TP 2: Optimisation d'un com

PP pur

T E' Tan delta d E"

°C Pa sans Pa
22 1.82E+09 0.0448448 8.14E+07
22.25 1.81E+09 0.0453191 8.21E+07
23.55 1.78E+09 0.0472991 8.41E+07
24.4 1.76E+09 0.0483251 8.50E+07
26.35 1.71E+09 0.0508079 8.71E+07
27.4 1.69E+09 0.0526148 8.89E+07
29.75 1.63E+09 0.0568018 9.28E+07
30.95 1.61E+09 0.0587288 9.43E+07
33.35 1.55E+09 0.0631822 9.79E+07
34.6 1.52E+09 0.0656057 9.97E+07
37.15 1.46E+09 0.0712159 1.04E+08
38.45 1.42E+09 0.074243 1.06E+08
40.95 1.36E+09 0.0815926 1.11E+08
42.25 1.32E+09 0.0848545 1.12E+08
44.95 1.25E+09 0.0924355 1.15E+08
47.5 1.18E+09 0.100171 1.18E+08
48.8 1.14E+09 0.103545 1.18E+08
51.55 1.07E+09 0.111366 1.20E+08
52.9 1.04E+09 0.115055 1.20E+08
55.4 9.75E+08 0.122822 1.20E+08
56.65 9.43E+08 0.126128 1.19E+08
59.45 8.77E+08 0.133989 1.17E+08
60.7 8.47E+08 0.137019 1.16E+08
63.4 7.80E+08 0.144869 1.13E+08
64.7 7.59E+08 0.146567 1.11E+08
67.4 6.99E+08 0.154032 1.08E+08
68.75 6.71E+08 0.157998 1.06E+08
71.4 6.20E+08 0.163894 1.02E+08
72.7 5.98E+08 0.165527 9.90E+07
75.3 5.50E+08 0.173389 9.54E+07
78 5.02E+08 0.178203 8.95E+07
79.3 4.82E+08 0.180473 8.70E+07
81.85 4.40E+08 0.187638 8.26E+07
83.15 4.16E+08 0.191934 7.99E+07
85.95 3.61E+08 0.201223 7.26E+07
87.2 3.25E+08 0.207645 6.75E+07
89.9 1.95E+08 0.245752 4.79E+07
92.65 5.54E+07 0.304869 1.69E+07
93.85 3.92E+07 0.286517 1.12E+07
95 3.00E+07 0.292211 8.77E+06
 97.8 1.89E+07 0.335769 6.33E+06
99.15 1.57E+07 0.35338 5.56E+06
101.7 1.11E+07 0.41191 4.58E+06
104.3 8.31E+06 0.478096 3.98E+06
105.7 7.07E+06 0.521764 3.69E+06
108.2 5.13E+06 0.630899 3.24E+06
109.6 4.25E+06 0.706436 3.00E+06
112.1 2.96E+06 0.886338 2.63E+06
113.35 1.85E+06 1.3063 2.41E+06
116.15 1.30E+06 1.67891 2.17E+06
119.25 1714.98 1036.58 1.78E+06
120.2 -410056 6000 1.69E+06
120.8 -747929 6000 1.60E+06
121.1 -884520 6000 1.56E+06
121.1 -884089 6000 1.55E+06
120.95 -808152 6000 1.57E+06
120.9 -810434 6000 1.56E+06
120.85 -782807 6000 1.57E+06
120.7 -737929 6000 1.57E+06
120.65 -715386 6000 1.57E+06
120.55 -672788 6000 1.58E+06
120.6 -658289 6000 1.61E+06
120.5 -627925 6000 1.60E+06
120.45 -668331 6000 1.58E+06
120.35 -582170 6000 1.57E+06
120.5 -569405 6000 1.58E+06
120.35 -550998 6000 1.59E+06
120.35 -504749 6000 1.60E+06
120.3 -519461 6000 1.60E+06
120.25 -486615 6000 1.61E+06
120.2 -458054 6000 1.60E+06
120.25 -433742 6000 1.59E+06
120.25 -444046 6000 1.60E+06
120.25 -442110 6000 1.58E+06
120.2 -426409 6000 1.61E+06
120.25 -422615 6000 1.60E+06
120.15 -401768 6000 1.60E+06
120.05 -384123 6000 1.60E+06
120 -327942 6000 1.60E+06
120.15 -404548 6000 1.60E+06
120.05 -378098 6000 1.58E+06
120.15 -338581 6000 1.60E+06
120.1 -342939 6000 1.60E+06
120.05 -325463 6000 1.59E+06
120.05 -322255 6000 1.58E+06
120.15 -330310 6000 1.57E+06
120.1 -320019 6000 1.59E+06
120.15 -309005 6000 1.58E+06
120.05 -273064 6000 1.59E+06
120.05 -255303 6000 1.59E+06
120.1 -269312 6000 1.59E+06
120.05 -238822 6000 1.57E+06
120 -257347 6000 1.59E+06
120 -224878 6000 1.59E+06
120.15 -203177 6000 1.57E+06
120.1 -210683 6000 1.58E+06
120 -200608 6000 1.57E+06
120.05 -212083 6000 1.57E+06
120 -195760 6000 1.58E+06
120 -200742 6000 1.57E+06
119.95 -198130 6000 1.57E+06
120.05 -203764 6000 1.58E+06
120.05 -200735 6000 1.57E+06
120.1 -233709 6000 1.56E+06
120 -210161 6000 1.56E+06
120 -186893 6000 1.58E+06
120.05 -216549 6000 1.57E+06
120.05 -222177 6000 1.58E+06
120 -236371 6000 1.56E+06
120 -220739 6000 1.56E+06
120.05 -256440 6000 1.56E+06
119.9 -233844 6000 1.57E+06
120 -249677 6000 1.58E+06
119.95 -247169 6000 1.57E+06
120 -244000 6000 1.57E+06
120 -243564 6000 1.56E+06
120 -257724 6000 1.56E+06
120.05 -257662 6000 1.55E+06
Storage modulus variation with tempera
T(°C) 22 22.25
E'1 (Pa) 1.82E+09 1.81E+09
E'2 (Pa)
E'3 (Pa)
E'4 (Pa)

