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(
= +
(
= +
. (2)
As long as the specimen is not punctured or totally
fractured, and as long as the specimen remains in
contact with the tup, the specimen displacement will
be equal to x t ( ).
The LabVIEW
tot
Fig. 6. Two representative impact tests, one showing
brittle response and one showing ductile response.
TAM 224/CEE 210 Impact Testing and Fracture Toughness 95
Charpy impact
The long-established Charpy impact test is a
relatively inexpensive and standardized way to test
materials (primarily metals) to rapid failure in bend-
ing. Charpy results, like the newer plate-penetration
results, are useful for comparative purposes.
It has been found that body-centered-cubic
materials, such as steel at ordinary temperatures,
exhibit a brittle-to-ductile transition (BDT) tem-
perature below which they absorb very little energy
and above which they absorb considerable energy
(Fig. 7). Face-centered-cubic materials, such as stain-
less steel and aluminum, generally do not exhibit a
noticeable BDT. (See, for example, Askeland (1989) or
Flinn and Trojan (1990) for additional details.)
9A.7. Analysis of Results
Plate penetration
1. For each polymer tested, plot the values of maxi-
mum load and total absorbed energy as functions
of test temperature. Use linear graph paper for
this purpose.
2. Sketch the probable dependence of maximum load
and absorbed energy on temperature.
Charpy impact
3. Using data points on linear graph paper, plot
energy absorbed (in joules) as a function of
temperature (in C) for the samples tested. If the
Charpy specimen dimensions are significantly
different from the standard values, make an
appropriate notation on the plot.
4. Sketch the probable dependence of energy
absorbed as a function of temperature, extrapo-
lating to slightly higher and lower temperatures
than those actually used in the lab. Keep in mind
that the minimum energy that can be absorbed is
zero; the maximum energy that can be absorbed is
the initial potential energy WH of the impactor,
which in the standard Charpy impact test is 358 J
(264 ftlb).
9A.8. Points for Discussion
Note.Your lab instructor will indicate which of the
following questions are to be addressed in your report.
Plate penetration
1. Compare the energy absorbed, the maximum
load, the time to failure, and the type of fracture
for the different samples at the various
temperatures. (Refer to your sketches of the failed
samples.) What can be said about the ductility of
each polymer tested?
2. State whether the glass-transition temperatures for
your materials appear to be within the range of
temperatures considered in this laboratory. If so,
what is your estimate of their values? If not, then
is the glass-transition temperature higher than
your highest temperature or lower than your
lowest one?
3. State how the temperature dependence of
absorbed energy correlates with the published
values of glass-transition temperature T
g
for your
polymers. (See accompanying table.)
4. Is there any correlation between T
g
and fracture
toughness for a polymer? (See table above.)
5. Compare the impact velocity and resulting
FCC
BCC
E
n
e
r
g
y
a
b
s
o
r
b
e
d
Temperature, T
T
BDT
0
Brittle
Ductile
Fig. 7. Brittle-to-ductile transition.
T
g
E
K
IC
Abbr. Polymer
name
C GPa MPa
m
ABS Acrylonitrile-
butadiene-
styrene
copolymer
80 2.1
HDPE High-density
polyethylene
7 0.75 25
LDPE Low-density
polyethylene
3 0.2 12
PMMA Polymethyl-
methacrylate
105 3.3 1.6
PP Polypropylene 27 1.3 3.5
96 Behavior of Engineering Materials TAM 224/CEE 210
absorbed energy for the polymer tested at two
different heights. How is the ductility of the
polymer related to strain rate?
6. If epoxy samples were used, then they consist of a
resin mixed with varying amounts of flexibilizer
and a curing agent. Suggested ratios of resin and
flexibilizer are shown in the following table for
each type of sample:
The thin discs (Fig. 2) of each epoxy composition
are fabricated by pouring the appropriate resin
mixture into a circular mold at room temperature
and then curing at an elevated temperature
(typically 70C) for one hour.
Compare the energy absorbed, the maximum
load, the time to failure, and the type of fracture
for the different flexibilizer concentrations. (Refer
to your sketches of the failed samples.) What can
be said about the ductility of each epoxy tested?
Charpy impact
7. For each of the materials tested, is there a
noticeable brittle-to-ductile transition? If so, esti-
mate the BDT temperature. How is the nature of
the fracture surface related to the test temperature,
within the range of temperatures used?
8. If 6061-T6 aluminum was used in your test, would
you expect 7075-T6 aluminum to behave in a
similar fashion? (Or, if 7075-T6 was used, would
you expect 6061-T6 to behave similarly?)
