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\charscalex161 2120-84\par\pard\li1963\sb157\sl-207\slmult0\fi2961 \up0 \expndtw
0\charscalex161 DETERMINACION DE HIERRO\par\pard\li1963\sb158\sl-207\slmult0\fi2
822 \up0 \expndtw0\charscalex161 METODO DE LA FENANTROLINA\par\pard\li1963\sb0\s
l-207\slmult0\par\pard\li1963\sb172\sl-207\slmult0\fi2433\tx4656 \up0 \expndtw0\
charscalex161 1\tab \dn3 \expndtw0\charscalex161 \ul0\nosupersub\cf7\f8\fs18\ul
NORMAS COVENIN A CONSULTAR\par\pard\li1963\sb0\sl-207\slmult0\par\pard\li1963\sb
80\sl-207\slmult0\fi71\tx3086\tx4771 \up0 \expndtw0\charscalex106 \ul0\nosupersu
b\cf8\f9\fs18 COVENIN\tab \up0 \expndtw0\charscalex161 10:XIII-010\tab \dn2 \exp
ndtw0\charscalex161 Agua potable. Metodo para la toma de muestras.\par\pard\li19
63\sb0\sl-207\slmult0\par\pard\li1963\sb52\sl-207\slmult0\fi3321\tx5668 \up0 \ex
pndtw0\charscalex161 2\tab \dn3 \expndtw0\charscalex161 \ul0\nosupersub\cf7\f8\f
s18\ul OBJETO\par\pard\li1963\sb0\sl-207\slmult0\par\pard\li1963\sb75\sl-207\slm
ult0\fi67\tx2673 \up0 \expndtw0\charscalex161 \ul0\nosupersub\cf8\f9\fs18 2.1\ta

b \up0 \expndtw0\charscalex161 Esta norma contempla la determinacion de hierro e

n aguas natura-\par\pard\li1963\sb187\sl-207\slmult0\fi47 \up0 \expndtw0\charsca
lex161 les y tratadas,por el metodo de la fenantrolina.\par\pard\li1963\sb0\sl-2
07\slmult0\par\pard\li1963\sb32\sl-207\slmult0\fi52\tx2663 \up0 \expndtw0\charsc
alex161 2.2\tab \up0 \expndtw0\charscalex161 Este metodo permite detector direct
amente concentraciones entre\par\pard\li1963\sb153\sl-207\slmult0\fi52\tx2659\tx
2927\tx3441\tx5404 \up0 \expndtw0\charscalex161 0,02\tab \up0 \expndtw-2\charsca
lex100 y\tab \up0 \expndtw0\charscalex161 4,0\tab \up0 \expndtw0\charscalex161 m
g/l de hierro\tab \up0 \expndtw0\charscalex161 (total, disuelto o hierro ferroso
) y pueden\par\pard\li1963\sb163\sl-207\slmult0\fi47 \up0 \expndtw0\charscalex16
1 determinarse concentraciones altos mediante el use do muestras peque-\par\pard
\li1963\sb153\sl-207\slmult0\fi33\tx9398 \up0 \expndtw0\charscalex161 nas o dilu
ciones. La concentraci6n minima detectable es\tab \up0 \expndtw0\charscalex161 5
0j con un\par\pard\li1963\sb153\sl-207\slmult0\fi38\tx4612\tx5126\tx7708\tx7963
\up0 \expndtw0\charscalex161 espectrofot6metro a\tab \up0 \expndtw0\charscalex13
0 510\tab \dn2 \expndtw0\charscalex161 nm con una celda de\tab \up0 \expndtw0\ch
arscalex161 1\tab \dn2 \expndtw0\charscalex161 cm.\par\pard\li1963\sb0\sl-218\sl
mult0\par\pard\li1963\sb61\sl-218\slmult0\fi2390\tx4737 \up0 \expndtw0\charscale
x161 3\tab \up0 \expndtw0\charscalex161 \ul0\nosupersub\cf10\f11\fs20\ul PRINCIP
IO Y RESUMEN DEL ENSAYO\par\pard\li1963\sb0\sl-207\slmult0\par\pard\li1963\sb60\
sl-207\slmult0\fi33 \up0 \expndtw0\charscalex161 \ul0\nosupersub\cf8\f9\fs18 El
hierro puede ser disuelto y reducido al estado ferroso por ebtilli-\par\pard\li1
963\sb158\sl-207\slmult0\fi33\tx7828 \up0 \expndtw0\charscalex161 ci6n con acido
a hidroxilamina y tratado con\tab \up0 \expndtw0\charscalex161 1,10-fenantrolin
a a pH\par\pard\li1963\sb153\sl-207\slmult0\fi33\tx2520\tx2783\tx3556 \up0 \expn
dtw0\charscalex161 3,2\tab \up0 \expndtw-2\charscalex100 a\tab \up0 \expndtw0\ch
arscalex161 3,3.\tab \up0 \expndtw0\charscalex161 Tres moleculas de fenantrolina
quelan cada atomo de hie-\par\pard\li1963\sb157\sl-207\slmult0\fi33 \up0 \expnd
tw0\charscalex161 rro ferroso para formar un complejo rojo-anaranjado. La soluci
on co-\par\pard\li1963\sb172\sl-207\slmult0\fi23 \up0 \expndtw0\charscalex161 lo
reada cumple con la Ley de Beer; su intensidad es independiente del\par\pard\li1
963\sb139\sl-207\slmult0\fi23\tx3945\tx4195\tx4463\tx4972 \dn2 \expndtw0\charsca
lex161 rango de pH de\tab \up0 \expndtw-2\charscalex100 3\tab \up0 \expndtw-2\ch
arscalex100 a\tab \up0 \expndtw0\charscalex161 9.\tab \dn2 \expndtw0\charscalex1
61 A ualores de pH entre 2,9 y3,5 se asegura el desa\par\pard\li1963\sb153\sl-20
7\slmult0\fi23 \up0 \expndtw0\charscalex161 rrollo de una coloraci6n rapida an p
resencia do un exceso de fenantro\par\pard\li1963\sb153\sl-207\slmult0\fi14 \up0
\expndtw0\charscalex161 Tina.\par\pard\li1963\sb158\sl-207\slmult0\fi4 \up0 \ex
pndtw0\charscalex161 En la presencia de cantidades excesivas de constituyentes o
rganicos,\par\pard\sect\sectd\sbknone\cols3\colno1\colw7395\colsr20\colno2\colw5
44\colsr110\colno3\colw4041\colsr160\ql \li1968\sb148\sl-207\slmult0 \up0 \expnd
tw0\charscalex168 la muestra primero debe ser digerida con H\par\pard\column \ql
\li1963\sb0\sl-144\slmult0 \par\pard\ql \li1963\sb0\sl-144\slmult0 \par\pard\ql
\li20\sb33\sl-144\slmult0 \up0 \expndtw0\charscalex116 2SO4\par\pard\column \ql
\li20\sb153\sl-207\slmult0 \up0 \expndtw0\charscalex172 para destruir comples \
par\pard\sect\sectd\sbknone \li1963\sb43\sl-207\slmult0\fi9 \up0 \expndtw0\chars
calex177 jos organicos y asegurar la completa disolucion del hierro. La solu-\pa
r\pard\sect\sectd\sbknone \li1963\sb148\sl-207\slmult0\fi4\tx7281\tx7795\tx8971
\up0 \expndtw0\charscalex177 cion resultante se ileva a normalidad do\tab \up0 \
expndtw0\charscalex144 7-8\tab \up0 \expndtw0\charscalex135 N an HC1\tab \up0 \e
xpndtw0\charscalex177 y el hierro se\par\pard\sect\sectd\sbknone \li1963\sb159\s
l-218\slmult0\fi0\tx10132 \dn3 \expndtw0\charscalex177 separa do las sustancias
interferentes por extraccion de FeCl\tab \up0 \expndtw0\charscalex177 \ul0\nosup
ersub\cf9\f10\fs20 en eter\par\pard\ql \li9878\sb0\sl-170\slmult0 \up0 \expndtw2\charscalex100 3 \par\pard\ql \li1958\sb0\sl-162\slmult0 \up0 \expndtw0\charsca
lex180 \ul0\nosupersub\cf8\f9\fs18 isopropllico. Despu6s de la re-extraccion del
hierro en agua este se \par\pard\ql \li1958\sb159\sl-207\slmult0 \up0 \expndtw0
\charscalex164 reduce con hidroxilamina. \par\pard\sect\sectd\fs24\paperw12240\p
aperh15840{\bkmkstart Pg5}{\bkmkend Pg5}\par\pard\ql \li10300\sb0\sl-207\slmult0
\par\pard\ql\li10300\sb0\sl-207\slmult0 \par\pard\ql\li10300\sb0\sl-207\slmult0

\par\pard\ql\li10300\sb0\sl-207\slmult0 \par\pard\ql\li10300\sb0\sl-207\slmult0
\par\pard\ql\li10300\sb0\sl-207\slmult0 \par\pard\ql\li10300\sb0\sl-207\slmult0
\par\pard\ql\li10300\sb0\sl-207\slmult0 \par\pard\ql\li10300\sb0\sl-207\slmult0
\par\pard\ql\li10300\sb186\sl-207\slmult0 \up0 \expndtw0\charscalex167 \ul0\nos
upersub\cf8\f9\fs18 /2 \par\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb0\s
l-207\slmult0\par\pard\li2063\sb102\sl-207\slmult0\fi3936\tx6384 \up0 \expndtw0\
charscalex160 4\tab \up0 \expndtw0\charscalex160 \ul0\nosupersub\cf7\f8\fs18\ul
EQUIPO\par\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb0\sl-207\slmult0\par
\pard\li2063\sb108\sl-207\slmult0\fi38\tx2750 \up0 \expndtw0\charscalex160 \ul0\
nosupersub\cf8\f9\fs18 4.1\tab \dn2 \expndtw0\charscalex160 EQUIPO COLORIIETRICO
. Se requiere uno de los siguientes:\par\pard\li2063\sb0\sl-207\slmult0\par\pard
\li2063\sb66\sl-207\slmult0\fi33\tx3009\tx7415\tx7934 \up0 \expndtw0\charscalex1
60 4.1.1\tab \up0 \expndtw0\charscalex160 \ul0\nosupersub\cf7\f8\fs18\ul Espectr
ofotometro\ul0\nosupersub\cf8\f9\fs18 . Para usarlo a\tab \up0 \expndtw0\charsca
lex130 510\tab \up0 \expndtw0\charscalex160 nm, provisto de un paso\par\pard\li2
063\sb158\sl-207\slmult0\fi33\tx3407\tx3662 \up0 \expndtw0\charscalex160 de luz
de\tab \up0 \expndtw0\charscalex160 1\tab \up0 \expndtw0\charscalex160 cm de lon
gitud o mayor.\par\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb61\sl-207\sl
mult0\fi24\tx3004\tx9758\tx10003 \up0 \expndtw0\charscalex160 4.1.2\tab \up0 \ex
pndtw0\charscalex160 \ul0\nosupersub\cf7\f8\fs18\ul Fotometro con filtro\ul0\nos
upersub\cf8\f9\fs18 , provisto de un Paso de luz de\tab \up0 \expndtw0\charscale
x160 1\tab \up0 \expndtw0\charscalex160 cm de\par\pard\li2063\sb158\sl-207\slmul
t0\fi24 \up0 \expndtw0\charscalex160 longitud y equipado con un filtro verde con
un maximo de transmitan-\par\pard\li2063\sb148\sl-207\slmult0\fi19\tx3907\tx443
0 \up0 \expndtw0\charscalex160 cia cercano a\tab \up0 \expndtw0\charscalex132 51
0\tab \up0 \expndtw0\charscalex160 nm.\par\pard\li2063\sb0\sl-207\slmult0\par\pa
rd\li2063\sb66\sl-207\slmult0\fi14\tx2985\tx5467\tx5971 \up0 \expndtw0\charscale
x160 4.1.3\tab \up0 \expndtw0\charscalex160 \ul0\nosupersub\cf7\f8\fs18\ul Tubos
deNessler\ul0\nosupersub\cf8\f9\fs18 de\tab \up0 \expndtw0\charscalex130 100\t
ab \up0 \expndtw0\charscalex160 ml, de forma alta.\par\pard\li2063\sb0\sl-207\sl
mult0\par\pard\li2063\sb66\sl-207\slmult0\fi4\tx2721 \up0 \expndtw0\charscalex16
0 4.2\tab \dn2 \expndtw0\charscalex160 MATERIAL DE VIDRIO LAVADO CON ACIDO\par\p
ard\li2063\sb158\sl-207\slmult0\fi0\tx8179 \up0 \expndtw0\charscalex160 Se lava
todo el material con acido clorhidrico\tab \dn2 \expndtw0\charscalex160 (HC1) co
ncentrado y\par\pard\li2063\sb158\sl-207\slmult0\fi4 \up0 \expndtw0\charscalex16
0 se enjuaga con agua destilada antes deusarlo, Para eliminar deposi-\par\pard\l
i2063\sb148\sl-207\slmult0\fi9\tx2980 \up0 \expndtw0\charscalex160 tor de\tab \d
n2 \expndtw0\charscalex160 6xido de hierro.\par\pard\li2063\sb0\sl-207\slmult0\p
ar\pard\li2063\sb61\sl-207\slmult0\fi0\tx2712\tx6095\tx6600 \up0 \expndtw0\chars
calex160 4.3\tab \dn2 \expndtw0\charscalex123 EIIBUDOS DE SEPARACION, de\tab \up
0 \expndtw0\charscalex128 125\tab \dn2 \expndtw0\charscalex160 ml con have de te
flon.\par\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb0\sl-207\slmult0\par\
pard\li2063\sb104\sl-207\slmult0\fi3643\tx6081 \up0 \expndtw0\charscalex160 5\ta
b \dn2 \expndtw0\charscalex160 \ul0\nosupersub\cf7\f8\fs18\ul REACTIVOS\par\pard
\qj \li2059\ri1236\sb256\sl-353\slmult0 \up0 \expndtw0\charscalex158 \ul0\nosupe
rsub\cf9\f10\fs20 Todos los reactivos deberan ser de grado analitico y bajo cont
enido \line \up0 \expndtw0\charscalex179 \ul0\nosupersub\cf8\f9\fs18 de hierro y
almacenados an botellas con tapa de vidrio. Las solucio \line \up0 \expndtw0\ch
arscalex173 nes deberan prepararse con agua destilada, deionizada, Libre de meta
\line \dn2 \expndtw0\charscalex174 les, con una conductancia especifica entre \
up0 \expndtw0\charscalex158 0,5 \up0 \expndtw-2\charscalex100 a \up0 \expndtw-2\
charscalex100 5 \dn2 \expndtw0\charscalex143 micromhos-cm maxi \par\pard\ql \li2
035\ri1236\sb24\sl-357\slmult0\fi19 \up0 \expndtw0\charscalex176 mo. Los reactiv
os deben almacenarse an botellas de vidrio bien tapa \up0 \expndtw0\charscalex18
0 das. El acido clorhidrico y las soluciones de acetato de amonio son \up0 \expn
dtw0\charscalex179 estables indefinidamente si estan bien tapadas. La hidroxilam
ina, \up0 \expndtw0\charscalex182 la fenantrolina y las soluciones de reserva de
hierro son estables \up0 \expndtw0\charscalex179 por varios meses. Las solucion
es patron de hierro no son estables \up0 \expndtw0\charscalex179 y deben prepara
rse diariamente a partir de la solucion de reserva. \up0 \expndtw0\charscalex175