loss modulus variation with temperature

T(°C) 22 22.25
E''1(Pa) 8.14E+07 8.21E+07
E''2(Pa)
E''3(Pa)
E''4(Pa)

Damping factor (tan delta)

T(°C) 22 22.25
tan(delta)1 0.0448448 0.0453191
tan(delta)2
tan(delta)3
tan(delta)4
 cole-cole plot
E' (Pa) 1.82E+09 1.81E+09
E''1(Pa) 8.14E+07 8.21E+07
E''2(Pa)
E''3(Pa)
E''4(Pa)

1.40E+08

1.20E+08

Loss Modulus (MPa) 1.00E+08

8.00E+07

6.00E+07

4.00E+07

2.00E+07

0.00E+00
-5.00E+08 0.00E+00 5

Pourcentage des éléments chimiques

100%WF 5%WF 10%WF
C 46.83 53.69 63.35
O 51.86 45.90 36.28
Trace des
métaux (Al, Si, 1.3 0.41 0.37
S, K, Ca, Cu)

Travail demandé
1) Choix des facteurs influents
2) Donner le modèle mathématique d'un composite de farine de bo
3) Donner tous les interactions possibles?
4) Suivant les échantillons, choisir d'autres réponses concernant l'as
un composite
pp+5% farine de bois

T E' Tan delta d E"