Consider such aspects as maximum load, energy
absorbed, time to failure, and BDT temperature.
9. Determine whether your instrumented Charpy
tests were conducted under standard conditions
for the Charpy test.
9A.9. References
Plate penetration
American Society for Testing and Materials. 1986.
Standard test method for high-speed puncture
properties of plastics using load and displacement
sensors. ASTM Standard D 376386. Philadel-
phia: ASTM.
Ashby, M. F., and D. R. H. Jones. 1986. Engineering
Materials 2An Introduction to Microstructures,
Processing and Design. Oxford: Pergamon.
Cheresh, M. C., and S. McMichael. 1987. Instru-
mented impact test data interpretation. In Instru-
mented Impact Testing of Plastics and Composite
Materials, ASTM STP 936. Philadelphia: ASTM,
9-23.
Charpy impact
Askeland, D. R. 1989. The Science and Engineering of
Materials, 2nd ed. Boston: PWS-Kent, 159-162.
Callister Jr., W. D. 2003. Materials Science and Engi-
neeringAn Introduction, 6th ed. New York:
Wiley, Section 8.6.
Flinn, R. A., and P. K. Trojan. 1990. Engineering
Materials and Their Applications, 4th ed. Boston:
Houghton Mifflin, 162-164.
Composition of epoxy samples
Sample Parts by weight
type Resin Flexibilizer
F-0 100 0
F-40 60 40
F-80 20 80
TAM 224/CEE 210 Impact Testing and Fracture Toughness 97
Table 1Plate-penetration data (Polymers)
Measurement or property Material
Name Symbol Units PMMA
Specimen dimensions and impact parameters
Specimen shape
Specimen diameter or
edge length
2b mm
Specimen thickness h mm
Crosshead height H m
Crosshead weight W N
Avail. energy (theor.) WH
J
Measurements of time to failure, maximum load, and energy absorbed
Environment
Time
t
fail
(msec)
Max.
load
P (kN)
Total
energy
(J)
Time
t
fail
(msec)
Max.
load
P (kN)
Total
energy
(J)
Impact data
Freezing water
(____C)
Sketch of fracture
surface
Impact data
Room temperature
(____C)
Sketch of fracture
surface
Impact data
Boiling water
(____C)
Sketch of fracture
surface
Test date: Group: Students name:
98 Behavior of Engineering Materials TAM 224/CEE 210
Table 2Charpy impact data
Measurement or property Material
Name Symbol Units _____ Steel __________ Aluminum
Specimen dimensions and impact parameters
Length L mm
Depth D mm
Width w mm
Notch depth d mm
Notch root radius r mm
Crosshead height H m
Crosshead weight W N
Avail. energy (theor.) WH J
Measurements of maximum load and energy absorbed
Temperature T C
Max. load
(kN)
Energy
(J)
Max. load
(kN)
Energy
(J)
Impact data
Freezing water
(____C)
Sketch of fracture
surface
Impact data
Room temperature
(____C)
Sketch of fracture
surface
Impact data
Boiling water
(____C)
Sketch of fracture
surface
Test date: Group: Students name:
TAM 224/CEE 210 Impact Testing and Fracture Toughness 99
Fracture Toughness
9B.1 Objective
The purpose of fracture-toughness testing is to
determine the value of the critical stress-intensity
value, or plane-strain fracture toughness K
C I
, of high-
strength materials. This material property is used in
the design of structural members made of high-
strength materials, which are often susceptible to
rapid fracture in loading situations that would
normally cause lower-strength materials to yield
without fracturing.
9B.2. Apparatus
An MTS 90-kN (20-kip) capacity servo-hydraulic
test frame with swivel-pin grips is used to load a
compact tension specimen that has been precracked in
fatigue. See Fig. 1. A load cell is used to measure the
load P applied to the specimen, and a clip gage is
used to measure the crack-opening displacement
(COD) of the specimen. LabVIEW
software is used
to control the test and to obtain a plot of load P versus
crack-opening displacement .
9B.3. Material
Type 7075-T6 aluminum is generally used to make
the compact tension specimen. This high-strength,
lightweight alloy is commonly used in aircraft
structures.
9B.4. Experimental Procedure
Note.The laboratory technician will normally have
the specimen installed and COD gage already attached.
1. Observe the fatigue precrack in the vicinity of the
machined crack tip of the compact tension speci-
men, using a video camera fitted to a microscope
(Fig. 1).
2. Prepare the data-acqusition system to plot load P
versus crack-opening displacement .
