles. The lamina bundles
reduction of load, the load fluctuates constantly with sharp resist the applied loads and fall down when the volume of the
peaks and troughs increasing with displacement. After that lamina bundles reaches a critical value. Some specimens
52 E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57

Fig. 4. Load–displacement curve for the FWL carbon/glass hybrid circular–cylindrical shell.

exhibit a change in the crushing mode. They begin to crush failure zone acts as a low modulus zone causes the load to
in a fracture mode at the top end (at fixed end) then change to drop sharply. This is in qualitative agreement with the load–
shear failure around the middle portion of FWL glass/carbon displacement curve. Two crushing patterns were observed
hybrid composite circular–cylindrical shell. This change in and described in the proceeding paragraphs.
crushing mode results in a significant load drop. For the CGG cylinder, as the load picked up again, after
the initial failure, the FWL hybrid composite cylinder shell
wall expanded outward and cracked. The interface delami-
7. Failure mode of G/C hybrid circular–cylindrical nation between the carbon layer and the glass fibre layer is
shells increasing slowly with increasing load level as shown in
Fig. 8. Thereafter, shear failure mode, interlaminar crack
All the specimens were first crushed at both ends of the and delamination mode interact together to form the non-
cylinder in transverse cracking splaying mode failure. The linear behaviour of the specimens. On the other hand for the
E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57 53

Fig. 5. Typical crushing history of FWL CGG under axial compressive load.

Fig. 6. Typical crushing history of GGC under axial compressive load.

GCG cylinder, as the platen moving upwards the failure due to transverse shear, while the glass layers were debonded
mode changed into transverse cracks at the middle section of due to matrix failure as well as fibre breakage as shown in
the cylinder. Splitting the cylinder into two approximately Fig. 10.
equal segments as shown in Fig. 9 has advanced the trans-
verse cracks. These segments were forced by the axial load
to slide in each other. As the load increased the glass layers 8. Crushing energy absorption of G/C hybrid
fractured due to transverse and axial shear cracks, and the circular–cylindrical shells
carbon layers were buckled and bent inward due to the axial
force. For the GGC, as the platen moves upward, the failure The energy absorbed during the crushing process is the
mode changed into transverse cracks at the middle section of area under load–displacement curve. However, using the
the cylinder. The transverse cracks are highly evolved by area for comparing the energy absorption capability of
splitting the cylinder into two segments. These segments different structures is misleading for many composite struc-
were forced by the axial load slide into each other. As the ture problems. Therefore, the specific crushing energy (ES)
load increased the carbon layers fractured and bent outward which is independent of the structure geometry was used for

Fig. 7. Typical crushing history of FWL GCG under axial compressive load.
54 E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57

Fig. 8. Optical micrograph of a section through the crush zone for CGG at initial crushing with magnification of 100 mm.

comparing the energy absorption of the FWL glass/epoxy, where


carbon/epoxy and the hand laid up oil palm frond fibre/
epoxy cylindrical shells. Specific crushing energy (ES) is A ¼ 14 pD21 (2)
obtained by using the equation:
 is the mean crush load obtained by averaging the crushing
P
P
ES ¼ (1) loads over the crush displacements through the stable load–
Ar displacement stage.

Fig. 9. Optical micrograph of a section through the crush zone for GCG at initial crushing with magnification of 100 mm.
E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57 55

Fig. 10. Optical micrograph of a section through the crush zone for GGC at initial crushing with magnification of 100 mm.

The density of circular–cylindrical shells is calculated by The volume occupied by the circular–cylindrical shell
using the equation: before crushing can be calculated as the product of cross-
section area and the total height (HTOT).
M The specific crushing energy absorption Es of three glass/
r¼ (3)
V epoxy and carbon/epoxy FWL hybrid composite cylinder

Fig. 11. Initial (ICL), average (ACL) failure load, specific crushing energy (SCE) and structural volume reduction (SVR) of the FWL carbon/glass hybrid
circular–cylindrical shell.
56 E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57

Table 2
Crush loads specific energy absorption and structural volume reduction of FWL glass/carbon hybrid composite circular–cylindrical shells

Specimen type Initial crushing failure load Mean crushing failure load Specific energy absorption Structural volume reduction

PICL (kN) S.D. (%) PMCL (kN) S.D. (%) ES (kJ/kg) S.D. (%) VR (%) S.D. (%)

CCC 156.00 1.45 64.00 1.23 29.00 2.54 78.0 3.43


GGG 71.00 1.20 45.00 1.65 24.00 2.48 93.0 3.09
CGG 59.26 1.85 45.20 2.23 18.86 2.56 83.07 3.08
GGC 33.40 1.64 22.26 2.05 9.29 2.36 85.47 2.83
GCG 92.68 1.44 62.52 1.51 26.09 1.73 71.39 2.08

Fig. 12. Ratio between the initial and average crush loads.
E. Mahdi et al. / Journal of Materials Processing Technology 132 (2003) 49–57 57

shell has been obtained and presented in Fig. 11 and listed in crushing behaviour as well as the energy absorption of the
Table 2. The GCG shells have been observed to exhibit the hybrid composite circular–cylindrical shells. From the
highest Es value of 26.087 kJ/kg, while the CGG and GGC energy absorption capability point of view, GCG seem to
have Es values of 18.86 and 9.29 kJ/kg, respectively. stand higher compressive load other when compared to the
other types of cylinders tested. This is due to the fact that the
interface of this reinforcement sequence is more adequate
9. Structural volume reduction of G/C hybrid than the CGG and GGC.
circular–cylindrical shells

Reduction in volume or space occupied by the glass/epoxy 12. Conclusion


and carbon/epoxy/epoxy FWL hybrid composite cylinder
shell is found to be significant. The structural volume reduc- Glass/carbon FWL hybrid circular–cylindrical shells
tion (VR) has been evaluated and seems to fall between were fabricated. Static crushing tests of FWL C/G hybrid
85.47% for GGC, and 71.39% for GCG. It was also noticed circular–cylindrical shells were conducted to study the effect
that GCG shows high stiffness value and as the stiffness of hybridisation and the reinforcement sequence on the
increases the structural volume reduction (VR) decreases. crushing behaviour and energy absorption. Based upon
The results of specific crushing energy, structural volume the test results the following remarks can be made:
reduction, initial crushing failure and mean crushing failure
1. The static crushing behaviour of FWL C/G hybrid
load were plotted in Fig. 11 and listed in Table 2.
circular–cylindrical shell is strongly affected by the
reinforcement sequence.
2. GCG exhibited good energy absorption capability
10. The effect of hybridisation on crush failure loads
compared to CGG and GGC.
3. The transverse crack created caused a catastrophic drop
The high stiffness–weight ratio of composites makes them
in load–displacement curve.
potentially attractive up to initial failure stage. The initial
4. Volume reduction has also been investigated and found
crush failure loads of circular–cylindrical composite shells
to be significant.
were calculated and given in Table 2. The values obtained
5. As the stiffness increases for the composite shells tested,
show that the CCC specimen has the largest value of 156 kN
the volume reduction reduces.
followed by GCG specimen, which has a value of 96 kN.
The two lowest initial crush failure loads noticed were for
the GGC and CGG, respectively. In general, the initial crush References
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