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Thermogravimetric Analysis (TGA) dan

Differential thermal analysis (DTA)

Kelompok 2
- Bianda Aufar
- Chofifah Fitrotul Hasanah
- Dewi Yuliani
- Desi wulandari
- Dinda farrah Firdaus

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Pengukuran sifat-sifat fisik
Analisis Thermal dan kimia material sebagai
fungsi dari suhu

Thermogravimetric Analysis Differential Thermal Analysis


(TGA) (DTA)

Teknik untuk Teknik dimana suhu


mengukur dari sampel
perubahan berat dibandingkan
dari suatu dengan material
senyawa sebagai pembanding inert
fungsi dari suhu / selama perubahan
waktu suhu terprogram
Perbedaan TGA dan DTA

TGA DTA

• Mendeteksi efek yang melibatkan • DTA dapat mendeteksi efek lainnya


hanya perubahan massa saja seperti transisi polymorfik, yang
tidak melibatkan perubahan berat.

Prinsip
• Pengukuran perbedaan temperatur yang terjadi antara material sampel
dan pembanding sebagai hasil dari reaksi dekomposisi
DTA

• Mengukur kecepatan rata-rata perubahan massa suatu bahan/cuplikan


sebagai fungsi dari suhu atau waktu pada atmosfir yang terkontrol
TGA
Instrumentasi

• Microbalance : merekam perubahan massa pada


sampel
• Furnace : untuk menghasilkan pemanasan yang linear
pada seluruh range temperatur
• Pengukur dan Kontrol Temperatur : untuk mengontrol
atau mevariasikan temperatur menggunakan program
kontroler
• Recorder : membuat plot antara berat dengan
temperatur.

 Range temperatur pada TGA : 0°C-2400°C


Instrumen yang digunakan pada termogravimetri (TG) disebut termobalance. Termobalance terdiri dari
beberapa komponen utama yang tersedia untuk menghasilkan data dalam bentuk kurva TGA.
Komponen utama dari termobalance seperti yang terlihat pada gambar di bawah ini:
Skema
Kegunaan TGA
Dapat digunakan untuk mengukur laju evaporasi, seperti untuk
01 mengukur emisi campuran cairan yang mudah menguap

Mengukur berat fiberglass dan material anorganik dalam plastik,


02 melaminasi, mengecat, primer, dan material composite dengan
pembakaran resin polymer

Menentukan temperatur dan perubahan berat reaksi dekomposisi,


03 analisa komposisi kuantitatif, serta menentukan kandungan air

04 Analisa reaksi dengan udara, oksigen, atau gas reaktif lainnya

Dapat mengukur material yang ditambahkan ke beberapa makanan,


05 seperti silika gel, dan titanium diaoksida
Kegunaan DTA

01

02

03 You can simply impress your audience and add a unique zing and appeal to your Presentations.

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05 You can simply impress your audience and add a unique zing and appeal to your Presentations.
Hasil Pengukuran
TGA

Tipe Kurva TGA


DTA
Kelebihan Kekurangan

Dapat digunakan pada suhu Memerlukan kalibrasi untuk ekspansi


yang sangat tinggi perbedaan panas neraca timbangan

Dapat menentukan kondisi


Keterbatasan dari DTA adalah
eksperimental sampel (baik dengan
sensitivitasnya yang cukup rendah
tekanan tinggi atau vakum)

Karakteristik transisi dan reaksi


pada temperatur tertentu dapat
dideteksi dengan baik
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