Los patrones visuales an tubas de Nessler son estables por varios me \up0 \expn
dtw0\charscalex176 ses si estan sellados y protegidos de la luz. \par\pard\sect\
sectd\fs24\paperw12240\paperh15840{\bkmkstart Pg6}{\bkmkend Pg6}\par\pard\ql \li
10238\sb0\sl-207\slmult0 \par\pard\ql\li10238\sb0\sl-207\slmult0 \par\pard\ql\li
10238\sb0\sl-207\slmult0 \par\pard\ql\li10238\sb0\sl-207\slmult0 \par\pard\ql\li
10238\sb0\sl-207\slmult0 \par\pard\ql\li10238\sb0\sl-207\slmult0 \par\pard\ql\li
10238\sb0\sl-207\slmult0 \par\pard\ql\li10238\sb0\sl-207\slmult0 \par\pard\ql\li
10238\sb113\sl-207\slmult0 \up0 \expndtw0\charscalex167 \ul0\nosupersub\cf8\f9\f
s18 /3 \par\pard\li1891\sb0\sl-207\slmult0\par\pard\li1891\sb0\sl-207\slmult0\pa
r\pard\li1891\sb0\sl-207\slmult0\par\pard\li1891\sb45\sl-207\slmult0\fi48\tx2587
\tx6494 \up0 \expndtw0\charscalex137 5.1\tab \up0 \expndtw0\charscalex112 ACIDO
CLORHIDRICO CONCENTRADO\tab \up0 \expndtw0\charscalex137 (HC1), quo contenga men
os de\par\pard\li1891\sb158\sl-207\slmult0\fi43\tx2961 \up0 \expndtw0\charscalex
137 0,00005\tab \up0 \expndtw0\charscalex137 % de hierro.\par\pard\li1891\sb0\sl
-207\slmult0\par\pard\li1891\sb71\sl-207\slmult0\fi38\tx2577\tx4430 \up0 \expndt
w0\charscalex137 5.2\tab \up0 \expndtw0\charscalex110 HIDROXILAMINA\tab \up0 \ex
pndtw0\charscalex137 (NH2OH.HC1).\par\pard\li1891\sb0\sl-207\slmult0\par\pard\li
1891\sb186\sl-207\slmult0\fi33\tx2563\tx7900\tx8275 \dn2 \expndtw0\charscalex137
5.3\tab \dn2 \expndtw0\charscalex137 SOLUCION DE HIDROXILAMINA. Se disuelven\ta
b \up0 \expndtw0\charscalex137 10\tab \up0 \expndtw0\charscalex137 g de hidroxil
amina\par\pard\li1891\sb154\sl-230\slmult0\fi24\tx2313\tx2827 \up0 \expndtw0\cha
rscalex137 an\tab \up0 \expndtw0\charscalex118 \ul0\nosupersub\cf9\f10\fs20 100\
tab \up0 \expndtw0\charscalex137 ml de agua destilada.\par\pard\li1891\sb0\sl-20
7\slmult0\par\pard\li1891\sb37\sl-207\slmult0\fi24\tx2558\tx4924 \up0 \expndtw0\
charscalex137 \ul0\nosupersub\cf8\f9\fs18 5.4\tab \dn2 \expndtw0\charscalex112 A
CETATO DE AMONIO\tab \dn2 \expndtw0\charscalex137 (NH4C2H302).\par\pard\li1891\s
b0\sl-207\slmult0\par\pard\li1891\sb186\sl-207\slmult0\fi14\tx2553\tx5433 \up0 \
expndtw0\charscalex137 5.5\tab \dn2 \expndtw0\charscalex118 ACIDO ACETICO GLACIA
L\tab \dn2 \expndtw0\charscalex137 (CH3000H), concentrado.\par\pard\li1891\sb0\s
l-230\slmult0\par\pard\li1891\sb149\sl-230\slmult0\fi14\tx2543\tx9297\tx9815 \up
0 \expndtw0\charscalex137 \ul0\nosupersub\cf9\f10\fs20 5.6\tab \up0 \expndtw0\ch
arscalex119 SOLUCION BUFFER DE ACETATO DE AMONIO. Se disuelven\tab \up0 \expndtw
0\charscalex120 250\tab \up0 \expndtw0\charscalex137 g de\par\pard\li1891\sb158\
sl-207\slmult0\fi0\tx4646\tx5155\tx9556\tx10075 \up0 \expndtw0\charscalex137 \ul
0\nosupersub\cf8\f9\fs18 acetato de amonio an\tab \up0 \expndtw0\charscalex137 1
50\tab \up0 \expndtw0\charscalex137 ml de agua destilada. Se agregan\tab \up0 \e
xpndtw0\charscalex137 700\tab \up0 \expndtw0\charscalex137 ml de\par\pard\ql \li
1891\sb141\sl-207\slmult0 \up0 \expndtw0\charscalex174 acido acatico glacial. Au
n cuando el acetato do amonio tenga un \par\pard\qj \li1891\ri1451\sb27\sl-360\s
lmult0\fi9 \up0 \expndtw0\charscalex155 \ul0\nosupersub\cf9\f10\fs20 buen grado
de pureza,contiene una cantidad significativa de hierro,_ \up0 \expndtw0\charsca
lex155 par lo cual deben preparerse nuevos patrones de referencia can cada \up0
\expndtw0\charscalex151 buffer preparado. \par\pard\li1852\sb0\sl-207\slmult0\pa
r\pard\li1852\sb52\sl-207\slmult0\fi48\tx2539\tx4780 \up0 \expndtw0\charscalex15
0 \ul0\nosupersub\cf8\f9\fs18 5.7\tab \up0 \expndtw0\charscalex117 ACETATO DE SO
DIO\tab \up0 \expndtw0\charscalex150 (NaC2H302.3H20).\par\pard\li1852\sb0\sl-207
\slmult0\par\pard\li1852\sb181\sl-207\slmult0\fi43\tx2534\tx8251\tx8769 \up0 \ex
pndtw0\charscalex150 5.8\tab \up0 \expndtw0\charscalex137 SOLUCION DE ACETATO DE
SODIO. Se disuelven\tab \up0 \expndtw0\charscalex150 200\tab \up0 \expndtw0\cha
rscalex150 g de acetate de\par\pard\li1852\sb139\sl-230\slmult0\fi33\tx3067\tx35
90 \up0 \expndtw0\charscalex150 \ul0\nosupersub\cf9\f10\fs20 sodio en\tab \up0 \
expndtw0\charscalex120 800\tab \up0 \expndtw0\charscalex150 ml de agua destilada
.\par\pard\li1852\sb0\sl-207\slmult0\par\pard\li1852\sb62\sl-207\slmult0\fi38\tx
2543\tx6700 \up0 \expndtw0\charscalex150 \ul0\nosupersub\cf8\f9\fs18 5.9\tab \up
0 \expndtw0\charscalex113 1,10-FENANTROLINA MONOHIDRATADA\tab \up0 \expndtw0\cha
rscalex150 \ul0\nosupersub\cf9\f10\fs20 (C12H8N2.H2O).\par\pard\li1852\sb0\sl-20
7\slmult0\par\pard\li1852\sb182\sl-207\slmult0\fi33\tx2654\tx7857\tx8366\tx9163\
tx9307\tx9417 \up0 \expndtw0\charscalex150 \ul0\nosupersub\cf8\f9\fs18 5.10\tab
\up0 \expndtw0\charscalex136 SOLUCION DE FENANTROLINA. Se disuelven\tab \up0 \ex
pndtw0\charscalex130 100\tab \up0 \expndtw0\charscalex150 mg de\tab \up0 \expndt

w-4\charscalex100 1\tab \up0 \expndtw-4\charscalex100 ,\tab \up0 \expndtw0\chars

calex150 10-Fenan-\par\pard\li1852\sb153\sl-207\slmult0\fi28\tx2932\tx4108\tx461
7 \up0 \expndtw0\charscalex150 trolina\tab \up0 \expndtw0\charscalex150 (5.9) an
\tab \up0 \expndtw0\charscalex128 100\tab \up0 \expndtw0\charscalex150 ml de agu
a destilada par agitacion y calenta-\par\pard\li1852\sb157\sl-207\slmult0\fi19\t
x3052 \up0 \expndtw0\charscalex150 miento a\tab \up0 \expndtw0\charscalex150 809
C, Pero no debe hervir. Si la solucion esta oscura se\par\pard\li1852\sb153\sl-2
07\slmult0\fi14\tx9268\tx9527 \up0 \expndtw0\charscalex150 descarta. El calentam
iento no as necesario si se anaden\tab \up0 \expndtw0\charscalex150 2\tab \up0 \
expndtw0\charscalex150 gotas de\par\pard\li1852\sb158\sl-207\slmult0\fi4\tx8107\
tx9134 \up0 \expndtw0\charscalex150 acido clorhidrico concentrado al agua destil
ada\tab \up0 \expndtw0\charscalex114 (NOTA:\tab \up0 \expndtw0\charscalex150 Par
a solu-\par\pard\li1852\sb148\sl-207\slmult0\fi4\tx4483\tx8620\tx8870 \up0 \expn
dtw0\charscalex150 ciones con menos de\tab \up0 \expndtw0\charscalex150 100 /4g
de hierro as suficiente\tab \up0 \expndtw0\charscalex150 1\tab \up0 \expndtw0\ch
arscalex150 ml do este\par\pard\li1852\sb130\sl-230\slmult0\fi0 \up0 \expndtw0\c
harscalex150 \ul0\nosupersub\cf9\f10\fs20 reactiuo).\par\pard\li1852\sb0\sl-207\
slmult0\par\pard\li1852\sb62\sl-207\slmult0\fi0\tx2625\tx7310 \up0 \expndtw0\cha
rscalex150 \ul0\nosupersub\cf8\f9\fs18 5.11\tab \up0 \expndtw0\charscalex115 SOL
UCION DE PERMANGANATO DE POTASIO\tab \up0 \expndtw0\charscalex150 0,1N\par\pard\
li1852\sb0\sl-207\slmult0\par\pard\li1852\sb70\sl-207\slmult0\fi0\tx2620\tx6264
\up0 \expndtw0\charscalex150 5.12\tab \dn2 \expndtw0\charscalex119 SOLUCION DE A
CIDO SULFURICO\tab \up0 \expndtw0\charscalex150 6N\par\pard\sect\sectd\fs24\pape
rw12240\paperh15840{\bkmkstart Pg7}{\bkmkend Pg7}\par\pard\ql \li10454\sb0\sl-20
7\slmult0 \par\pard\ql\li10454\sb0\sl-207\slmult0 \par\pard\ql\li10454\sb0\sl-20
7\slmult0 \par\pard\ql\li10454\sb0\sl-207\slmult0 \par\pard\ql\li10454\sb0\sl-20
7\slmult0 \par\pard\ql\li10454\sb0\sl-207\slmult0 \par\pard\ql\li10454\sb0\sl-20
7\slmult0 \par\pard\ql\li10454\sb0\sl-207\slmult0 \par\pard\ql\li10454\sb0\sl-20
7\slmult0 \par\pard\ql\li10454\sb66\sl-207\slmult0 \up0 \expndtw0\charscalex167
\ul0\nosupersub\cf8\f9\fs18 /4 \par\pard\li2256\sb0\sl-207\slmult0\par\pard\li22
56\sb0\sl-207\slmult0\par\pard\li2256\sb0\sl-207\slmult0\par\pard\li2256\sb135\s
l-207\slmult0\fi9\tx3043\tx7175\tx7430 \up0 \expndtw0\charscalex138 5.13\tab \up
0 \expndtw0\charscalex116 ALAMBRE DE HIERRO ELECTROLITICO\tab \up0 \expndtw0\cha
rscalex138 0\tab \up0 \expndtw0\charscalex138 SULFATO FERRO AMONICO,\par\pard\li
2256\sb167\sl-207\slmult0\fi263 \up0 \expndtw0\charscalex138 Fe(NH4)2(504)2.6H20
\par\pard\li2256\sb0\sl-207\slmult0\par\pard\li2256\sb181\sl-207\slmult0\fi0\tx3
028\tx6921 \up0 \expndtw0\charscalex138 5.14\tab \dn2 \expndtw0\charscalex118 SO
LUCION DE RESERVA DE HIERRO\tab \up0 \expndtw0\charscalex138 (200,,_g/ml).\par\p
ard\li2256\sb153\sl-207\slmult0\fi0\tx6787\tx8476 \up0 \expndtw0\charscalex138 P
ara prepararla puede usarse metal\tab \up0 \expndtw0\charscalex138 (a) o la sal\
tab \up0 \expndtw0\charscalex138 (b):\par\pard\ql \li2236\ri1198\sb15\sl-360\slm
ult0\fi19 \up0 \expndtw0\charscalex176 (a) Para preparar la solucion debe usarse
alambre do hierro electro \line \up0 \expndtw0\charscalex179 litico o "alambre
de hierro Para estandarizaci6n". Si fuese necesa \line \up0 \expndtw0\charscalex
177 rio se limpia el alambre con papel arena fino Para eliminar cual-\line \up0
\expndtw0\charscalex174 quier cubierta do \up0 \expndtw0\charscalex178 6xido y P
ara producir una superficie brillante. \par\pard\li2188\sb130\sl-207\slmult0\fi4
3\tx3403\tx3926 \dn2 \expndtw0\charscalex157 Se pesan\tab \up0 \expndtw0\charsca
lex135 200\tab \dn2 \expndtw0\charscalex171 mg del alambre y se colocan en un ma
traz aforado de\par\pard\li2188\sb143\sl-207\slmult0\fi52\tx2491\tx3004\tx4953\t
x5337\tx9744 \up0 \expndtw0\charscalex171 1\tab \up0 \expndtw0\charscalex171 1.\
tab \dn2 \expndtw0\charscalex171 Se disuelve en\tab \up0 \expndtw0\charscalex127
20\tab \dn2 \expndtw0\charscalex171 ml de solucion de acido sulfurico\tab \dn2
\expndtw0\charscalex171 6N y se\par\pard\li2188\sb167\sl-207\slmult0\fi47 \up0 \
expndtw0\charscalex171 diluye haste el aforo con ague destilada libre de hierro.
\par\pard\li2188\sb140\sl-230\slmult0\fi52\tx2616\tx2995 \up0 \expndtw0\charscal
ex171 (1\tab \up0 \expndtw0\charscalex108 \ul0\nosupersub\cf9\f10\fs20 ml\tab \u
p0 \expndtw0\charscalex171 = 200/ de hierro).\par\pard\li2188\sb0\sl-207\slmult0
\par\pard\li2188\sb52\sl-207\slmult0\fi43 \up0 \expndtw0\charscalex171 \ul0\nosu
persub\cf8\f9\fs18 (b) Si se prefiere utilizer sulfato ferro-am6nico, se agregan