°C Pa sans Pa
21.15 7.70E+08 0.0453129 3.49E+07
21.3 7.71E+08 0.045304 3.49E+07
22.55 7.57E+08 0.0472602 3.58E+07
23.4 7.48E+08 0.0482488 3.61E+07
25.35 7.28E+08 0.0511848 3.73E+07
26.45 7.15E+08 0.0531604 3.80E+07
28.7 6.89E+08 0.0572631 3.95E+07
29.9 6.75E+08 0.0598293 4.04E+07
32.35 6.43E+08 0.0646907 4.16E+07
33.6 6.27E+08 0.0676904 4.25E+07
36.1 5.93E+08 0.0737436 4.37E+07
37.4 5.75E+08 0.0768373 4.42E+07
40.05 5.38E+08 0.0836402 4.50E+07
41.35 5.21E+08 0.0878234 4.57E+07
43.9 4.83E+08 0.0954331 4.61E+07
45.3 4.66E+08 0.098437 4.58E+07
47.85 4.29E+08 0.106225 4.56E+07
49.25 4.13E+08 0.109776 4.54E+07
51.85 3.80E+08 0.118053 4.48E+07
53.2 3.62E+08 0.121518 4.40E+07
55.8 3.28E+08 0.128914 4.23E+07
57.15 3.11E+08 0.132925 4.13E+07
59.75 2.79E+08 0.140517 3.92E+07
61.15 2.63E+08 0.144172 3.79E+07
63.75 2.30E+08 0.152203 3.50E+07
65.1 2.14E+08 0.15674 3.35E+07
67.75 1.79E+08 0.16488 2.96E+07
70.4 1.49E+08 0.172756 2.58E+07
71.7 1.36E+08 0.177199 2.41E+07
74.2 1.08E+08 0.186311 2.01E+07
75.6 9.45E+07 0.191723 1.81E+07
78.25 7.33E+07 0.200212 1.47E+07
79.6 6.51E+07 0.203657 1.33E+07
82.15 4.96E+07 0.215258 1.07E+07
83.5 4.30E+07 0.220748 9.49E+06
86.1 3.42E+07 0.228424 7.81E+06
87.4 3.01E+07 0.236857 7.12E+06
90.1 2.34E+07 0.247944 5.81E+06
91.4 2.08E+07 0.254073 5.29E+06
94.1 1.68E+07 0.270424 4.53E+06
 95.45 1.51E+07 0.280534 4.23E+06
97.95 1.19E+07 0.305308 3.62E+06
99.35 1.06E+07 0.316923 3.36E+06
101.95 8.59E+06 0.345943 2.97E+06
103.25 7.87E+06 0.360384 2.84E+06
105.9 6.42E+06 0.393858 2.53E+06
107.15 5.72E+06 0.412474 2.36E+06
109.9 4.43E+06 0.467627 2.07E+06
111.15 3.91E+06 0.499218 1.95E+06
113.65 2.88E+06 0.582669 1.68E+06
115 2.42E+06 0.640219 1.55E+06
118.9 1.37E+06 0.906745 1.24E+06
120.3 835485 1.27549 1.07E+06
120.75 649366 1.56074 1.01E+06
120.95 531695 1.83752 977001
121.1 523307 1.86233 974572
121.1 572464 1.71214 980138
121.05 641578 1.54729 992705
120.85 701372 1.42114 996746
120.6 790184 1.2828 1.01E+06
120.65 860352 1.19911 1.03E+06
120.8 964694 1.08094 1.04E+06
120.5 1.03E+06 1.0167 1.05E+06
120.45 1.11E+06 0.96411 1.07E+06
120.6 1.15E+06 0.937916 1.08E+06
120.4 1.19E+06 0.900686 1.07E+06
120.45 1.27E+06 0.858871 1.09E+06
120.45 1.32E+06 0.833192 1.10E+06
120.35 1.35E+06 0.812552 1.10E+06
120.35 1.40E+06 0.791552 1.11E+06
120.2 1.46E+06 0.763346 1.11E+06
120.25 1.48E+06 0.760239 1.12E+06
120.25 1.51E+06 0.742577 1.12E+06