3. Load the specimen slowly until failure occurs,
observing the loaddeflection plot and viewing
the deformation of the specimen in the area of the
crack tip. After the specimen fails, note the
appearances of the machined surfaces, the fatigue-
precracked surface, and the final fracture surface.
Record comments in Table 3.
4. Using calipers or a micrometer, measure the speci-
men and crack dimensions, and record these data
in Table 3. See Fig. 2.
Fig. 1. Removing upper pin from a failed
compact tension specimen.
Fatigue
precrack
Thickness
=
Notch for
COD gage
d
h
a
B
w
P
P
Fig. 2. Nomenclature for a
compact tension specimen.
Specimen
910 Behavior of Engineering Materials TAM 224/CEE 210
9B.5. Theoretical Considerations
The stress-intensity factor K
I
at the tip of the
precrack in a compact tension specimen
2
is given by
K
P
B w
f
I
= ( ) , (4)
where P is the applied load, w is the specimen width
(illustrated in Fig. 2), B is the specimen thickness, and
f ( ) is a geometrical factor; denotes the ratio a w / ,
where a is the crack length (including the precrack
see Fig. 2). The function f ( ) is plotted in Fig. 3.
3
For a sufficiently large load P
Q
, the specimen fails,
and a provisional value of fracture toughness K
Q
is
calculated from Eqn. (4), i.e.
K
P
B w
f
Q
Q
= ( ) . (5)
The value K
Q
may turn out to be the critical stress-
intensity factor, or fracture toughness, K
IC
, but only if
some conditions are met.
2
The singular nature of the stress field surrounding a mode-I
loaded crack, and the visualization of this singularity using
photoelasticity, are considered in the Discussion
(Section 9B.7).
3
The ASTM (1987) formula for f ( ) is
f ( ) =
( 2 + )
(1 )
3 2
( 0.886 + 4. 64 13. 32
2
+14.72
3
5. 6
4
) .
For proper fracture-toughness testing, should be in the
range
0. 45 < <0.55 .
First of all, the correct value of P
Q
must be
established; there are three principal types of load-
versus-COD curves that are encountered, as shown in
Fig. 4. The dashed line OP
5
in the figure is drawn at
0.95 of the slope of the linear portion of the P vs.
curve. The point of intersection of this secant with the
original curve defines point P
5
. Then, point P
Q
is
determined as follows: If the load at every point on
the record that precedes P
5
is lower than P
5
, then the
loaddeflection curve is of type I, and P
Q
= P
5
; but if
there is a maximum load preceding P
5
that exceeds P
5
,
then the loaddeflection curve is of type II or III, and
P
Q
is this maximum load.
Second, the conditions for plane strain at the root
of the fatigue precrack must also be checked; if the
plastic zone size at the root of the crack is too large, as
illustrated in Fig. 5, then the state of stress is rather
more plane-stress-like than plane-strain-like, and the
apparent fracture toughness K
Q
of the material will be
larger than the actual plane-strain value K
IC
that is
sought. By analysis and experience, it has been found
that plane-strain conditions exist if the thickness B and
crack length a are sufficiently large compared with the
plastic zone size; the accepted rule (ASTM 1987) is:
2
, 2.5
Q
y
K
B a
| |
|
|
\ .
, (6)
where
y
is the yield strength of the material being
tested. If B and a meet the minimum criteria in
Eqn. (6), as they would for the specimen illustrated in
Fig. 6, then
K K
C Q I
= . (7)
0.45 0.50 0.55 0.60
6
8
10
14
12
Ratio of crack length to width, = a/w
F
u
n
c
t
i
o
n
f
(
)
a
w
P
P
Fig. 3. Plot of the function f ( ) for
a compact tension specimen.
L
o
a
d
,
P
Crack-opening displacement,
Type I Type II Type III
P = P
P
P
P
P
P
P = P
Q 5
Q
5
max max
5
Q max
O O O
Fig. 4. Types of loaddisplacement curves observed in K
IC
testing.
TAM 224/CEE 210 Impact Testing and Fracture Toughness 911
Otherwise, K
IC
< K
Q
; that is, K
Q
is an upper bound to
the true value of fracture toughness K
IC
.
9B.6. Analysis of Results
1. Compute the value = a w / , where a is the initial
crack length and w is the effective width of the
compact tension specimen. Find the value of the
geometry factor f ( ) from Fig. 3.
2. Determine the value of the critical load P
Q
from
the loaddeflection plot obtained in the labora-
tory. Determine the type (I, II or III) of the loading
curve.
3. Compute a provisional value of the critical stress-
intensity factor, K
Q
, given by Eqn. (5).