lenta\par\pard\li2188\sb138\sl-207\slmult0\fi33\tx3004\tx3398\tx8044\tx8438 \up
0 \expndtw0\charscalex140 mente\tab \up0 \expndtw0\charscalex130 20\tab \up0 \ex
pndtw0\charscalex171 ml de acido sulfurico concentrado a\tab \up0 \expndtw0\char
scalex129 50\tab \up0 \expndtw0\charscalex171 ml de agua destilada\par\pard\li21
88\sb172\sl-207\slmult0\fi47\tx5332\tx5476\tx6095 \dn2 \expndtw0\charscalex171 y
en ella se disuelven\tab \up0 \expndtw-4\charscalex100 1\tab \up0 \expndtw0\cha
rscalex146 ,404\tab \dn2 \expndtw0\charscalex171 g de sulfato ferro-am6nico. Se
agre-\par\pard\li2188\sb146\sl-207\slmult0\fi28\tx7262\tx7920\tx10243 \up0 \expn
dtw0\charscalex166 ga solucion de permanganato de potasio\tab \up0 \expndtw0\cha
rscalex134 0,1N\tab \up0 \expndtw0\charscalex171 (5.11) gota a gota\tab \dn3 \ex
pndtw0\charscalex171 ,,has-\par\pard\li2188\sb156\sl-207\slmult0\fi33\tx10382\tx
10636 \dn2 \expndtw0\charscalex171 ta que aparezca un leve color rosado persiste
nte. Se diluye a\tab \up0 \expndtw0\charscalex171 1\tab \up0 \expndtw0\charscale
x171 li\par\pard\li2188\sb153\sl-207\slmult0\fi23\tx8827\tx9206\tx9580 \dn2 \exp
ndtw0\charscalex171 tro con ague destilada libre de hierro y se mezcla\tab \up0
\expndtw0\charscalex171 (1\tab \up0 \expndtw0\charscalex117 ml\tab \up0 \expndtw
0\charscalex171 = 200//,t,,g\par\pard\li2188\sb138\sl-207\slmult0\fi23 \up0 \exp
ndtw0\charscalex171 de hierro).\par\pard\li2188\sb0\sl-207\slmult0\par\pard\li21
88\sb57\sl-207\slmult0\fi14\tx2976 \up0 \expndtw0\charscalex171 5.15\tab \dn3 \e
xpndtw0\charscalex145 SOLUCIONES PATRONDEHIERRO. Deben prepararse diariamente pa
-\par\pard\li2188\sb139\sl-230\slmult0\fi4 \up0 \expndtw0\charscalex171 \ul0\nos
upersub\cf9\f10\fs20 ra su uso.\par\pard\li2188\sb0\sl-207\slmult0\par\pard\li21
88\sb57\sl-207\slmult0\fi4\tx3225\tx6974\tx7363 \up0 \expndtw0\charscalex171 \ul
0\nosupersub\cf8\f9\fs18 5.15.1\tab \dn2 \expndtw0\charscalex171 Se transfiere c
on una pipeta\tab \dn2 \expndtw0\charscalex127 50\tab \dn3 \expndtw0\charscalex1
71 ml de solucion de reserve\par\pard\li2188\sb153\sl-207\slmult0\fi0\tx3527\tx7
396\tx7651 \up0 \expndtw0\charscalex171 do hierro\tab \dn3 \expndtw0\charscalex1
71 (5.14) a un matraz aforado do\tab \dn3 \expndtw0\charscalex171 1\tab \dn3 \ex
pndtw0\charscalex171 litro y se diluye haste el\par\pard\sect\sectd\sbknone\cols
2\colno1\colw8839\colsr60\colno2\colw3201\colsr160\ql \li2203\sb153\sl-207\slmul
t0\tx7900\tx8284\tx8562 \up0 \expndtw0\charscalex180 aforo con ague destilada li
bre de hierro \up0 \expndtw0\charscalex125 (1\tab \up0 \expndtw0\charscalex117 m
l\tab \up0 \expndtw0\charscalex110 =\tab \up0 \expndtw0\charscalex121 10\par\par
d\column \ql \li2193\sb0\sl-144\slmult0 \par\pard\ql \li2193\sb0\sl-144\slmult0
\par\pard\ql \li20\sb14\sl-144\slmult0 \up0 \expndtw0\charscalex161 /t-"g de Fe)
. \par\pard\sect\sectd\sbknone \li2193\sb140\sl-207\slmult0\fi19\tx3240\tx6993\t
x7252 \up0 \expndtw0\charscalex161 5.15.2\tab \up0 \expndtw0\charscalex161 Se tr
ansfiere con una pipeta\tab \up0 \expndtw0\charscalex161 5\tab \up0 \expndtw0\ch
arscalex161 ml de la solucion de reserve\par\pard\sect\sectd\sbknone \li2193\sb1
38\sl-230\slmult0\fi14\tx3523 \up0 \expndtw0\charscalex161 \ul0\nosupersub\cf9\f
10\fs20 de hierro\tab \up0 \expndtw0\charscalex161 (5.14) a un matraz aforado do
I litro y se diluye haste el\par\pard\sect\sectd\sbknone \li2193\sb149\sl-207\s
lmult0\fi0\tx7646\tx8025\tx8404\tx8687\tx9124 \up0 \expndtw0\charscalex161 \ul0\
nosupersub\cf8\f9\fs18 aforo con ague destilada libre de hierro.\tab \up0 \expnd
tw0\charscalex161 (1\tab \up0 \expndtw0\charscalex117 ml\tab \up0 \expndtw0\char
scalex120 =\tab \up0 \expndtw0\charscalex161 1\tab \up0 \expndtw0\charscalex161
.g do Fe).\par\pard\sect\sectd\sbknone \li2193\sb0\sl-207\slmult0\par\pard\li219
3\sb57\sl-207\slmult0\fi9\tx2980\tx4800\tx5044 \up0 \expndtw0\charscalex161 5.16
\tab \up0 \expndtw0\charscalex126 DI-ISOPROPILO\tab \up0 \expndtw-2\charscalex10
0 0\tab \up0 \expndtw0\charscalex161 ETER ISOPROPILICO\par\pard\sect\sectd\fs24\
paperw12240\paperh15840{\bkmkstart Pg8}{\bkmkend Pg8}\par\pard\ql \li10358\sb0\s
l-207\slmult0 \par\pard\ql\li10358\sb0\sl-207\slmult0 \par\pard\ql\li10358\sb0\s
l-207\slmult0 \par\pard\ql\li10358\sb0\sl-207\slmult0 \par\pard\ql\li10358\sb0\s
l-207\slmult0 \par\pard\ql\li10358\sb0\sl-207\slmult0 \par\pard\ql\li10358\sb0\s
l-207\slmult0 \par\pard\ql\li10358\sb0\sl-207\slmult0 \par\pard\ql\li10358\sb53\
sl-207\slmult0 \up0 \expndtw0\charscalex167 \ul0\nosupersub\cf8\f9\fs18 /5 \par\
pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb0\sl-207\slmult0\par\pard\li206
3\sb0\sl-207\slmult0\par\pard\li2063\sb163\sl-207\slmult0\fi2995\tx5438 \up0 \ex
pndtw0\charscalex145 6\tab \dn2 \expndtw0\charscalex145 \ul0\nosupersub\cf7\f8\f
s18\ul CONDICIONES DE ENSAYO\par\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\

sb0\sl-207\slmult0\par\pard\li2063\sb113\sl-207\slmult0\fi4\tx2731 \up0 \expndtw

0\charscalex145 \ul0\nosupersub\cf8\f9\fs18 6.1\tab \up0 \expndtw0\charscalex145
INTERFERENCIAS\par\pard\li2063\sb0\sl-230\slmult0\par\pard\li2063\sb49\sl-230\s
lmult0\fi0\tx2971 \up0 \expndtw0\charscalex145 6.1.1\tab \up0 \expndtw0\charscal
ex50 \ul0\nosupersub\cf9\f10\fs20 l F\t \up0 \expndtw0\charscalex145 \ul0\nosupe
rsub\cf8\f9\fs18 uchas de las sustancias interferentes son agentes fuertemen\par
\pard\ql \li2063\sb119\sl-207\slmult0\tx8932 \up0 \expndtw0\charscalex182 to oxi
dantes tales como: cianuro, nitrito y fosfatos \tab \up0 \expndtw0\charscalex178
(polifosfatos \par\pard\ql \li2054\ri1384\sb35\sl-350\slmult0 \up0 \expndtw0\ch
arscalex170 mas que ortofosfatas), cromo, zinc an concentraciones que exceden \l
ine \up0 \expndtw0\charscalex124 10 \up0 \expndtw0\charscalex173 veces la de hie
rro, cobalto y cobra an concentraciones mayores \line \dn2 \expndtw0\charscalex1
32 de \up0 \expndtw-2\charscalex100 5 \dn3 \expndtw0\charscalex167 mg/l y niquel
an concentraciones mayores de \dn2 \expndtw-2\charscalex100 2 \dn2 \expndtw0\ch
arscalex174 mg/l. El bismu-\par\pard\ql \li2059\sb149\sl-207\slmult0 \up0 \expnd
tw0\charscalex177 to, cadmio, molibdato y plata precipitan con fenantrolina. \pa
r\pard\ql \li2040\ri1380\sb147\sl-360\slmult0\fi9\tx2961 \up0 \expndtw0\charscal
ex169 6.1.2 \tab \up0 \expndtw0\charscalex182 La ebullici6n inicial con acido co
nvierte los polifosfatos a \line\up0 \expndtw0\charscalex182 ortofoafatos y elim
ina cianuro y nitrito los cuales pueden interfe-\line \up0 \expndtw0\charscalex1
79 rir. La adici6n de un exceso de hidroxilamina eliminara errores \line \up0 \e
xpndtw0\charscalex154 \ul0\nosupersub\cf9\f10\fs20 causados por concentraciones
excesivas de reactivos fuertemente oxi \line \up0 \expndtw0\charscalex149 dantes
. \par\pard\ql \li2020\ri1384\sb120\sl-360\slmult0\fi14\tx2947 \up0 \expndtw0\ch
arscalex151 6.1.3 \tab \up0 \expndtw0\charscalex158 En presencia de iones metali
cos qua causen interferencia, se \line\up0 \expndtw0\charscalex156 requiere un g
ran exceso de fenantrolina pars reemplazar aquella \line \up0 \expndtw0\charscal
ex155 acomplejada par los metales interferentes. Cuando hay una concen \up0 \exp
ndtw0\charscalex159 traci6n excesiva de Tones metalicos interferentes, puede usa
rse el \up0 \expndtw0\charscalex154 m6todo de extracci6n. \par\pard\qj \li2011\r
i1417\sb116\sl-365\slmult0\fi9\tx2927 \up0 \expndtw0\charscalex169 \ul0\nosupers
ub\cf8\f9\fs18 6.1.4 \tab \dn2 \expndtw0\charscalex175 Si la muestra eats muy co
loreada, o presenta cantidades nota \line\up0 \expndtw0\charscalex176 bles de ma
teria organica, puede ser necesario evaporar la muestra, \line \up0 \expndtw0\ch
arscalex158 \ul0\nosupersub\cf9\f10\fs20 se incinera cuidadosamente ei residuo y
se redisuelve an acido. La \line \up0 \expndtw0\charscalex181 \ul0\nosupersub\c
f8\f9\fs18 incineraci6npuede hacerse an crisoles de silice, porcelana o piati-\l
ine \up0 \expndtw0\charscalex175 no qua hayan sido hervidos varias horas an solu
ci6n de acido clorhi \par\pard\li2011\sb116\sl-207\slmult0\fi0\tx2793\tx3047\tx3
316 \up0 \expndtw0\charscalex155 drico\tab \up0 \expndtw0\charscalex155 1\tab \u
p0 \expndtw0\charscalex120 +\tab \up0 \expndtw0\charscalex155 1.\par\pard\sect\s
ectd\fs24\paperw12240\paperh15840{\bkmkstart Pg9}{\bkmkend Pg9}\par\pard\ql \li1
0468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li1
0468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li1
0468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li1
0468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li1
0468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb26\sl-207\slmult0 \up0 \expndtw0\
charscalex170 \ul0\nosupersub\cf8\f9\fs18 /6 \par\pard\li2145\sb0\sl-230\slmult0
\par\pard\li2145\sb0\sl-230\slmult0\par\pard\li2145\sb212\sl-230\slmult0\fi3273\
tx5803 \up0 \expndtw0\charscalex162 7\tab \dn3 \expndtw0\charscalex162 \ul0\nosu
persub\cf10\f11\fs20\ul PROCEDIMIENTO\par\pard\li2145\sb0\sl-207\slmult0\par\par
d\li2145\sb0\sl-207\slmult0\par\pard\li2145\sb89\sl-207\slmult0\fi28\tx2822 \up0
\expndtw0\charscalex162 \ul0\nosupersub\cf8\f9\fs18 7.1\tab \up0 \expndtw0\char
scalex162 PREPARACION DE LAS CURVAS DE CALIBRACION\par\pard\li2145\sb0\sl-207\sl
mult0\par\pard\li2145\sb66\sl-207\slmult0\fi24\tx3062\tx5712\tx7905 \up0 \expndt
w0\charscalex162 7.1.1\tab \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf7\f8\f
s18\ul Para un intervalo de\tab \up0 \expndtw0\charscalex154 0 -100,eq .Ve/100\t
ab \up0 \expndtw0\charscalex162 ml de solucion final\ul0\nosupersub\cf8\f9\fs18
.\par\pard\li2145\sb0\sl-207\slmult0\par\pard\li2145\sb66\sl-207\slmult0\fi19\tx
3326\tx7080\tx7233\tx7512\tx7857\tx8251\tx8505\tx8774\tx9153 \dn3 \expndtw0\char

