A SEMINAR PRESENTATION

ON

METHODS OF SYNTHESIS OF
NANOPARTICLES (NPs)
Under the guidance of
Prof. Sunil M. Badgujar
Presentation
By

ANIKET D. BAMGUDE
CONTENTS
• Introduction
• Role of different approaches in synthesis of nanoparticles
• Methods of synthesis of nanoparticles
• Characterization
• Conclusion
Introduction
• Nanoparticles are the particles whose size in between 1 to 100 µm.
Application of NPs
Different Approaches In Nanotechnology

Top-down Approach Bottom-up Approach

Creating Nano-scale materials by Assembling Nano materials atom-
physically or chemically breaking by-atom or molecule-by molecule
down larger materials (self assembling)
Method of Synthesis of Nanoparticles (NPs)
• Coprecipitation method
• Sol gel method
• Solution reduction method
• Microemulsion method
• Hydrothermal method
• Polyol method
Coprecipitation Method
Advantages of Coprecipitation Method
• Simple and rapid preparation.
• Easy control of particle size and composition.
• The process is lower temperature synthesis.
• Environmental friendly process
Sol Gel Method
Advantages of Sol Gel Method
• Simple, economic & effective
• Highly pure product form.
• Uniform nanostructure obtained.
• Low temperature preparation saving energy.
Solution Reduction Method
Advantages of Solution Reduction Method
• Simple, convenient, flexible.
• Producing metal nanoparticles like molybdenum, tungsten.
• Economical method.
Microemulsion Method
Advantages Of Microemulsion Method
• Process is simple and economic.
• Better size controlled possible in microemulsion process.
• Low process time.
Hydrothermal Method
Advantages of Hydrothermal Method
• Powder directly Obtained from the solution.
• Control particle size and shapes by using different starting materials
and hydrothermal conditions.
• Obtained highly reactive powder
Polyol Method
Advantages of Polyol Method
• Low temperature process.
• Control the properties of the particles such as size, shape and
uniformity, etc.
• Yields high purity powders.
Characterization of Nanoparticles
• Size (SEM, XRD)
• Shape (SEM)
• Crystalinity (XRD)
• Surface charge (ZPA)
• Functional group (FTIR)
Conclusion
• Extensively used in last recent years.
• Nanoparticles having wide range of application.
• Therefore scientist founding more methods to synthesis of
nanoparticles.
THANK YOU !