4. If the conditions in Eqn. (6) are met, then the
fracture toughness K
IC
is equal to the provisional
K
Q
. If the conditions in Eqn. (6) are not met, then
a thicker specimen (or one with a longer crack, or
both) must be used to determine K
IC
.
The uniaxial yield strength
y
of 7075-T6 alumi-
num is about 500 MPa (73 ksi), whereas the yield
strength of 6061-T6 aluminum is considerably
lowerabout 280 MPa (40 ksi), according to
Marks Handbook (1987).
Provide calculations, and state your final
conclusion(s).
9B.7. Points for Discussion
Note.Your lab instructor will indicate which of the
following questions are to be addressed in your report.
1. Discuss the features of the fracture surface of the
compact tension specimen, and correlate these
features with the condition(s) for plane-strain
fracture-toughness testing.
2. A typical loaddeflection plot is shown in Fig. 7
for a quenched and tempered 4340 steel. Analyze
the plot to determine, if possible, the fracture
toughness of this steel. Dimensions of the sample
are w = 50.8 mm (2.00 in.), a = 25.4 mm (1.00 in.),
and B = 25.4 mm (1.00 in.). Assume that the yield
strength of this 4340 steel is 1500 MPa (220 ksi).
Are the conditions for plane-strain testing met?
Fig. 5. Failed compact tension specimen of 6061-T6
aluminum, showing large shear lips and associated lack
of plane-strain conditions at the crack tip.
Fig. 6. Failed compact tension specimen of 7075-T6
aluminum, showing a flat fracture surface and
associated plane-strain conditions at the crack tip.
0 0.01 0.02 0.03 0.04 0.05
0
2
4
6
8
10
12
Crack-opening displacement, (in.)
L
o
a
d
,
P
(
k
i
p
s
)
Quenched and tempered
4340 steel
Fig. 7. Fracture-toughness loaddeflection curve
for a 4340 steel.
912 Behavior of Engineering Materials TAM 224/CEE 210
Explain your work, and include the calculations.
Give answers in both SI and U.S. customary units.
3. Consider how fracture mechanics and photo-
elasticity can be used together to investigate the
state of stress surrounding a mode-I loaded sharp
crack (Fig 8). Under plane-strain conditions, if the
stresses remain elastic, the stress distribution for a
sharp-tipped, flat crack in an infinitely large body
can be shown to be
I
3
1 sin sin
2 2
3
1 sin sin
cos 2 2
2 2
3
sin cos
2 2
2
x
y
xy
z
K
r
+
=
` `
)
)
, (8)
where
z
is the out-of-plane normal stress, and
K
I
is the mode-I stress-intensity factor. Recall that
the in-plane principal-stress difference
1 2
,
which gives rise to fringes in a photoelastic model,
can be calculated for any combination of
x
,
y
,
and
xy
from the Mohrs circle equation
2
2
1 2
2
2
x y
xy
| |
= +
|
|
\ .
. (9)
Show by combining Eqns. (8) and (9) that the
principal-stress difference for a mode-I loaded
crack is given by
1 2
2
=
K
r
I
sin . (10)
(You will need to use the double-angle formula
sin sin cos
= 2
2 2
and the fact that the square root in Eqn. (9) is
taken to be positivethat is,
1
is always greater
than or equal to
2
.)
Finally, recall from Lab 8 that the photoelastic
fringe value N is related to the principal-stress
difference by the equation
1 2
=
Nf
h
, (11)
where f
=
I
2
. (12)
This distribution is illustrated in Fig. 9. Note that
along any radial line ( = const ), the value of N
increases as 1/ r as the crack tip is approached.
4. Using Eqn. (12), determine the value of the stress-
intensity factor K
I
for the crack in the compact
tension specimen that is illustrated in Fig. 10.
Note in particular that along a vertical line
Crack
P
P
x
y
xy
r
Fig. 8. Nomenclature for stresses surrounding a
mode-I loaded crack.
Crack
P
P
x
y
N = 1
N = 2
N = 3
(etc.)
N = 0
N = 1
Fig. 9. Theoretical photoelastic fringe pattern for a
mode-I loaded crack in an infinite medium.
TAM 224/CEE 210 Impact Testing and Fracture Toughness 913
emanating from the crack tip, = / 2 and
consequently r y = . Therefore, from Eqn. (12),
K
f
h
N y
I
=
2 | | . (13)
For the PSM-1
| |
|
|
\ .
mm
Derived quantities
Fracture toughness K
C I
MPa
m
Test date: Group: Students name:
Printed 7/9/03