scalex162 7.1.1.1\tab \dn3 \expndtw0\charscalex162 Se transfiere con Tina pipe'u

a\t \up0 \expndtw0\charscalex120 \ul0\nosupersub\cf12\f13\fs14 a\tab \up0 \expnd
tw-4\charscalex100 2 \ul0\nosupersub\cf8\f9\fs18 \u-3?\tab \dn3 \expndtw0\charsc
alex120 ,\tab \dn3 \expndtw-2\charscalex100 ,,\tab \dn2 \expndtw0\charscalex162
\ul0\nosupersub\cf13\f14\fs20\ul 6,\tab \up0 \expndtw0\charscalex162 \ul0\nosupe
rsub\cf14\f15\fs12 8\tab \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf12\f13\f
s14 y \ul0\nosupersub\cf8\f9\fs18 ,\tab \up0 \expndtw0\charscalex162 \ul0\nosupe
rsub\cf12\f13\fs14 10\tab \dn4 \expndtw0\charscalex162 ml\ul0\nosupersub\cf9\f10
\fs20 de\ul0\nosupersub\cf12\f13\fs14 la solu-\par\pard\li2145\sb153\sl-207\sl
mult0\fi14\tx5020\tx9163\tx9667 \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf8
\f9\fs18 cion patron de hierro\tab \up0 \expndtw0\charscalex162 (5.15.1) a matra
ces aforados de\tab \up0 \expndtw0\charscalex128 100\tab \up0 \expndtw0\charscal
ex162 ml, se a-\par\pard\li2145\sb158\sl-207\slmult0\fi9\tx7344\tx8375\tx8625 \u
p0 \expndtw0\charscalex162 grega I ml de solucion de hidroxilamina\tab \up0 \exp
ndtw0\charscalex162 (5.3) y\tab \up0 \expndtw0\charscalex162 1\tab \up0 \expndtw
0\charscalex162 ml de solucion de\par\pard\li2145\sb148\sl-207\slmult0\fi0\tx437
2 \up0 \expndtw0\charscalex162 acetato de sodio\tab \up0 \expndtw0\charscalex162
(5.8) a cada matraz. Se diluye el contenido de ca-\par\pard\li2145\sb153\sl-207
\slmult0\fi9\tx5260\tx5644\tx10060\tx10440 \up0 \expndtw0\charscalex162 da uno c
on alrededor de\tab \up0 \expndtw0\charscalex121 75\tab \up0 \expndtw0\charscale
x162 ml de ague destilada y as agregan\tab \up0 \expndtw0\charscalex124 10\tab \
up0 \expndtw0\charscalex162 ml\par\pard\li2145\sb153\sl-207\slmult0\fi9\tx5779\t
x6926 \up0 \expndtw0\charscalex162 de solucion de fenantrolina\tab \up0 \expndtw
0\charscalex162 (5.10).\tab \up0 \expndtw0\charscalex162 Se diluye a volumen y s
e mezcla\par\pard\li2145\sb153\sl-207\slmult0\fi4\tx7320 \up0 \expndtw0\charscal
ex162 vigorosamente, se deja an reposo por,10\tab \up0 \expndtw0\charscalex162 m
in.\par\pard\li2145\sb0\sl-207\slmult0\par\pard\li2145\sb66\sl-207\slmult0\fi0\t
x3307 \up0 \expndtw0\charscalex162 7.1.1.2\tab \up0 \expndtw0\charscalex162 Se m
ide la absorbancia de cada soluci6n en una celda de\par\pard\li2145\sb120\sl-230
\slmult0\fi0\tx2404\tx3057\tx3576 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\
cf9\f10\fs20 5\tab \dn2 \expndtw0\charscalex124 cm a\tab \dn2 \expndtw0\charscal
ex118 510\tab \dn2 \expndtw0\charscalex162 nm contra un blanco de referencia pre
parado con ague\ul0\nosupersub\cf10\f11\fs20\ul des\par\pard\ql \li2150\sb151\s
l-207\slmult0 \up0 \expndtw0\charscalex182 \ul0\nosupersub\cf8\f9\fs18 tilada tr
atada con las cantidades especificadas de todos los reacti-\par\pard\ql \li2145\
sb134\sl-230\slmult0 \up0 \expndtw0\charscalex160 \ul0\nosupersub\cf9\f10\fs20 v
os, excepto con la solucion patron de hierro. Alternativamente, si \par\pard\qj
\li2140\ri1169\sb3\sl-360\slmult0 \up0 \expndtw0\charscalex175 \ul0\nosupersub\c
f8\f9\fs18 se use agua destilada como referencia, deben corregirse los valores \
line \up0 \expndtw0\charscalex171 de absorbancia Para las concentraciones patron
de hierro sustrayendo \line \up0 \expndtw0\charscalex176 la absorbancia Para un
blanco de reactivos leido contra agua destila \line \up0 \expndtw0\charscalex14
9 da. \par\pard\qj \li2126\ri1173\sb0\sl-360\slmult0\fi4 \up0 \expndtw0\charscal
ex172 Con los datos obtenidos se construye una curve de calibraci6n de ab\up0 \e
xpndtw0\charscalex169 sorbancia contra mg de hierro. \par\pard\li2097\sb0\sl-207
\slmult0\par\pard\li2097\sb39\sl-207\slmult0\fi28\tx3009\tx5659\tx6038\tx6302 \d
n3 \expndtw0\charscalex165 7.1.2\tab \dn2 \expndtw0\charscalex165 \ul0\nosupersu
b\cf7\f8\fs18\ul Para un intervalo de\tab \up0 \expndtw0\charscalex124 50\tab \u
p0 \expndtw-2\charscalex100 a\tab \dn2 \expndtw0\charscalex165 500,9 Fe/100 ml d
e solucion final\ul0\nosupersub\cf8\f9\fs18 .\par\pard\li2097\sb162\sl-207\slmul
t0\fi14\tx7555\tx10550 \dn2 \expndtw0\charscalex165 Se sigue el procedimiento es
pecificado on\tab \dn2 \expndtw0\charscalex165 7.1.1, Pero utilizando\tab \up0 \
expndtw0\charscalex165 10,\par\pard\li2097\sb139\sl-207\slmult0\fi19\tx2630\tx31
53\tx3542\tx3801\tx4190\tx8337 \up0 \expndtw0\charscalex165 20,\tab \up0 \expndt
w0\charscalex165 30,\tab \up0 \expndtw0\charscalex129 40\tab \up0 \expndtw-2\cha
rscalex100 y\tab \up0 \expndtw0\charscalex129 50\tab \dn2 \expndtw0\charscalex16
5 ml de solucion patron de hierro\tab \dn2 \expndtw0\charscalex165 (5.15.1) y se
mide\par\pard\li2097\sb158\sl-207\slmult0\fi14\tx5740\tx5990 \up0 \expndtw0\cha
rscalex165 la absorbancia en celdas de\tab \up0 \expndtw0\charscalex165 1\tab \u
p0 \expndtw0\charscalex165 cm.\par\pard\li2097\sb0\sl-207\slmult0\par\pard\li209

7\sb56\sl-207\slmult0\fi14\tx2755 \up0 \expndtw0\charscalex165 7.2\tab \up0 \exp

ndtw0\charscalex165 HIERRO TOTAL\par\pard\li2097\sb0\sl-207\slmult0\par\pard\li2
097\sb71\sl-207\slmult0\fi4\tx3009\tx8975\tx9355 \up0 \expndtw0\charscalex165 7.
2.1\tab \dn2 \expndtw0\charscalex165 Se mezola la muestra vigorosamente y se mid
en\tab \up0 \expndtw0\charscalex121 50\tab \up0 \expndtw0\charscalex165 ml en un
ma-\par\pard\li2097\sb158\sl-207\slmult0\fi9\tx4574\tx5073\tx5476\tx9484\tx9744
\up0 \expndtw0\charscalex165 traz Erlenmeyer de\tab \up0 \expndtw0\charscalex12
4 125\tab \up0 \expndtw0\charscalex117 ml\tab \dn2 \expndtw0\charscalex165 (Si l
a muestra contiene mas de\tab \up0 \expndtw-2\charscalex100 2\tab \up0 \expndtw0
\charscalex165 mg de\par\pard\li2097\sb162\sl-207\slmult0\fi0 \up0 \expndtw0\cha
rscalex165 Fe/l, se diluye una porcion medida exactamente que contenga no mas\pa
r\pard\li2097\sb149\sl-207\slmult0\fi4\tx2491\tx3787\tx4171 \dn2 \expndtw0\chars
calex121 do\tab \up0 \expndtw0\charscalex140 100 /zAg a\tab \up0 \expndtw0\chars
calex127 50\tab \dn2 \expndtw0\charscalex165 ml, o as utilize mas fenantrolina y
un Paso de luz\par\pard\sect\sectd\fs24\paperw12240\paperh15840{\bkmkstart Pg10
}{\bkmkend Pg10}\par\pard\ql \li10339\sb0\sl-207\slmult0 \par\pard\ql\li10339\sb
0\sl-207\slmult0 \par\pard\ql\li10339\sb0\sl-207\slmult0 \par\pard\ql\li10339\sb
0\sl-207\slmult0 \par\pard\ql\li10339\sb0\sl-207\slmult0 \par\pard\ql\li10339\sb
0\sl-207\slmult0 \par\pard\ql\li10339\sb0\sl-207\slmult0 \par\pard\ql\li10339\sb
0\sl-207\slmult0 \par\pard\ql\li10339\sb0\sl-207\slmult0 \par\pard\ql\li10339\sb
86\sl-207\slmult0 \up0 \expndtw0\charscalex167 \ul0\nosupersub\cf8\f9\fs18 /7 \p
ar\pard\li2092\sb0\sl-207\slmult0\par\pard\li2092\sb0\sl-207\slmult0\par\pard\li
2092\sb206\sl-207\slmult0\fi91\tx2577\tx2827\tx3091\tx3345 \up0 \expndtw0\charsc
alex169 de\tab \up0 \expndtw0\charscalex169 1\tab \up0 \expndtw-2\charscalex100
6\tab \up0 \expndtw-2\charscalex100 2\tab \up0 \expndtw0\charscalex169 cm).\par\
pard\li2092\sb0\sl-207\slmult0\par\pard\li2092\sb71\sl-207\slmult0\fi86\tx3076\t
x4521\tx4776\tx9695\tx9945 \up0 \expndtw0\charscalex169 7.2.2\tab \up0 \expndtw0
\charscalex159 Se agregan\tab \up0 \expndtw-2\charscalex100 2\tab \up0 \expndtw0
\charscalex169 ml de acido clorhidrico concentrado y\tab \up0 \expndtw0\charscal
ex169 1\tab \up0 \expndtw0\charscalex169 ml de\par\pard\li2092\sb163\sl-207\slmu
lt0\fi76 \up0 \expndtw0\charscalex169 soluci6n de hidroxilamina. Se agregan unas
paces perlas de vidrio\par\pard\li2092\sb153\sl-207\slmult0\fi81 \up0 \expndtw0
\charscalex169 y as calienta a ebullici6n. Para asegurar la disoluci6n de todo e
l\par\pard\li2092\sb158\sl-207\slmult0\fi76 \up0 \expndtw0\charscalex169 hierro,
se continua la ebullici6n haste que el volumen se reduzca a\par\pard\li2092\sb1
43\sl-207\slmult0\fi81\tx2543\tx2812\tx3201\tx3868\tx9676\tx10065 \up0 \expndtw0
\charscalex119 15\tab \up0 \expndtw-2\charscalex100 -\tab \up0 \expndtw0\charsca
lex127 20\tab \up0 \expndtw0\charscalex169 ml.\tab \dn2 \expndtw0\charscalex169
(Si la muestra se incinera coma se describi6\tab \dn2 \expndtw0\charscalex118 \u
l0\nosupersub\cf9\f10\fs20 an\tab \dn2 \expndtw0\charscalex169 \ul0\nosupersub\c
f8\f9\fs18 6.1.4,\par\pard\li2092\sb163\sl-207\slmult0\fi67\tx5280\tx5529 \dn2 \
expndtw0\charscalex169 se retoma el residua an\tab \up0 \expndtw-2\charscalex100
2\tab \dn2 \expndtw0\charscalex169 ml de acido clorhidrico concentrado y 5 ml\p
ar\pard\li2092\sb148\sl-207\slmult0\fi67 \up0 \expndtw0\charscalex169 de agua de
stilada). Se enfria a temperature ambiente y se transfie\par\pard\li2092\sb148\s
l-207\slmult0\fi57\tx5524\tx5899\tx6172\tx6686 \up0 \expndtw0\charscalex169 re a
un matraz aforado de\tab \up0 \expndtw0\charscalex127 50\tab \dn2 \expndtw-2\ch
arscalex100 -\tab \dn2 \expndtw0\charscalex130 100\tab \dn2 \expndtw0\charscalex
169 ml a a un tuba de Nessler. Se\par\pard\li2092\sb148\sl-207\slmult0\fi52\tx32
01\tx3585\tx9412\tx9667 \up0 \expndtw0\charscalex153 agregan\tab \up0 \expndtw0\
charscalex124 10\tab \dn2 \expndtw0\charscalex169 ml de soluci6n buffer de aceta
to de amonio y\tab \up0 \expndtw-2\charscalex100 2\tab \up0 \expndtw0\charscalex
169 ml de so-\par\pard\li2092\sb144\sl-230\slmult0\fi62 \up0 \expndtw0\charscale
x169 \ul0\nosupersub\cf9\f10\fs20 luci6n de fenantrolina, se diluye hasta el afo
ro con ague destila=\par\pard\li2092\sb149\sl-207\slmult0\fi67\tx9672\tx10051 \d
n2 \expndtw0\charscalex169 \ul0\nosupersub\cf8\f9\fs18 da, as mezcla a agita fue
rtemente y se deja an reposo par\tab \up0 \expndtw0\charscalex124 10\tab \up0 \e
xpndtw0\charscalex120 a\par\pard\li2092\sb143\sl-207\slmult0\fi62\tx2534 \up0 \e
xpndtw0\charscalex124 15\tab \up0 \expndtw0\charscalex169 min Para desarrollar e
l color al maxima.\par\pard\li2092\sb0\sl-230\slmult0\par\pard\li2092\sb24\sl-23

0\slmult0\fi57\tx2798 \up0 \expndtw0\charscalex169 \ul0\nosupersub\cf9\f10\fs20

7.3\tab \dn2 \expndtw0\charscalex169 HIERRO FILTRABLE\par\pard\li2092\sb0\sl-230
\slmult0\par\pard\li2092\sb25\sl-230\slmult0\fi52\tx3067 \up0 \expndtw0\charscal
ex169 7.3.1\tab \dn2 \expndtw0\charscalex169 Inmediatamente despues de recolecta
r la muestra, as filtra a\par\pard\li2092\sb130\sl-230\slmult0\fi52\tx6806 \up0
\expndtw0\charscalex154 traves de una membrane filtrante de\tab \up0 \expndtw0\c
harscalex169 0,45/4.m a un matraz de vacio\par\pard\li2092\sb149\sl-207\slmult0\
fi43\tx3840\tx4084\tx9916\tx10430 \up0 \expndtw0\charscalex157 \ul0\nosupersub\c
f8\f9\fs18 qua contenga\tab \up0 \expndtw0\charscalex169 1\tab \dn2 \expndtw0\ch
arscalex169 ml de acido clorhidrico concentrado par cada\tab \dn2 \expndtw0\char
scalex132 100\tab \up0 \expndtw0\charscalex169 ml\par\pard\li2092\sb134\sl-230\s
lmult0\fi43 \up0 \expndtw0\charscalex169 \ul0\nosupersub\cf9\f10\fs20 de muestra
.\par\pard\li2092\sb0\sl-230\slmult0\par\pard\li2092\sb20\sl-230\slmult0\fi33\tx
3028 \up0 \expndtw0\charscalex169 7.3.2\tab \dn2 \expndtw0\charscalex169 Se anal
iza el filtrado Para determiner hierro filtrable to-\par\pard\li2092\sb149\sl-20
7\slmult0\fi33\tx2783\tx7315\tx8356 \up0 \expndtw0\charscalex169 \ul0\nosupersub
\cf8\f9\fs18 tal\tab \dn2 \expndtw0\charscalex169 (7.2) y/o hierro ferroso filtr
able\tab \dn2 \expndtw0\charscalex169 (7.4).\tab \dn2 \expndtw0\charscalex169 (E
ste procedimiento\par\pard\li2092\sb163\sl-207\slmult0\fi33 \up0 \expndtw0\chars
calex169 tambi6n puede ser utilizado an el laboratorio, con el conocimiento\par\
pard\li2092\sb153\sl-207\slmult0\fi28 \up0 \expndtw0\charscalex169 de que la exp
osici6n normal de la muestra al aire durante ei envio\par\pard\li2092\sb153\sl-2
07\slmult0\fi14 \up0 \expndtw0\charscalex169 puede provocar la precipitaci6n del
hierro).\par\pard\li2092\sb0\sl-207\slmult0\par\pard\li2092\sb61\sl-207\slmult0
\fi19\tx3014 \up0 \expndtw0\charscalex169 7.3.3\tab \up0 \expndtw0\charscalex169
Se calcula el hierro suspendido par diferencia entre el hie-\par\pard\li2092\sb
153\sl-207\slmult0\fi14 \up0 \expndtw0\charscalex169 rro filtrable y el hierro t
otal.\par\pard\li2092\sb0\sl-230\slmult0\par\pard\li2092\sb19\sl-230\slmult0\fi4
\tx2755 \up0 \expndtw0\charscalex169 \ul0\nosupersub\cf9\f10\fs20 7.4\tab \dn2 \
expndtw0\charscalex169 HIERRO FERROSO\par\pard\li2092\sb0\sl-207\slmult0\par\par
d\li2092\sb62\sl-207\slmult0\fi0\tx3009 \up0 \expndtw0\charscalex169 \ul0\nosupe
rsub\cf8\f9\fs18 7.4.1\tab \dn3 \expndtw0\charscalex169 Para determiner hierro f
erroso, as acidifica una muestra par\par\pard\li2092\sb153\sl-207\slmult0\fi0\tx
3787\tx4046\tx9883\tx10396 \up0 \expndtw0\charscalex160 separado con\tab \up0 \e
xpndtw-2\charscalex100 2\tab \dn2 \expndtw0\charscalex169 ml de acido clorhidric
o concentrado par cada\tab \up0 \expndtw0\charscalex132 100\tab \up0 \expndtw0\c
harscalex169 ml\par\pard\ql \li2097\sb156\sl-207\slmult0 \up0 \expndtw0\charscal
ex172 de muestra an el momenta de la recoleccio'n Para prevenir la oxida-\par\pa
rd\sect\sectd\fs24\paperw12240\paperh15840{\bkmkstart Pg11}{\bkmkend Pg11}\par\p
ard\ql \li10415\sb0\sl-207\slmult0 \par\pard\ql\li10415\sb0\sl-207\slmult0 \par\
pard\ql\li10415\sb0\sl-207\slmult0 \par\pard\ql\li10415\sb0\sl-207\slmult0 \par\
pard\ql\li10415\sb0\sl-207\slmult0 \par\pard\ql\li10415\sb0\sl-207\slmult0 \par\
pard\ql\li10415\sb0\sl-207\slmult0 \par\pard\ql\li10415\sb0\sl-207\slmult0 \par\
pard\ql\li10415\sb0\sl-207\slmult0 \par\pard\ql\li10415\sb86\sl-207\slmult0 \up0
\expndtw0\charscalex167 \ul0\nosupersub\cf8\f9\fs18 /8 \par\pard\ql \li2140\sb0
\sl-207\slmult0 \par\pard\ql\li2140\sb0\sl-207\slmult0 \par\pard\ql\li2140\sb59\
sl-207\slmult0 \up0 \expndtw0\charscalex187 ci6n. Se llena la botella directamen
te de la fuente y se tapa. \par\pard\li2136\sb0\sl-207\slmult0\par\pard\li2136\s
b68\sl-207\slmult0\fi9\tx3067\tx10425 \dn2 \expndtw0\charscalex165 7.4.2\tab \dn
2 \expndtw0\charscalex165 Inmediatamente antes del analisis se toma una porcion
de\tab \up0 \expndtw0\charscalex165 50 ml\par\pard\li2136\sb148\sl-207\slmult0\f
i9 \up0 \expndtw0\charscalex166 de is muestra acidificada y se agrega 20 ml de s
olucion de fenantrolina y\par\pard\li2136\sb148\sl-207\slmult0\fi9\tx2529 \up0 \
expndtw0\charscalex124 10\tab \dn3 \expndtw0\charscalex165 ml de is solucion de
acetato de amonio y se agita vigorosamente.\par\pard\li2136\sb0\sl-230\slmult0\p
ar\pard\li2136\sb29\sl-230\slmult0\fi0\tx3038\tx4612\tx5112\tx10535\tx10790 \up0
\expndtw0\charscalex165 \ul0\nosupersub\cf9\f10\fs20 7.4.3\tab \up0 \expndtw0\c
harscalex155 Se diluye a\tab \dn2 \expndtw0\charscalex115 100\tab \dn2 \expndtw0
\charscalex159 ml y se mide la intensidad de color entre\tab \dn2 \expndtw-2\cha
rscalex100 5\tab \dn2 \expndtw0\charscalex120 a\par\pard\li2136\sb144\sl-207\slm