120.15 1.56E+06 0.72535 1.13E+06
120.25 1.58E+06 0.709498 1.12E+06
120.25 1.60E+06 0.70764 1.13E+06
120.2 1.60E+06 0.70635 1.13E+06
120.2 1.61E+06 0.699032 1.13E+06
120.2 1.63E+06 0.692105 1.13E+06
120.15 1.67E+06 0.67772 1.13E+06
120 1.71E+06 0.657729 1.12E+06
120.1 1.73E+06 0.656917 1.14E+06
120 1.75E+06 0.649019 1.13E+06
120.1 1.74E+06 0.650732 1.13E+06
120.15 1.76E+06 0.646434 1.13E+06
120.1 1.79E+06 0.631091 1.13E+06
120.1 1.81E+06 0.626583 1.13E+06
120 1.84E+06 0.624884 1.15E+06
120.1 1.87E+06 0.607544 1.14E+06
120.05 1.89E+06 0.607059 1.15E+06
120.15 1.90E+06 0.604223 1.15E+06
 120.1 1.91E+06 0.598417 1.15E+06
120.05 1.94E+06 0.591668 1.15E+06
120.1 1.93E+06 0.590345 1.14E+06
120.1 1.94E+06 0.588503 1.14E+06
120 1.96E+06 0.583398 1.14E+06
120.1 1.98E+06 0.578124 1.14E+06
120 1.99E+06 0.575133 1.14E+06
119.95 2.00E+06 0.565061 1.13E+06
120 1.99E+06 0.571209 1.14E+06
120.05 2.04E+06 0.558912 1.14E+06
120.05 2.06E+06 0.557614 1.15E+06
120.05 2.06E+06 0.553025 1.14E+06
120 2.04E+06 0.55721 1.13E+06
120 2.07E+06 0.552698 1.14E+06
119.95 2.10E+06 0.544909 1.15E+06
120 2.09E+06 0.545048 1.14E+06
120 2.09E+06 0.543867 1.13E+06
120.05 2.12E+06 0.536361 1.14E+06
120 2.13E+06 0.529331 1.13E+06
120.05 2.15E+06 0.527685 1.13E+06
120.05 2.15E+06 0.531159 1.14E+06
120.05 2.17E+06 0.524672 1.14E+06
119.95 2.19E+06 0.519814 1.14E+06
120 2.19E+06 0.520394 1.14E+06
120.05 2.19E+06 0.516084 1.13E+06
119.95 2.20E+06 0.512916 1.13E+06
120.05 2.22E+06 0.51103 1.14E+06
120 2.24E+06 0.509691 1.14E+06
119.95 2.27E+06 0.501677 1.14E+06
120.05 2.26E+06 0.50621 1.15E+06
119.95 2.27E+06 0.502435 1.14E+06
120.05 2.28E+06 0.501709 1.14E+06
120 2.30E+06 0.495622 1.14E+06
119.95 2.30E+06 0.492641 1.13E+06
120.05 2.33E+06 0.488299 1.14E+06
120.05 2.34E+06 0.488565 1.14E+06
120 2.36E+06 0.483763 1.14E+06
120.05 2.35E+06 0.481264 1.13E+06
119.95 2.36E+06 0.480486 1.13E+06
120.05 2.37E+06 0.477325 1.13E+06
120.05 2.39E+06 0.474271 1.13E+06
120 2.38E+06 0.478013 1.14E+06
119.95 2.41E+06 0.469942 1.13E+06
119.95 2.42E+06 0.470139 1.14E+06
119.95 2.43E+06 0.469192 1.14E+06
120 2.44E+06 0.465539 1.14E+06
120 2.45E+06 0.463565 1.14E+06
119.9 2.46E+06 0.462315 1.14E+06
119.95 2.46E+06 0.458464 1.13E+06
120 2.46E+06 0.457381 1.13E+06
119.95 2.50E+06 0.453475 1.13E+06
 120.1 2.50E+06 0.450078 1.12E+06
120 2.50E+06 0.452494 1.13E+06
119.95 2.52E+06 0.454254 1.14E+06

