BLANKO METANOL

0.800 hamida-nurul 2011 #5 blanko metanol UV_VIS_1

mAU WVL:278 nm
15
1617--7.267
-7.313
7.373

0.700

0.600

0.500

2 - 1.733
0.400

18 - 9.300
0.300

0.200
1920- 10.887
- 11.013
3 - 3.313
456- -3.620 2122- 11.833
- 11.947
2324
0.100
-73.680
3.713
- 3.853 14 - 5.487 25-26-12.227
-12.280
12.313
- 12.407
89--4.347 12 13- 5.227
- 5.353 27 - 13.08728 - 13.733
4.38010 -114.887
- 5.080 29 - 13.780
30 -3114.160
- 14.353
323334
- -14.693
14.747
35- 14.860
- 14.973
1 - 0.240
0.000

-0.100 min
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0
Kaffein 10 ppm

Methanol 20 air 80

Flow 1 ml/min

Panjang gel 278nm

Run time 15 menit

10.0 hamida-nurul 2011 #1 std kafein 10ppm-1 UV_VIS_1

mAU WVL:278 nm

9.0 64 - 12.833

8.0

7.0

6.0

5.0

4.0

3.0

2.0

1.0 21 - 3.067 666768

65 -14.720
-14.760
14.813
--14.687

22 -23
3.227
- 3.420

20 - 2.807 2425- 3.507

- 26
3.607
- 3.80727 - 4.273
1 2- Peak
- 0.113 1-560.387
--0.027
3 4- 0.300 7-0.487
- 80.613
0.540
- 0.7471011- 1.140
9 - 0.967 - 1.207
1213- 1.527
-14
1.600 161.847
15- -1.787 18- 19
-172.020 - 2.407
2.193
- 2.267 282930--4.547
4.587
- 4.653
31 32
-33
4.960
--5.107
5.147 - 36
34 355.9736.17337 -38
- -6.113 39- 40
6.613 41
- 6.993
6.793 -427.120
- 6.880 - 7.287
43 44
- 7.553
- 7.68745 - 8.140 46 -4748- 8.960
8.780 - 9.060 50 - 9.707
49 - 9.387 51 - 10.027
5253- 10.327
-55
5410.427
- -10.560 59
5657--58
10.613 60
-61
-11.080
10.88011.120
--11.213
10.920
62 11.247
63 - 11.607
- 11.320
0.0

-1.0 min
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0
Kaffein 5 ppm

Methanol 20 air 80

Flow 1 ml/min

Panjang gel 278nm

Run time 15 menit

10.0 hamida-nurul 2011 #2 std kafein 5 ppm-1 UV_VIS_1

mAU WVL:278 nm

9.0
51 - 12.760

8.0

7.0

6.0

5.0

4.0

3.0

2.0

1.0

10 - 3.020 52
53- -14.693
14.747
0.0
11 -12
3.180
- 3.367
45-6-2.353
1 - 1.600 23- -2.133
2.187 -92.640
--2.480
72.400 - 2.753
82.520 13 - 3.760 14
15--4.307
4.347 16 17
- 4.920
- 5.053 1819- 5.633
212224
-23 -6.107
6.153
- -6.060 2526
-27
6.980
- -7.107
7.160 2829 3132
- 7.713
30 --8.073
- 7.820 8.100
33 3435- 8.600
- 8.227
- 8.340 - 8.667
36 -37
9.027 38 - 9.47339
- 9.220 40--41
9.940
9.967
42-43
10.133
- 10.213
- 10.300
44 - 10.440
4546
- 10.807
47 - 11.040
- 48
10.933
- 11.127
49
50- -11.500
11.553
- 20 -5.913
5.700 5.973
-1.0

-2.0 min
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0
Kaffein 10 ppm

Methanol 50 air 50

Flow 1 ml/min

Panjang gel 278nm

Run time 25 menit

35.0 hamida-nurul 2011 #6 std kafein 10ppm-1 UV_VIS_1

mAU WVL:278 nm

16 - 3.753
30.0

25.0

20.0

15.0

10.0

5.0

15 - 2.600
1 - 0.587
2345-6-70.913
-0.987
-1.020
1.067
81.133
1.167
910- 11
- 1.367 12 14---2.020
-131.813
1.753 2.080
-2.140
2.233 1718- 5.180
- 5.387
1920--6.127
6.187
21 - 22
6.860
23 --7.280
7.327
252627
24 -7.920
8.020
28- -7.820
7.853
8.053
29
3031
-32
-33
8.593
8.633
--34
8.860
3637
38
8.927
35
8.960 --9.353
-39
9.473
9.520
- -9.253
9.393
- -9.860
4041
42 -9.980
-10.100
10.153
43444546
- -10.607
-10.693
-10.787
10.900
47 - 11.273
48
4950
--12.073
51
-52
53 55
12.327
54---12.580
12.127 575859
-56
-12.660
12.700
12.773 --60
13.020 - 13.647
-13.387
13.440
13.500
-61
6213.773
63
64
--14.073
14.120
-65
-14.287
14.340
- 14.627
666768
69-70
-71
15.073
-15.133
72-15.253
7315.307
-74
75
-15.380
-76
-15.460
15.507
-15.573
-15.687
-15.747
7715.867
7879- 16.153
--16.320
16.387
808182-83
16.773
--16.927
16.993
- 17.147
84 - 17.607 85 - 19.600 868788
89--21.093
--21.167
21.233
21.280
90 - 22.020
919293--22.580
22.647
- 22.793
9495
96
97- -23.220
-23.313
23.347
23.380
98
99100
--101
24.040
24.093
- 24.180
- 24.447
0.0

-5.0 min
0.0 1.3 2.5 3.8 5.0 6.3 7.5 8.8 10.0 11.3 12.5 13.8 15.0 16.3 17.5 18.8 20.0 21.3 22.5 23.8 25.0