ult0\fi0\tx2515\tx8342 \up0 \expndtw0\charscalex124 \ul0\nosupersub\cf8\f9\fs18

10\tab \dn2 \expndtw0\charscalex165 minutos. No debe exponerse a la luz solar.\t
ab \dn2 \expndtw0\charscalex165 (El color se desarro-\par\pard\qj \li2107\ri1196
\sb35\sl-360\slmult0\fi23 \up0 \expndtw0\charscalex176 lla rapidamente an presen
cia de un exceso de fenantrolina. El volu\up0 \expndtw0\charscalex169 men de fen
antrolina dado as adecuado pare menos de'50 ^g de hierro \up0 \expndtw0\charscal
ex171 total; si estan presentes cantidades mayores debe usarse un volumen \up0 \
expndtw0\charscalex168 mayor de fenantrolina o un reactivo mas concentrado). \pa
r\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb28\sl-207\slmult0\fi52\tx3014
\up0 \expndtw0\charscalex162 7.4.4\tab \dn2 \expndtw0\charscalex162 Se calcula
el hierro ferrico por diferencia entre el hierro\par\pard\li2063\sb143\sl-230\sl
mult0\fi43 \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf9\f10\fs20 ferroso y e
l hierro total.\par\pard\li2063\sb0\sl-207\slmult0\par\pard\li2063\sb53\sl-207\s
lmult0\fi43\tx2740 \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf8\f9\fs18 7.5\
tab \up0 \expndtw0\charscalex162 fEDICION DEL COLOR\par\pard\li2063\sb0\sl-207\s
lmult0\par\pard\li2063\sb66\sl-207\slmult0\fi38\tx3004 \up0 \expndtw0\charscalex
162 7.5.1\tab \dn3 \expndtw0\charscalex162 Se prepare una aerie de patrones, pip
eteando exactamente volume-\par\pard\li2063\sb148\sl-230\slmult0\fi33 \up0 \expn
dtw0\charscalex163 \ul0\nosupersub\cf9\f10\fs20 nee calculados de soluciones pat
ron de hierro (debe usarse la solucion mas\par\pard\li2063\sb130\sl-230\slmult0\
fi33 \up0 \expndtw0\charscalex143 dilulda Para medir porciones de 1 a 10/ug) a m
atraces Erlenmeyer de 125 ml,\par\pard\li2063\sb120\sl-230\slmult0\fi33\tx3662\t
x4046\tx9340 \up0 \expndtw0\charscalex146 diluyendo a\tab \up0 \expndtw0\charsca
lex114 50\tab \dn2 \expndtw0\charscalex143 ml y continuando como se indica a par
tir de\tab \dn2 \expndtw0\charscalex162 7.2.\par\pard\li2063\sb0\sl-207\slmult0\
par\pard\li2063\sb58\sl-207\slmult0\fi28\tx3004 \up0 \expndtw0\charscalex162 \ul
0\nosupersub\cf8\f9\fs18 7.5.2\tab \up0 \expndtw0\charscalex162 Para comparaci6n
visual, se prepare una aerie de por lo menos\par\pard\li2063\sb134\sl-230\slmul
t0\fi28\tx2471\tx5596\tx5841\tx6115 \up0 \expndtw0\charscalex114 \ul0\nosupersub
\cf9\f10\fs20 10\tab \up0 \expndtw0\charscalex152 patrones an un rango de\tab \u
p0 \expndtw0\charscalex162 1\tab \up0 \expndtw0\charscalex120 a\tab \dn2 \expndt
w0\charscalex162 1OO /c-,g de hierro en el volumen final\par\pard\li2063\sb130\s
l-230\slmult0\fi24\tx2481\tx3000\tx9729\tx10238 \up0 \expndtw0\charscalex118 de\
tab \up0 \expndtw0\charscalex118 100\tab \up0 \expndtw0\charscalex157 ml. Se com
paran los colores an tubos de Nessler de\tab \up0 \expndtw0\charscalex116 100\ta
b \up0 \expndtw0\charscalex162 ml.\par\pard\li2063\sb0\sl-230\slmult0\par\pard\l
i2063\sb15\sl-230\slmult0\fi19\tx2995\tx8553\tx8812 \up0 \expndtw0\charscalex162
7.5.3\tab \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf8\f9\fs18 Para la medi
dafotometrica, se use la Table\tab \up0 \expndtw0\charscalex162 1\tab \up0 \expn
dtw0\charscalex162 como guia Para\par\pard\li2063\sb154\sl-207\slmult0\fi14 \up0
\expndtw0\charscalex162 seleccionar el Paso de luz apropiado. Se lean los patro
nes contra\par\pard\li2063\sb148\sl-207\slmult0\fi14\tx5971\tx6460\tx8947 \up0 \
expndtw0\charscalex162 un blanco de ague destilada a\tab \up0 \expndtw0\charscal
ex130 100\tab \dn3 \expndtw0\charscalex162 % de transmitancia\tab \up0 \expndtw0
\charscalex162 (absorbancia ce-\par\pard\li2063\sb153\sl-207\slmult0\fi9\tx10497
\up0 \expndtw0\charscalex162 ro) y se construye una curve de calibracion incluy
endo un blanco\tab \up0 \expndtw0\charscalex162 (ver\par\pard\li2063\sb129\sl-23
0\slmult0\fi9\tx3120 \up0 \expndtw0\charscalex145 \ul0\nosupersub\cf9\f10\fs20 s
eccion\tab \up0 \expndtw0\charscalex162 5.6).\par\pard\li2063\sb0\sl-207\slmult0
\par\pard\li2063\sb57\sl-207\slmult0\fi9\tx2976 \up0 \expndtw0\charscalex162 \ul
0\nosupersub\cf8\f9\fs18 7.5.4\tab \up0 \expndtw0\charscalex162 Si las muestras
estan coloreadas o turbias, se hace una se-\par\pard\li2063\sb139\sl-230\slmult0
\fi4 \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf9\f10\fs20 gunda serie de mu
estras siguiendo todas las etapas del procedimien-\par\pard\li2063\sb149\sl-207\
slmult0\fi4 \up0 \expndtw0\charscalex162 \ul0\nosupersub\cf8\f9\fs18 to sin adic
ionar fenantrolina. En lugar de ague destilada, se usa\par\pard\li2063\sb153\sl207\slmult0\fi0\tx6864\tx7348 \up0 \expndtw0\charscalex162 el blanco Para llevar
el fotometro a\tab \dn2 \expndtw0\charscalex128 100\tab \dn3 \expndtw0\charscal
ex162 % de transmitencia y se\par\pard\sect\sectd\fs24\paperw12240\paperh15840{\
bkmkstart Pg12}{\bkmkend Pg12}\par\pard\ql \li10339\sb0\sl-253\slmult0 \par\pard

\ql\li10339\sb0\sl-253\slmult0 \par\pard\ql\li10339\sb0\sl-253\slmult0 \par\pard

\ql\li10339\sb0\sl-253\slmult0 \par\pard\ql\li10339\sb0\sl-253\slmult0 \par\pard
\ql\li10339\sb0\sl-253\slmult0 \par\pard\ql\li10339\sb0\sl-253\slmult0 \par\pard
\ql\li10339\sb140\sl-253\slmult0 \up0 \expndtw0\charscalex143 \ul0\nosupersub\cf
16\f17\fs26 /\ul0\sub\cf8\f9\fs27 9 \par\pard\ql \li2049\sb0\sl-360\slmult0 \par
\pard\ql\li2049\sb0\sl-360\slmult0 \par\pard\ql\li2049\ri1389\sb139\sl-360\slmul
t0\fi9 \up0 \expndtw0\charscalex180 lee cada desarrollo de las muestras con fena
ntrolina con el corres-\line \up0 \expndtw0\charscalex180 pondiente blanco sin f
enantrolina. Se transforman las lectures ob-\line \up0 \expndtw0\charscalex177 t
enidas en el fotometro en valores de hierro mediante la curve de \line \up0 \exp
ndtw0\charscalex174 calibracion. \par\pard\qj \li2035\ri1407\sb20\sl-360\slmult0
\fi4 \up0 \expndtw0\charscalex170 Este procedimiento no compensa la presencia de
Tones interferentes. \up0 \expndtw0\charscalex175 Si el color y la turbiedad es
ta'n ausentes, es ma's ra'pido e igualmen \up0 \expndtw0\charscalex187 to satisf
actorio leer las muestras, al igual que los patrones, con\up0 \expndtw0\charscal
ex181 tra ague destilada. \par\pard\li3057\sb0\sl-230\slmult0\par\pard\li3057\sb
0\sl-230\slmult0\par\pard\li3057\sb14\sl-230\slmult0\fi0\tx3849\tx4358 \up0 \exp
ndtw-9\charscalex100 \ul0\nosupersub\cf9\f10\fs20 TABLA\tab \up0 \expndtw0\chars
calex156 1.\tab \up0 \expndtw0\charscalex156 \ul0\nosupersub\cf10\f11\fs20\ul Se
leccion de la longitud del peso de\par\pard\li3057\sb154\sl-207\slmult0\fi1305 \
up0 \expndtw0\charscalex156 \ul0\nosupersub\cf7\f8\fs18\ul luz Para varies conce
ntraciones de\par\pard\li3057\sb134\sl-230\slmult0\fi3110 \up0 \expndtw0\charsca
lex156 \ul0\nosupersub\cf10\f11\fs20\ul hierro\ul0\nosupersub\cf9\f10\fs20 .\par
\pard\li2793\sb0\sl-230\slmult0\par\pard\li2793\sb0\sl-230\slmult0\par\pard\li27
93\sb25\sl-230\slmult0\fi1732 \up0 \expndtw0\charscalex136 \u-3?,cg Fe\par\pard\
li2793\sb34\sl-207\slmult0\fi5438 \up0 \expndtw0\charscalex136 \ul0\nosupersub\c
f8\f9\fs18 Paso de Luz\par\pard\li2793\sb37\sl-207\slmult0\fi0\tx5515 \up0 \expn
dtw0\charscalex136 Volumen Final\tab \up0 \expndtw0\charscalex136 Volumen Final\
par\pard\li2793\sb125\sl-230\slmult0\fi518\tx3700\tx5913\tx6484\tx8745 \up0 \exp
ndtw0\charscalex136 \ul0\nosupersub\cf9\f10\fs20 50\tab \up0 \expndtw0\charscale
x136 ml\tab \up0 \expndtw0\charscalex136 100\tab \up0 \expndtw0\charscalex136 -m
l\tab \up0 \expndtw0\charscalex136 cm\par\pard\li2793\sb0\sl-230\slmult0\par\par
d\li2793\sb140\sl-230\slmult0\fi384\tx5908\tx8884 \up0 \expndtw0\charscalex136 5
0-200\tab \up0 \expndtw0\charscalex136 100-400\tab \up0 \expndtw0\charscalex136
1\par\pard\li2793\sb154\sl-207\slmult0\fi379\tx6028\tx8870 \up0 \expndtw0\charsc
alex136 \ul0\nosupersub\cf8\f9\fs18 25-100\tab \up0 \expndtw0\charscalex136 50-2
00\tab \up0 \expndtw0\charscalex136 2\par\pard\li2793\sb148\sl-207\slmult0\fi384
\tx3691\tx6024\tx6542\tx8875 \up0 \expndtw0\charscalex136 10-\tab \up0 \expndtw0
\charscalex136 40\tab \up0 \expndtw0\charscalex136 20-\tab \up0 \expndtw0\charsc
alex136 80\tab \up0 \expndtw0\charscalex136 5\par\pard\li2793\sb129\sl-230\slmul
t0\fi508\tx3691\tx6028\tx6537\tx8755 \up0 \expndtw0\charscalex136 \ul0\nosupersu
b\cf9\f10\fs20 5-\tab \up0 \expndtw0\charscalex136 20\tab \up0 \expndtw0\charsca
lex136 10-\tab \up0 \expndtw0\charscalex136 40\tab \up0 \expndtw0\charscalex136
10\par\pard\li1972\sb0\sl-207\slmult0\par\pard\li1972\sb0\sl-207\slmult0\par\par
d\li1972\sb0\sl-207\slmult0\par\pard\li1972\sb133\sl-207\slmult0\fi23\tx2644 \up
0 \expndtw0\charscalex162 \ul0\nosupersub\cf8\f9\fs18 7.6\tab \dn2 \expndtw0\cha
rscalex162 IIUESTRAS QUE CONTIENEN INTERFERENCIAS ORGANICAS\par\pard\li1972\sb0\
sl-207\slmult0\par\pard\li1972\sb47\sl-207\slmult0\fi23\tx2908 \up0 \expndtw0\ch
arscalex162 7.6.1\tab \up0 \expndtw0\charscalex162 Las muestras que contengan su
stancias orga'nicas an cantida-\par\pard\li1972\sb157\sl-207\slmult0\fi14 \up0 \
expndtw0\charscalex162 des sustanciales se digieren de acuerdo a lo siguiente:\p
ar\pard\li1972\sb0\sl-207\slmult0\par\pard\li1972\sb62\sl-207\slmult0\fi4\tx3143
\up0 \expndtw0\charscalex162 7.6.1.1\tab \up0 \expndtw0\charscalex162 Se agita
la muestra Para obtener una suspension homogenea.\par\pard\li1972\sb157\sl-207\s
lmult0\fi0\tx5620\tx9235 \up0 \expndtw0\charscalex155 Se mide un volumen adecuad
o\tab \up0 \expndtw0\charscalex162 (determinado segun la Table\tab \up0 \expndtw
0\charscalex162 2) con Una\par\pard\li1972\sb158\sl-207\slmult0\fi0 \up0 \expndt
w0\charscalex162 pipeta o matraz aforado y se transfiere a una capsula de evapor
acion\par\pard\li1972\sb158\sl-207\slmult0\fi14\tx6767\tx7281 \dn2 \expndtw0\cha
rscalex162 (si el volumen requerido as mayor de\tab \up0 \expndtw0\charscalex131