with temperature
23.55 24.4 26.35 27.4 29.75 30.95
1.78E+09 1.76E+09 1.71E+09 1.69E+09 1.63E+09 1.61E+09

temperature
23.55 24.4 26.35 27.4 29.75 30.95
8.41E+07 8.50E+07 8.71E+07 8.89E+07 9.28E+07 9.43E+07

23.55 24.4 26.35 27.4 29.75 30.95

0.0472991 0.0483251 0.0508079 0.0526148 0.0568018 0.0587288

Storage modulus variation with temperature the basic polypropylene PP a

10FW/PP and 20FW/PP

1,800,000,000

1,300,000,000
Storage modulus E' (MPa)

800,000,000

300,000,000

20 40 60 80
 800,000,000

Storage m
300,000,000

20 40 60 80
(200,000,000) Température (°C)

1.78E+09 1.76E+09 1.71E+09 1.69E+09 1.63E+09 1.61E+09

8.41E+07 8.50E+07 8.71E+07 8.89E+07 9.28E+07 9.43E+07

+08

+08

+08

+07
E''1(Pa)
+07 E''2(Pa)
E''3(Pa)
E''4(Pa)
+07

+07

+00
0.00E+00 5.00E+08 1.00E+09 1.50E+09 2.00E+09
Storage Modulus (MPa)

20%WF 100%PP
54.52 53.28
45.28 46.72
0.20 0
e farine de bois et polypropylène?

oncernant l'aspect?
 pp+10% farine de bois

T E' Tan delta E" T

°C Pa sans Pa °C
62.6 7.37E+07 0.182232 1.34E+07 21.95
66.75 6.54E+07 0.183032 1.20E+07 22.15
68.55 6.18E+07 0.1842 1.14E+07 23.5
69 6.10E+07 0.183257 1.12E+07 24.3
69.85 5.92E+07 0.184169 1.09E+07 26.2
70.6 5.74E+07 0.187546 1.08E+07 27.3
72.3 5.37E+07 0.190681 1.02E+07 29.6
74.35 4.92E+07 0.196743 9.68E+06 30.8
75.55 4.69E+07 0.200266 9.38E+06 33.2
77.75 4.29E+07 0.20594 8.84E+06 34.45
78.95 4.06E+07 0.209543 8.51E+06 37
81.5 3.61E+07 0.218201 7.88E+06 38.25
82.8 3.38E+07 0.222615 7.52E+06 40.95
85.35 3.00E+07 0.229503 6.89E+06 42.2
88 2.55E+07 0.241021 6.14E+06 44.8
89.3 2.35E+07 0.246813 5.81E+06 47.45
91.85 1.97E+07 0.260063 5.12E+06 48.75
93.25 1.75E+07 0.269193 4.72E+06 51.4
96 1.39E+07 0.294587 4.08E+06 52.75
98.55 1.06E+07 0.327991 3.48E+06 55.5
101.3 7.95E+06 0.366816 2.92E+06 56.7
102.65 6.89E+06 0.393041 2.71E+06 59.45
103.95 5.94E+06 0.425674 2.53E+06 60.75
106.7 4.29E+06 0.506724 2.17E+06 63.35
109.35 3.06E+06 0.61953 1.89E+06 64.75
110.65 2.59E+06 0.678311 1.76E+06 67.25
113.3 1.80E+06 0.844262 1.52E+06 68.7
114.55 1.46E+06 0.963214 1.41E+06 71.2
118.25 605548 1.88836 1.14E+06 73.8
119.65 283458 3.63151 1.03E+06 75.15
120.3 166915 5.97576 997444 77.7
120.55 125944 7.64757 963164 79.1
120.75 106124 8.88838 943267 81.75
120.6 102235 9.2784 948576 83.1
120.5 126233 7.48551 944917 85.65
120.55 149065 6.30256 939488 86.95
120.5 173452 5.50321 954545 89.45
120.55 206997 4.61133 954531 90.75
120.4 213385 4.50933 962221 93.75
120.35 208016 4.60425 957760 95.9
 120.4 201614 4.71717 951049 97.3
120.35 225367 4.22223 951549 100.1
120.2 240428 3.97645 956051 101.4
120.25 255007 3.76972 961305 103.75
120.25 244095 3.89021 949583 105.25
120.2 266937 3.58641 957344 107.85
120.15 240461 3.95715 951542 108.9
120.2 272076 3.47262 944817 112
120.2 295474 3.2756 967854 114.25
120.1 276492 3.46453 957916 115.55
120.1 291586 3.28386 957527 118.95
120.15 302080 3.16699 956683 120.3
120.05 284888 3.33793 950938 120.75
120.05 327385 2.93341 960355 121.15
120 333416 2.87858 959766 121
120.1 332529 2.8768 956619 120.9
120.1 328589 2.88458 947843 120.9
120 340807 2.82816 963856 121
120.1 334832 2.85344 955421 120.9
120.1 339966 2.80598 953937 120.75
120 359889 2.63837 949519 120.65
119.95 375818 2.55314 959517 120.5
120.05 380085 2.53221 962456 120.7
120 388115 2.48353 963896 120.3
120.1 397812 2.43457 968500 120.5
120 398837 2.40933 960929 120.5
120.1 383114 2.51185 962328 120.45
120.05 400268 2.39776 959749 120.5
120 408748 2.34793 959712 120.45
120 422283 2.28564 965189 120.4
119.95 431097 2.2435 967167 120.25
119.95 438685 2.19278 961940 120.3
120.05 437483 2.20654 965322 120.25
119.95 440578 2.18586 963041 120.1
120.1 436824 2.20025 961123 120.25
119.95 448112 2.14603 961662 120.3
120 471945 2.04057 963035 120.25
120 484095 2.00128 968809 120.15
119.9 489778 1.97375 966697 120.15
120.05 473437 2.04127 966413 120.2
120.1 478763 2.01333 963906 120.1
119.95 494149 1.95034 963758 120.1
120 484991 1.9991 969546 120.1
120 506182 1.91864 971181 120.2
120.05 503764 1.92571 970101 120.1
120.05 488250 1.99451 973821 120.1
120.05 504949 1.89449 956623 120.05
120.05 521222 1.87478 977179 120.05
119.95 529943 1.83632 973142 120
119.95 525544 1.86288 979025 120.05
120 525367 1.84154 967487 120.1
 120.1 523434 1.86242 974851 120
120 539327 1.79693 969132 120.1
120.05 537423 1.81091 973226 120.05
120 552686 1.78131 984506 120
119.95 560329 1.74414 977293 120.05
120.05 560169 1.73231 970388 120
119.95 558797 1.7321 967892 119.95
120 560341 1.74785 979394 120.05
120.05 553169 1.75992 973533 120.05
119.95 561141 1.72733 969278 120.05
120.1 551384 1.76955 975702 120
120.05 573681 1.70169 976225 120
120 582854 1.6757 976688 119.9
119.9 610436 1.61151 983721 120.05
119.95 577933 1.6908 977169 120
119.95 587566 1.6652 978412 120.05
120 601867 1.62851 980144 119.9
119.95
119.95
 33.35 34.6 37.15 38.45 40.95 42.25
1.55E+09 1.52E+09 1.46E+09 1.42E+09 1.36E+09 1.32E+09