250\tab \up0 \expndtw0\charscalex162 ml, se transfiere an por-\par\pard\sect\se

ctd\fs24\paperw12240\paperh15840{\bkmkstart Pg13}{\bkmkend Pg13}\par\pard\ql \li
10560\sb0\sl-207\slmult0 \par\pard\ql\li10560\sb0\sl-207\slmult0 \par\pard\ql\li
10560\sb0\sl-207\slmult0 \par\pard\ql\li10560\sb0\sl-207\slmult0 \par\pard\ql\li
10560\sb0\sl-207\slmult0 \par\pard\ql\li10560\sb0\sl-207\slmult0 \par\pard\ql\li
10560\sb0\sl-207\slmult0 \par\pard\ql\li10560\sb0\sl-207\slmult0 \par\pard\ql\li
10560\sb0\sl-207\slmult0 \par\pard\ql\li10560\sb106\sl-207\slmult0 \up0 \expndtw
0\charscalex159 \ul0\nosupersub\cf8\f9\fs18 /10 \par\pard\ql \li2260\sb0\sl-207\
slmult0 \par\pard\ql\li2260\sb0\sl-207\slmult0 \par\pard\ql\li2260\sb0\sl-207\sl
mult0 \par\pard\ql\li2260\sb12\sl-207\slmult0 \up0 \expndtw0\charscalex169 cione
s coma los evaporados de la muestra). \par\pard\li4065\sb0\sl-207\slmult0\par\pa
rd\li4065\sb0\sl-207\slmult0\par\pard\li4065\sb105\sl-207\slmult0\fi0\tx4852\tx5
366 \up0 \expndtw0\charscalex100 TABLA\tab \up0 \expndtw0\charscalex127 2.\tab \
up0 \expndtw0\charscalex127 \ul0\nosupersub\cf7\f8\fs18\ul Volumen de muestra a
medir\par\pard\li4065\sb0\sl-207\slmult0\par\pard\li4065\sb0\sl-207\slmult0\par\
pard\li4065\sb99\sl-207\slmult0\fi383\tx7291 \up0 \expndtw0\charscalex127 \ul0\n
osupersub\cf8\f9\fs18 CONCENTRACION\tab \up0 \expndtw0\charscalex127 UOLUPIEN\pa
r\pard\li4065\sb148\sl-207\slmult0\fi782\tx7435 \up0 \expndtw0\charscalex127 (mg
/l)\tab \up0 \expndtw0\charscalex127 (ml)\par\pard\li4065\sb0\sl-230\slmult0\par
\pard\li4065\sb149\sl-230\slmult0\fi3360 \up0 \expndtw0\charscalex127 \ul0\nosup
ersub\cf9\f10\fs20 1000\par\pard\li4065\sb0\sl-207\slmult0\par\pard\li4065\sb57\
sl-207\slmult0\fi902\tx5207\tx5735\tx7550 \up0 \expndtw0\charscalex127 \ul0\nosu
persub\cf8\f9\fs18 1\tab \up0 \expndtw0\charscalex120 -\tab \up0 \expndtw0\chars
calex127 10\tab \up0 \expndtw0\charscalex127 100\par\pard\li4065\sb0\sl-207\slmu
lt0\par\pard\li4065\sb76\sl-207\slmult0\fi763\tx5203\tx5601\tx7675 \up0 \expndtw
0\charscalex127 10\tab \up0 \expndtw0\charscalex120 -\tab \up0 \expndtw0\charsca
lex127 100\tab \up0 \expndtw0\charscalex127 10\par\pard\li4065\sb134\sl-230\slmu
lt0\fi633\tx5198\tx5472\tx7800 \up0 \expndtw0\charscalex127 \ul0\nosupersub\cf9\
f10\fs20 100\tab \up0 \expndtw0\charscalex120 -\tab \up0 \expndtw0\charscalex127
1000\tab \up0 \expndtw0\charscalex127 1\par\pard\li2188\sb0\sl-207\slmult0\par\
pard\li2188\sb0\sl-207\slmult0\par\pard\li2188\sb0\sl-207\slmult0\par\pard\li218
8\sb0\sl-207\slmult0\par\pard\li2188\sb26\sl-207\slmult0\fi28\tx3383 \up0 \expnd
tw0\charscalex173 \ul0\nosupersub\cf8\f9\fs18 7.6.1.2\tab \dn3 \expndtw0\charsca
lex173 Se acidifica an presencia de anaranjado de metilo con aci-\par\pard\li218
8\sb153\sl-207\slmult0\fi23\tx7660\tx7915 \up0 \expndtw0\charscalex173 do sulfur
ico concentrado, luego se agrega\tab \up0 \expndtw-2\charscalex100 5\tab \up0 \e
xpndtw0\charscalex173 ml de acido nitrico con\par\pard\li2188\sb149\sl-207\slmul
t0\fi28\tx3643\tx3907\tx9475\tx9849 \up0 \expndtw0\charscalex166 centrado y\tab
\up0 \expndtw-2\charscalex100 2\tab \up0 \expndtw0\charscalex170 ml de soluci6n
de per6xido de hidr6geno al\tab \up0 \expndtw0\charscalex127 30\tab \up0 \expndt
w0\charscalex173 %, para\par\pard\li2188\sb153\sl-207\slmult0\fi23 \up0 \expndtw
0\charscalex173 reducir los cromatos. Se evapora en4baf1o de vapor a an plancha
de\par\pard\li2188\sb148\sl-207\slmult0\fi28\tx5855\tx6225\tx6489\tx6878 \up0 \e
xpndtw0\charscalex170 calentamiento haste obtener\tab \up0 \expndtw0\charscalex1
19 15\tab \up0 \expndtw-2\charscalex100 a\tab \up0 \expndtw0\charscalex130 20\ta
b \up0 \expndtw0\charscalex173 ml cubriendo el envase con un\par\pard\li2188\sb1
53\sl-207\slmult0\fi23 \up0 \expndtw0\charscalex173 vidrio de reloj, cuando sea
necesario, para evitar perdidas de mate\par\pard\li2188\sb148\sl-207\slmult0\fi2
3 \up0 \expndtw0\charscalex173 rial par salpicaduras. Puede colocarse una lampar
a infraroja sabre\par\pard\li2188\sb148\sl-207\slmult0\fi23 \up0 \expndtw0\chars
calex173 la muestra para acelerar la evaporaci6n.\par\pard\li2188\sb0\sl-207\slm
ult0\par\pard\li2188\sb61\sl-207\slmult0\fi14\tx3379 \up0 \expndtw0\charscalex17
3 7.6.1.3\tab \up0 \expndtw0\charscalex173 La soluci6n evaporada se transfiere j
unto con cualquier\par\pard\li2188\sb153\sl-207\slmult0\fi9\tx8947\tx9455 \up0 \
expndtw0\charscalex173 s6lido remenente en la place, a un matraz c6nico de\tab \
up0 \expndtw0\charscalex128 125\tab \up0 \expndtw0\charscalex173 ml. Se a-\par\p
ard\li2188\sb149\sl-207\slmult0\fi4\tx3110\tx3364 \up0 \expndtw0\charscalex152 g
regan\tab \up0 \expndtw-2\charscalex100 5\tab \up0 \expndtw0\charscalex173 ml de
acido nitrico concentrado que fue usado pare enjua-\par\pard\li2188\sb148\sl-20
7\slmult0\fi0\tx6215\tx6595 \up0 \expndtw0\charscalex173 gar la capsula de evapo

raci6n;\tab \up0 \expndtw0\charscalex124 10\tab \up0 \expndtw0\charscalex173 ml

de acido sulfurico concentra-\par\pard\qj \li2174\ri1255\sb24\sl-360\slmult0\fi1
4 \up0 \expndtw0\charscalex176 do; unas perlas de vidrio, astillas de carborundu
m a granulos Hen-\line \up0 \expndtw0\charscalex177 gar para minimizer la ebulli
ci6n. Se evapora sabre una plancha de \line \up0 \expndtw0\charscalex170 calenta
miento bajo campana de extracci3n,justo haste que aparezcan \line \up0 \expndtw0
\charscalex167 an el matraz humos blancos densos de SO3, pero no debe continuars
e \line \up0 \expndtw0\charscalex184 el calentamiento mas ally de este punto. Si
'la soluci6n no as cla-\line \up0 \expndtw0\charscalex177 ra, se agregan \up0 \e
xpndtw0\charscalex127 10 \up0 \expndtw0\charscalex180 ml de acido nitrico y se r
epite la evaporaci6n \par\pard\sect\sectd\fs24\paperw12240\paperh15840{\bkmkstar
t Pg14}{\bkmkend Pg14}\par\pard\ql \li10276\sb0\sl-207\slmult0 \par\pard\ql\li10
276\sb0\sl-207\slmult0 \par\pard\ql\li10276\sb0\sl-207\slmult0 \par\pard\ql\li10
276\sb0\sl-207\slmult0 \par\pard\ql\li10276\sb0\sl-207\slmult0 \par\pard\ql\li10
276\sb0\sl-207\slmult0 \par\pard\ql\li10276\sb0\sl-207\slmult0 \par\pard\ql\li10
276\sb0\sl-207\slmult0 \par\pard\ql\li10276\sb113\sl-207\slmult0 \up0 \expndtw0\
charscalex145 \ul0\nosupersub\cf8\f9\fs18 /11 \par\pard\qj \li1977\sb0\sl-360\sl
mult0 \par\pard\qj\li1977\ri1333\sb167\sl-360\slmult0\fi14 \up0 \expndtw0\charsc
alex175 haste obtener humos de S03. Debe asegurarse que todo el acido nitri \up0
\expndtw0\charscalex178 co ha sido eliminado, Como lo indica la claridad de la
soluci6n y la \up0 \expndtw0\charscalex166 ausencia de humos marrones an el matr
az. \par\pard\li1982\sb0\sl-207\slmult0\par\pard\li1982\sb58\sl-207\slmult0\fi4\
tx3153 \up0 \expndtw0\charscalex170 7.6.1.4\tab \dn2 \expndtw0\charscalex170 Se
enfria a temperature ambiente y se diluye cuidadosamen-\par\pard\li1982\sb153\sl
-207\slmult0\fi0\tx3158\tx3547 \up0 \expndtw0\charscalex170 te haste\tab \up0 \e
xpndtw0\charscalex127 50\tab \dn2 \expndtw0\charscalex170 ml aproximadamente con
agua bidestilada. Se calienta\par\pard\ql \li1963\ri1335\sb35\sl-353\slmult0\fi
14 \up0 \expndtw0\charscalex180 haste cerca del punto de ebullicion pars disolve
r lentamente las sa-\line \up0 \expndtw0\charscalex190 les solubles y se filtra
a traves de un crisol filtro de porcelana \line \up0 \expndtw0\charscalex177 o v
idrio sinterizado, a un matraz de filtraci6n cuidadosamente lim-\line \up0 \expn
dtw0\charscalex166 pio. \par\pard\li1905\sb0\sl-207\slmult0\par\pard\li1905\sb59
\sl-207\slmult0\fi62\tx3134 \up0 \expndtw0\charscalex166 7.6.1.5\tab \dn2 \expnd
tw0\charscalex166 Se enjuaga el matraz de la muestra con dos porciones de\par\pa
rd\li1905\sb148\sl-207\slmult0\fi57\tx2222 \up0 \expndtw-2\charscalex100 5\tab \
dn2 \expndtw0\charscalex166 ml de agua bidestilada, pasandola a traves del criso
l pars lavar\par\pard\li1905\sb158\sl-207\slmult0\fi57\tx5731 \up0 \expndtw0\cha
rscalex166 cualquier residuo del filtro\tab \up0 \expndtw0\charscalex166 (puede
usarse un dispositivo de filtra-\par\pard\li1905\sb139\sl-230\slmult0\fi48 \up0
\expndtw0\charscalex166 \ul0\nosupersub\cf9\f10\fs20 cion que permita la recolec
cion del filtrado directamente an un ma-\par\pard\li1905\sb144\sl-207\slmult0\fi
62\tx4056\tx4560\tx5327 \up0 \expndtw0\charscalex166 \ul0\nosupersub\cf8\f9\fs18
traz aforado de\tab \up0 \expndtw0\charscalex130 100\tab \up0 \expndtw0\charsca
lex166 ml).\tab \up0 \expndtw0\charscalex166 Se transfiere el filtrado a un matr
az afo-\par\pard\li1905\sb129\sl-230\slmult0\fi52\tx3014\tx3527 \up0 \expndtw0\c
harscalex146 \ul0\nosupersub\cf9\f10\fs20 redo de\tab \up0 \expndtw0\charscalex1
18 100\tab \up0 \expndtw0\charscalex166 ml y se enjuaga el matraz de filtraci6n
con dos porcio-\par\pard\li1905\sb135\sl-230\slmult0\fi52\tx2870\tx3129 \up0 \ex
pndtw0\charscalex145 nes de\tab \up0 \expndtw-2\charscalex100 5\tab \up0 \expndt
w0\charscalex166 ml de ague bidestilada, agregando estos enjuagues al matraz\par
\pard\li1905\sb130\sl-230\slmult0\fi38\tx9993\tx10507 \up0 \expndtw0\charscalex1
63 aforado. Se diluye el contenido del matraz haste el aforo de\tab \up0 \expndt
w0\charscalex118 100\tab \up0 \expndtw0\charscalex166 ml\par\pard\li1905\sb149\s
l-207\slmult0\fi43 \up0 \expndtw0\charscalex166 \ul0\nosupersub\cf8\f9\fs18 y se
mezcla cuidadosamente. La solucion resultante as alrededor de\par\pard\li1905\s
b129\sl-230\slmult0\fi43\tx2198 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf
9\f10\fs20 3\tab \up0 \expndtw0\charscalex166 N an acido sulfurico. Se toman por
ciones de ella pars la determi-\par\pard\li1905\sb149\sl-207\slmult0\fi38 \up0 \
expndtw0\charscalex166 \ul0\nosupersub\cf8\f9\fs18 nacion de metales.\par\pard\l
i1905\sb0\sl-207\slmult0\par\pard\li1905\sb61\sl-207\slmult0\fi33\tx2841 \up0 \e

xpndtw0\charscalex166 7.6.2\tab \dn2 \expndtw0\charscalex166 Si una muestra dige

rida se ha preparado de acuerdo a lo indi-\par\pard\li1905\sb158\sl-207\slmult0\
fi28\tx2980\tx5443\tx5822\tx10228 \up0 \expndtw0\charscalex166 cado an\tab \up0
\expndtw0\charscalex166 7.6.1, se pipetean\tab \up0 \expndtw0\charscalex121 10\t
ab \dn2 \expndtw0\charscalex166 ml u otra porcion qua contenga de\tab \up0 \expn
dtw0\charscalex166 20\par\pard\li1905\sb125\sl-230\slmult0\fi14\tx2183\tx2707\tx
8030\tx8544\tx9187 \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf9\f10\fs20 a\
tab \up0 \expndtw0\charscalex120 500\tab \up0 \expndtw0\charscalex149 /cug de Fe
an un embudo de separacion de\tab \up0 \expndtw0\charscalex113 125\tab \up0 \ex
pndtw0\charscalex166 ml.\tab \dn2 \expndtw0\charscalex166 Si el volu-\par\pard\l
i1905\sb158\sl-207\slmult0\fi14\tx5054\tx5428 \up0 \expndtw0\charscalex153 \ul0\
nosupersub\cf8\f9\fs18 men tomando as manor de\tab \up0 \expndtw0\charscalex119
10\tab \dn2 \expndtw0\charscalex166 ml se adiciona agua destilada haste obte-\pa
r\pard\li1905\sb148\sl-207\slmult0\fi14\tx2443\tx2832\tx3484\tx8673\tx9052 \up0
\expndtw0\charscalex166 ner\tab \up0 \expndtw0\charscalex127 10\tab \up0 \expndt
w0\charscalex166 ml.\tab \up0 \expndtw0\charscalex166 En el embudo de separacion
se adicionan\tab \up0 \expndtw0\charscalex121 15\tab \up0 \expndtw0\charscalex1
66 ml de acido\par\pard\li1905\sb158\sl-207\slmult0\fi9\tx7502\tx7881 \up0 \expn
dtw0\charscalex166 clorhidrico concentrado pare un volumen de\tab \up0 \expndtw0
\charscalex124 10\tab \up0 \expndtw0\charscalex166 ml, o si la porcion to\par\pa
rd\li1905\sb148\sl-207\slmult0\fi0\tx4137\tx4512\tx6460\tx6604\tx6969 \up0 \expn
dtw0\charscalex155 made as mayor de\tab \up0 \expndtw0\charscalex121 10\tab \up0
\expndtw0\charscalex166 ml, se agregan\tab \up0 \expndtw-4\charscalex100 1\tab
\up0 \expndtw0\charscalex166 ,5\tab \up0 \expndtw0\charscalex166 ml de acido clo
rhidrico con-\par\pard\li1905\sb168\sl-207\slmult0\fi0 \up0 \expndtw0\charscalex
166 centrado/ml de muestra. Se mezcla, se enfria y se procede Como se\par\pard\l
i1905\sb138\sl-207\slmult0\fi4\tx3211 \up0 \expndtw0\charscalex166 indica an\tab
\up0 \expndtw0\charscalex166 7.6.4.\par\pard\sect\sectd\fs24\paperw12240\paperh
15840{\bkmkstart Pg15}{\bkmkend Pg15}\par\pard\ql \li10468\sb0\sl-207\slmult0 \p
ar\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \p
ar\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \p
ar\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \p
ar\pard\ql\li10468\sb0\sl-207\slmult0 \par\pard\ql\li10468\sb0\sl-207\slmult0 \p
ar\pard\ql\li10468\sb166\sl-207\slmult0 \up0 \expndtw0\charscalex155 \ul0\nosupe
rsub\cf8\f9\fs18 /12 \par\pard\li2111\sb0\sl-207\slmult0\par\pard\li2111\sb0\sl207\slmult0\par\pard\li2111\sb146\sl-207\slmult0\fi48\tx3067 \up0 \expndtw0\char
scalex173 7.6.3\tab \up0 \expndtw0\charscalex173 Para preparar una muestra solam
ente Para determiner hierro,\par\pard\li2111\sb158\sl-207\slmult0\fi38\tx7852\tx
8232\tx8500 \up0 \expndtw0\charscalex160 se mide un volumen adecuado que conteng
a de\tab \up0 \expndtw0\charscalex127 20\tab \up0 \expndtw-2\charscalex100 a\tab
\dn2 \expndtw0\charscalex173 500 /%'g de Fe y se\par\pard\li2111\sb153\sl-207\s
lmult0\fi38\tx5520\tx6547 \up0 \expndtw0\charscalex173 digiere coma se indica en
\tab \up0 \expndtw0\charscalex173 7.6.1.\tab \up0 \expndtw0\charscalex173 Sin em
bargo debe usarse solamente\par\pard\li2111\sb143\sl-207\slmult0\fi33\tx2404 \up
0 \expndtw-2\charscalex100 5\tab \up0 \expndtw0\charscalex173 ml de acido sulfur
ico y omitirse el use de per6xido de hidrogeno.\par\pard\li2111\sb167\sl-207\slm
ult0\fi28\tx5385\tx6686\tx10051\tx10430 \up0 \expndtw0\charscalex173 Cuando la d
igestion est6\tab \up0 \expndtw0\charscalex173 complete\tab \dn2 \expndtw0\chars
calex173 (se enfria, se diluye con\tab \up0 \expndtw0\charscalex121 10\tab \up0
\expndtw0\charscalex173 ml\par\pard\li2111\sb158\sl-207\slmult0\fi28 \up0 \expnd
tw0\charscalex173 de agua destilada),se calienta casi a ebullicion Para disolver
len-\par\pard\li2111\sb153\sl-207\slmult0\fi24 \up0 \expndtw0\charscalex173 tam
ente sales solubles y si la muestra esta todavia opaca, se fil-\par\pard\li2111\
sb153\sl-207\slmult0\fi24\tx10425 \dn2 \expndtw0\charscalex173 tra a trav6s de f
ibre de vidrio, vidrio sinterizado o filtro de\tab \up0 \expndtw0\charscalex120
-\par\pard\li2111\sb153\sl-207\slmult0\fi14\tx5116\tx5366\tx5630\tx5884 \dn2 \ex
pndtw0\charscalex167 porcelana, lavando con\tab \up0 \expndtw-2\charscalex100 2\
tab \up0 \expndtw-2\charscalex100 a\tab \up0 \expndtw-2\charscalex100 3\tab \dn2
\expndtw0\charscalex173 ml de agua destilada.\par\pard\li2111\sb0\sl-207\slmult
0\par\pard\li2111\sb61\sl-207\slmult0\fi14\tx3287 \up0 \expndtw0\charscalex173 7

.6.3.1\tab \dn2 \expndtw0\charscalex173 Se transfiere cuantitativamente el filtr

ado o la solucion\par\pard\li2111\sb153\sl-207\slmult0\fi9\tx5884\tx6268 \up0 \e
xpndtw0\charscalex173 clara a un matraz aforado de\tab \up0 \expndtw0\charscalex
124 25\tab \dn2 \expndtw0\charscalex173 ml y se diluye hasta el aforo con\par\pa
rd\li2111\sb153\sl-207\slmult0\fi0 \up0 \expndtw0\charscalex173 ague destilada.
Se vacla el matraz en un embudo de separacion, de\par\pard\li2111\sb149\sl-207\s
lmult0\fi19\tx2640\tx5112\tx5361 \up0 \expndtw0\charscalex126 125\tab \up0 \expn
dtw0\charscalex173 ml, se enjuaga con\tab \up0 \expndtw-2\charscalex100 5\tab \u
p0 \expndtw0\charscalex173 ml de acido clorhidrico concentrado que\par\pard\li21
11\sb153\sl-207\slmult0\fi9\tx6268\tx6652 \up0 \expndtw0\charscalex166 se agrega
al embudo y as anaden\tab \up0 \expndtw0\charscalex124 25\tab \up0 \expndtw0\ch
arscalex173 ml de acido clorhidrico concen-\par\pard\li2111\sb153\sl-207\slmult0
\fi14 \up0 \expndtw0\charscalex173 trado medido con el mismo matraz. Se mezcla y
se enfria a tempera\par\pard\li2111\sb129\sl-230\slmult0\fi9 \up0 \expndtw0\cha
rscalex173 \ul0\nosupersub\cf9\f10\fs20 tura ambiente.\par\pard\li2111\sb0\sl-23
0\slmult0\par\pard\li2111\sb15\sl-230\slmult0\fi9\tx3023 \up0 \expndtw0\charscal
ex173 7.6.4\tab \up0 \expndtw0\charscalex173 \ul0\nosupersub\cf8\f9\fs18 Se extr
ae-.el hierro de la solucion de acido clorhidrico en\par\pard\li2111\sb149\sl-20
7\slmult0\fi0\tx7166\tx7555\tx8332\tx8721 \dn2 \expndtw0\charscalex167 el embudo
de separacion agitandolo por\tab \dn2 \expndtw0\charscalex129 30\tab \dn2 \expn
dtw0\charscalex173 s con\tab \up0 \expndtw0\charscalex127 25\tab \dn2 \expndtw0\
charscalex173 ml de titer iso-\par\pard\qj \li2102\ri1451\sb42\sl-340\slmult0\fi
4 \up0 \expndtw0\charscalex177 propilico. Se transfiere la capa acida a un segun
do embudo de ser, \line \up0 \expndtw0\charscalex178 paracion. Se extrae de nuev
o la solucion acida con \up0 \expndtw0\charscalex124 25 \up0 \expndtw0\charscale
x152 \ul0\nosupersub\cf9\f10\fs20 ml de titer \par\pard\ql \li2088\ri1341\sb10\s
l-353\slmult0\fi14 \up0 \expndtw0\charscalex181 \ul0\nosupersub\cf8\f9\fs18 isop
ropilico, se drena la caps acida en un recipients limpio apro-\line \up0 \expndt
w0\charscalex178 piado y se combinan las dos porciones de titer isopropilico. Se
\line \up0 \expndtw0\charscalex175 vierte la caps acids en el segundo embudo de
separaci6n y se extras \line \dn2 \expndtw0\charscalex160 una vez mss con \up0
\expndtw0\charscalex127 25 \dn2 \expndtw0\charscalex176 ml de titer isopropilico
. Se decanta y se descar \par\pard\ql \li2092\sb148\sl-207\slmult0 \up0 \expndtw
0\charscalex183 to la capa acida y entonces se agrega la caps de titer a las otr
as \par\pard\ql \li2083\sb153\sl-207\slmult0 \up0 \expndtw0\charscalex177 capes
en el embudo de separacion original. La persistencia de un \par\pard\ql \li2083\
sb153\sl-207\slmult0 \up0 \expndtw0\charscalex177 color amarillo en la solucion
de acido clorhidrico despue's de las \par\pard\qj \li2068\ri1245\sb27\sl-360\slm
ult0\fi14 \up0 \expndtw0\charscalex178 tres extracciones no significa una separa
cion incomplete del hierro, \up0 \expndtw0\charscalex178 debido a que el cobra,
el cual no he sido extraido, da un color ama \up0 \expndtw0\charscalex179 rillo
similar. \par\pard\sect\sectd\fs24\paperw12240\paperh15840{\bkmkstart Pg16}{\bkm
kend Pg16}\par\pard\ql \li10324\sb0\sl-207\slmult0 \par\pard\ql\li10324\sb0\sl-2
07\slmult0 \par\pard\ql\li10324\sb0\sl-207\slmult0 \par\pard\ql\li10324\sb0\sl-2
07\slmult0 \par\pard\ql\li10324\sb0\sl-207\slmult0 \par\pard\ql\li10324\sb0\sl-2
07\slmult0 \par\pard\ql\li10324\sb0\sl-207\slmult0 \par\pard\ql\li10324\sb0\sl-2
07\slmult0 \par\pard\ql\li10324\sb173\sl-207\slmult0 \up0 \expndtw0\charscalex15
5 \ul0\nosupersub\cf8\f9\fs18 /13 \par\pard\li2121\sb0\sl-207\slmult0\par\pard\l
i2121\sb0\sl-207\slmult0\par\pard\li2121\sb0\sl-207\slmult0\par\pard\li2121\sb33
\sl-207\slmult0\fi33\tx3321\tx9412\tx9801 \dn2 \expndtw0\charscalex170 7.6.4.1\t
ab \dn2 \expndtw0\charscalex170 Se agitan los extractos etereos combinados con\t
ab \up0 \expndtw0\charscalex127 25\tab \up0 \expndtw0\charscalex170 ml de\par\pa
rd\li2121\sb158\sl-207\slmult0\fi23 \up0 \expndtw0\charscalex170 ague destilada
pars retornar el hierro a la Ease acuosa y transfe-\par\pard\li2121\sb158\sl-207
\slmult0\fi28\tx8769\tx9273\tx9916 \up0 \expndtw0\charscalex170 rir la capa acuo
sa inferior a un matraz aforado de\tab \up0 \expndtw0\charscalex128 100\tab \up0
\expndtw0\charscalex170 ml.\tab \up0 \expndtw0\charscalex170 Se re-\par\pard\li
2121\sb153\sl-207\slmult0\fi23\tx8102\tx8495 \up0 \expndtw0\charscalex170 pite l
a extracci6n con una segunda porcion de\tab \up0 \expndtw0\charscalex127 25\tab
\up0 \expndtw0\charscalex170 ml de agua destila\par\pard\li2121\sb158\sl-207\slm

ult0\fi23 \up0 \expndtw0\charscalex170 do, agregando este el primer extracto acu

oso. Se descarta la caps\par\pard\li2121\sb134\sl-230\slmult0\fi19 \up0 \expndtw
0\charscalex170 \ul0\nosupersub\cf9\f10\fs20 et6rea.\par\pard\li2121\sb0\sl-207\
slmult0\par\pard\li2121\sb57\sl-207\slmult0\fi14\tx3047\tx8889\tx9139 \up0 \expn
dtw0\charscalex170 \ul0\nosupersub\cf8\f9\fs18 7.6.5\tab \dn2 \expndtw0\charscal
ex167 A los extractos acuosos combinados as agrega\tab \up0 \expndtw0\charscalex
170 1\tab \up0 \expndtw0\charscalex170 ml de solu-\par\pard\li2121\sb157\sl-207\
slmult0\fi14\tx5135\tx5510\tx9792\tx10171 \up0 \expndtw0\charscalex170 cion de h
idroxilamina,\tab \up0 \expndtw0\charscalex121 10\tab \dn2 \expndtw0\charscalex1
70 ml de solucion de fenantrolina y\tab \up0 \expndtw0\charscalex124 10\tab \up0
\expndtw0\charscalex170 ml de\par\pard\li2121\sb153\sl-207\slmult0\fi9\tx7713\t
x8217 \up0 \expndtw0\charscalex170 soluci6n de acetato de sodio. Se diluye a\tab
\up0 \expndtw0\charscalex128 100\tab \up0 \expndtw0\charscalex170 ml con agua d
estila-\par\pard\li2121\sb153\sl-207\slmult0\fi9\tx8615\tx9000 \up0 \expndtw0\ch
arscalex170 do, se mezcla vigorosamente y se deja reposar por\tab \up0 \expndtw0
\charscalex124 10\tab \up0 \expndtw0\charscalex170 min. Se mide\par\pard\li2121\
sb149\sl-207\slmult0\fi4\tx4348\tx4867\tx10041\tx10295 \up0 \expndtw0\charscalex
170 la absorbancia a\tab \up0 \expndtw0\charscalex132 510\tab \dn2 \expndtw0\cha
rscalex170 nm utilizando una celda de absorcion de\tab \up0 \expndtw-2\charscale
x100 5\tab \up0 \expndtw0\charscalex170 cm\par\pard\li2121\sb138\sl-230\slmult0\
fi0\tx6931\tx9527\tx9772 \up0 \expndtw0\charscalex153 \ul0\nosupersub\cf9\f10\fs
20 pare cantidades de hierro menores de\tab \up0 \expndtw0\charscalex170 10O/ o
celdas de\tab \up0 \expndtw0\charscalex170 1\tab \up0 \expndtw0\charscalex170 cm
para\par\pard\li2121\sb149\sl-207\slmult0\fi0\tx3964\tx4463\tx4732\tx6009 \up0
\expndtw0\charscalex170 \ul0\nosupersub\cf8\f9\fs18 cantidades de\tab \up0 \expn
dtw0\charscalex128 100\tab \up0 \expndtw-2\charscalex100 a\tab \up0 \expndtw0\ch
arscalex170 500\ul0\nosupersub\cf17\f18\fs18 /t\tab \dn2 \expndtw0\charscalex17
0 \ul0\nosupersub\cf8\f9\fs18 Como referencie se puede usar agua des\par\pard\ql
\li2126\sb119\sl-230\slmult0 \up0 \expndtw0\charscalex154 \ul0\nosupersub\cf9\f
10\fs20 tilada o un blanco de muestra preparado siguiendo todos los pasos \par\p
ard\ql \li2121\sb149\sl-207\slmult0 \up0 \expndtw0\charscalex176 \ul0\nosupersub
\cf8\f9\fs18 del procedimiento analitico con las cantidades especificadas de aci
\par\pard\qj \li2116\ri1108\sb31\sl-380\slmult0 \up0 \expndtw0\charscalex150 \u
l0\nosupersub\cf9\f10\fs20 dos. Si se use agua.deatilada como referencia., se co
rrige la absorbancia \line \up0 \expndtw0\charscalex139 de is muestra po\u8226?i
r susteaccion de la absorbancia de un blanco de muestra. \par\pard\li2078\sb0\sl
-207\slmult0\par\pard\li2078\sb7\sl-207\slmult0\fi33\tx3014 \up0 \expndtw0\chars
calex168 \ul0\nosupersub\cf8\f9\fs18 7.6.6\tab \dn2 \expndtw0\charscalex168 Se d
eterminan los microgramos de hierro en la muestra usada\par\pard\li2078\sb157\sl
-207\slmult0\fi19\tx5620 \up0 \expndtw0\charscalex168 a partir de la absorbancia
\tab \dn2 \expndtw0\charscalex168 (corregida, si es necesario) y de la cur\par\p
ard\li2078\sb158\sl-207\slmult0\fi19 \up0 \expndtw0\charscalex168 va de calibrac
ion preparada como se indico anteriormente.\par\pard\li2078\sb0\sl-207\slmult0\p
ar\pard\li2078\sb0\sl-207\slmult0\par\pard\li2078\sb94\sl-207\slmult0\fi2880\tx5
342 \up0 \expndtw0\charscalex168 8\tab \dn2 \expndtw0\charscalex168 \ul0\nosuper
sub\cf7\f8\fs18\ul EXPRESION DE RESULTADOS\par\pard\li2078\sb0\sl-207\slmult0\pa
r\pard\li2078\sb0\sl-207\slmult0\par\pard\li2078\sb99\sl-207\slmult0\fi9\tx2736
\up0 \expndtw0\charscalex168 \ul0\nosupersub\cf8\f9\fs18 8.1\tab \dn2 \expndtw0\
charscalex168 El contenido de hierro an la muestra se expresa en miligramos\par\
pard\li2078\sb163\sl-207\slmult0\fi4 \up0 \expndtw0\charscalex168 por litro y se
calcula mediante la siguiente expresi6n:\par\pard\li2078\sb0\sl-207\slmult0\par
\pard\li2078\sb56\sl-207\slmult0\fi0\tx2990\tx9873 \up0 \expndtw0\charscalex168
8.1.1\tab \dn2 \expndtw0\charscalex168 Cuando la muestra he sido tratada segun s
e indica an\tab \up0 \expndtw0\charscalex168 7.2,\par\pard\li2078\sb134\sl-230\s
lmult0\fi0\tx2760\tx3412\tx3931 \up0 \expndtw0\charscalex168 \ul0\nosupersub\cf9
\f10\fs20 7.3,\tab \up0 \expndtw0\charscalex168 7.4,\tab \up0 \expndtw0\charscal
ex142 7.5\tab \up0 \expndtw0\charscalex168 6 7.6.3.\par\pard\li2078\sb0\sl-230\s
lmult0\par\pard\li2078\sb0\sl-230\slmult0\par\pard\li2078\sb40\sl-230\slmult0\fi
2337\tx5563\tx6302 \dn4 \expndtw0\charscalex130 mg Fe/1\tab \dn4 \expndtw0\chars
calex120 =\tab \up4 \expndtw0\charscalex168 \ul0\nosupersub\cf10\f11\fs20\ul ,U

g Fe\par\pard\ql \li6091\sb144\sl-207\slmult0 \up0 \expndtw0\charscalex168 \ul0\

nosupersub\cf8\f9\fs18 ml muestra \par\pard\sect\sectd\fs24\paperw12240\paperh15
840{\bkmkstart Pg17}{\bkmkend Pg17}\par\pard\ql \li10459\sb0\sl-230\slmult0 \par
\pard\ql\li10459\sb0\sl-230\slmult0 \par\pard\ql\li10459\sb0\sl-230\slmult0 \par
\pard\ql\li10459\sb0\sl-230\slmult0 \par\pard\ql\li10459\sb0\sl-230\slmult0 \par
\pard\ql\li10459\sb0\sl-230\slmult0 \par\pard\ql\li10459\sb0\sl-230\slmult0 \par
\pard\ql\li10459\sb0\sl-230\slmult0 \par\pard\ql\li10459\sb50\sl-230\slmult0 \up
0 \expndtw0\charscalex141 \ul0\nosupersub\cf9\f10\fs20 /14 \par\pard\li2294\sb0\
sl-207\slmult0\par\pard\li2294\sb0\sl-207\slmult0\par\pard\li2294\sb0\sl-207\slm
ult0\par\pard\li2294\sb146\sl-207\slmult0\fi0\tx3196\tx9940 \up0 \expndtw0\chars
calex165 \ul0\nosupersub\cf8\f9\fs18 8.1.2\tab \dn2 \expndtw0\charscalex165 Cuan
do la muestra ha sido tratada como se indica an\tab \up0 \expndtw0\charscalex165
7.6.2\par\pard\li2294\sb0\sl-230\slmult0\par\pard\li2294\sb158\sl-230\slmult0\f
i3086\tx7195\tx8510 \dn3 \expndtw0\charscalex165 \ul0\nosupersub\cf9\f10\fs20 /u
\ul0\nosupersub\cf10\f11\fs20\ul ,\ul0\nosupersub\cf9\f10\fs20 g Fe\tab \dn2 \ex
pndtw0\charscalex120 \ul0\nosupersub\cf8\f9\fs18 X\tab \up0 \expndtw0\charscalex
165 \ul0\nosupersub\cf9\f10\fs20 100\par\pard\li2294\sb0\sl-162\slmult0\fi1291\t
x4747 \up0 \expndtw0\charscalex165 \ul0\nosupersub\cf8\f9\fs18 mg Fe/l\tab \up0
\expndtw0\charscalex120 =\par\pard\li2294\sb4\sl-182\slmult0\fi2975\tx7718 \up0
\expndtw0\charscalex165 ml muestra\tab \up0 \expndtw0\charscalex165 ml de la por
c16n\par\pard\li2256\sb0\sl-207\slmult0\par\pard\li2256\sb0\sl-207\slmult0\par\p
ard\li2256\sb0\sl-207\slmult0\par\pard\li2256\sb17\sl-207\slmult0\fi23\tx2923 \u
p0 \expndtw0\charscalex166 8.2\tab \up0 \expndtw0\charscalex166 Deben referirse
detalles de la recoleccion de muestras, almace-\par\pard\li2256\sb158\sl-207\slm
ult0\fi23 \up0 \expndtw0\charscalex166 namiento y pretratamiento si ello as pert
inente Para la interpreta-\par\pard\li2256\sb153\sl-207\slmult0\fi19 \up0 \expnd
tw0\charscalex166 cion de resultados.\par\pard\li2256\sb0\sl-207\slmult0\par\par
d\li2256\sb0\sl-207\slmult0\par\pard\li2256\sb104\sl-207\slmult0\fi3648\tx6307 \
up0 \expndtw0\charscalex166 9\tab \dn2 \expndtw0\charscalex166 \ul0\nosupersub\c
f7\f8\fs18\ul INFORIYIE\par\pard\li2256\sb0\sl-207\slmult0\par\pard\li2256\sb181
\sl-207\slmult0\fi4 \up0 \expndtw0\charscalex166 \ul0\nosupersub\cf8\f9\fs18 El
informs del ensayo debera' indicar como minimo la siguiente infor\par\pard\li225
6\sb148\sl-207\slmult0\fi4 \up0 \expndtw0\charscalex166 macion:\par\pard\li2256\
sb0\sl-207\slmult0\par\pard\li2256\sb62\sl-207\slmult0\fi14\tx2913\tx9590 \up0 \
expndtw0\charscalex166 1.-\tab \up0 \expndtw0\charscalex152 Ensayo realizado seg
un la Norma Venezolana COVENIN\tab \up0 \expndtw0\charscalex166 2120.\par\pard\l
i2256\sb129\sl-230\slmult0\fi4\tx2908\tx6537 \up0 \expndtw0\charscalex166 \ul0\n
osupersub\cf9\f10\fs20 2.-\tab \dn2 \expndtw0\charscalex166 Fecha an is cual as
realiz6\tab \dn2 \expndtw0\charscalex166 el ensayo.\par\pard\li2256\sb135\sl-230
\slmult0\fi4\tx2923 \up0 \expndtw0\charscalex166 3.-\tab \up0 \expndtw0\charscal
ex166 Identificacion de la muestra.\par\pard\li2256\sb149\sl-207\slmult0\fi0\tx2
899 \up0 \expndtw0\charscalex166 \ul0\nosupersub\cf8\f9\fs18 4.-\tab \up0 \expnd
tw0\charscalex166 Resultedos del ensayo.\par\pard\li2256\sb148\sl-207\slmult0\fi
0\tx2908 \up0 \expndtw0\charscalex166 5.-\tab \dn2 \expndtw0\charscalex166 Obser
vaciones.\par\pard\li2231\sb0\sl-207\slmult0\par\pard\li2231\sb0\sl-207\slmult0\
par\pard\li2231\sb0\sl-207\slmult0\par\pard\li2231\sb0\sl-207\slmult0\par\pard\l
i2231\sb170\sl-207\slmult0\fi3657 \up0 \expndtw0\charscalex149 \ul0\nosupersub\c
f7\f8\fs18\ul BIBLIOGRAFIA\par\pard\li2231\sb0\sl-230\slmult0\par\pard\li2231\sb
0\sl-230\slmult0\par\pard\li2231\sb34\sl-230\slmult0\fi4\tx4329 \up0 \expndtw-7\
charscalex100 \ul0\nosupersub\cf9\f10\fs20 APHA-AWWA-WPCF\tab \up0 \expndtw0\cha
rscalex149 1975. Standard'Methods for the Examination of Water\par\pard\li2231\s
b144\sl-207\slmult0\fi0 \up0 \expndtw0\charscalex149 \ul0\nosupersub\cf8\f9\fs18
and Wastewater. American Public Health Association-American Water\par\pard\li22
31\sb148\sl-207\slmult0\fi4\tx9379 \up0 \expndtw0\charscalex149 Works Associatio
n-Water Pollution Control Federation.\tab \up0 \expndtw0\charscalex149 14th Edit
ion.\par\pard\li2231\sb148\sl-207\slmult0\fi0\tx5222 \up0 \expndtw0\charscalex14
9 Washington D.C.Seccion\tab \up0 \expndtw0\charscalex149 310A.\par\pard\sect\se
ctd\fs24\paperw12240\paperh15840{\bkmkstart Pg18}{\bkmkend Pg18}\par\pard\li1132
\sb0\sl-299\slmult0\par\pard\li1132\sb0\sl-299\slmult0\par\pard\li1132\sb269\sl299\slmult0\fi0\tx8793 \up2 \expndtw0\charscalex109 \ul0\nosupersub\cf16\f17\fs2

6 COVENIN\tab \dn5 \expndtw0\charscalex109 CATEGORIA\par\pard\li1132\sb23\sl-299

\slmult0\fi191\tx9556 \up2 \expndtw0\charscalex109 2120-84\tab \dn4 \expndtw0\ch
arscalex109 C\par\pard\ql \li1574\sb0\sl-380\slmult0 \par\pard\ql\li1574\sb0\sl380\slmult0 \par\pard\ql\li1574\sb0\sl-380\slmult0 \par\pard\ql\li1574\sb0\sl-38
0\slmult0 \par\pard\ql\li1574\sb0\sl-380\slmult0 \par\pard\ql\li1574\sb0\sl-380\
slmult0 \par\pard\ql\li1574\sb0\sl-380\slmult0 \par\pard\ql\li1574\sb0\sl-380\sl
mult0 \par\pard\ql\li1574\sb0\sl-380\slmult0 \par\pard\ql\li1574\sb0\sl-380\slmu
lt0 \par\pard\ql\li1574\ri1961\sb239\sl-380\slmult0\tx3720 \up0 \expndtw0\charsc
alex108 \ul0\nosupersub\cf6\f7\fs30 COMISION VENEZOLANA DE NORMAS INDUSTRIALES \
line\tab \up0 \expndtw0\charscalex109 MINISTERIO DE FOMENTO \par\pard\ql \li1924
\sb29\sl-345\slmult0 \up0 \expndtw0\charscalex108 Av. Andres Bello Edif. Torre F
ondo Coman Pisos 11 y 12 \par\pard\ql \li4156\sb51\sl-253\slmult0\tx5875 \up0 \e
xpndtw0\charscalex105 \ul0\nosupersub\cf15\f16\fs22 Telf. 575. 41. 11 \tab \up0
\expndtw0\charscalex107 Fax: 574. 13. 12 \par\pard\ql \li5236\sb27\sl-253\slmult
0 \up0 \expndtw0\charscalex107 CARACAS\par\pard\sect\sectd\sbknone\cols3\colno1\
colw4390\colsr160\colno2\colw3805\colsr160\colno3\colw3595\colsr160\ql \li955\sb
0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\
sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl
-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-2
53\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253
\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\s
lmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slm
ult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slmul
t0 \par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0
\par\pard\ql \li955\sb0\sl-253\slmult0 \par\pard\ql \li955\sb0\sl-253\slmult0 \
par\pard\ql \li955\sb139\sl-253\slmult0 \up0 \expndtw0\charscalex115 CDU: 628.1:
543.3:\par\pard\ql \li955\sb25\sl-253\slmult0 \up0 \expndtw0\charscalex104 546.
72\par\pard\column \ql \li4550\sb0\sl-644\slmult0 \par\pard\ql \li4550\sb0\sl-64
4\slmult0 \par\pard\ql \li4550\sb0\sl-644\slmult0 \par\pard\ql \li4550\sb0\sl-64
4\slmult0 \par\pard\ql \li4550\sb0\sl-644\slmult0 \par\pard\ql \li4550\sb0\sl-64
4\slmult0 \par\pard\ql \li20\sb355\sl-644\slmult0 \up0 \expndtw0\charscalex105 \
ul0\nosupersub\cf19\f20\fs56 publication de:\par\pard\ql \li4560\sb0\sl-207\slmu
lt0 \par\pard\ql \li4560\sb0\sl-207\slmult0 \par\pard\ql \li30\sb105\sl-207\slmu
lt0 \up0 \expndtw0\charscalex106 \ul0\nosupersub\cf8\f9\fs18 RESERVADOS TODOS LO
S DERECHOS\par\pard\column \ql \li20\sb2349\sl-2507\slmult0 \up0 \expndtw0\chars
calex60 \ul0\nosupersub\cf21\f22\fs218 F1\par\pard\ql \li35\sb0\sl-162\slmult0 \
up0 \expndtw0\charscalex106 \ul0\nosupersub\cf8\f9\fs18 FONDONORMA \par\pard\sec
t\sectd\sbknone \ql \li4560\sb24\sl-207\slmult0 \up0 \expndtw0\charscalex107 Pro
hibida la reproduccion total o parcial, por cualquier medio. \par\pard\sect\sect
d\fs24}