33.35 34.6 37.15 38.45 40.95 42.25

9.79E+07 9.97E+07 1.04E+08 1.06E+08 1.11E+08 1.12E+08

33.35 34.6 37.15 38.45 40.95 42.25

0.0631822 0.0656057 0.0712159 0.074243 0.0815926 0.0848545

he basic polypropylene PP as well as the 5FW/PP ,

and 20FW/PP Loss Modulus variation with temperatu
as the 5%WF/PP, 10%WF
1.20E+08

E'1 (Pa) 1.00E+08

Loss Modulus (MPa)

E'2 (Pa)
8.00E+07
E'3 (Pa)
E'4 (Pa) 6.00E+07

4.00E+07

2.00E+07

0.00E+00
20 30 40 50

80 100 120
 0.00E+00
20 30 40 50

80 100 120

ure (°C)

1.55E+09 1.52E+09 1.46E+09 1.42E+09 1.36E+09 1.32E+09

9.79E+07 9.97E+07 1.04E+08 1.06E+08 1.11E+08 1.12E+08
pp+20% farine de bois

E' Tan delta d E"

Pa sans Pa
1.98E+08 0.0555835 1.10E+07
1.97E+08 0.0561934 1.11E+07
1.92E+08 0.0585354 1.13E+07
1.90E+08 0.0598728 1.14E+07
1.84E+08 0.0627869 1.15E+07
1.80E+08 0.0646087 1.16E+07
1.72E+08 0.0696074 1.20E+07
1.68E+08 0.0717613 1.21E+07
1.59E+08 0.0778073 1.23E+07
1.54E+08 0.0808401 1.24E+07
1.44E+08 0.0872356 1.26E+07
1.38E+08 0.0913902 1.27E+07
1.28E+08 0.098459 1.26E+07
1.23E+08 0.102415 1.26E+07
1.14E+08 0.109047 1.24E+07
1.04E+08 0.117931 1.23E+07
9.88E+07 0.122118 1.21E+07
9.00E+07 0.129819 1.17E+07
8.54E+07 0.134462 1.15E+07
7.71E+07 0.142942 1.10E+07
7.39E+07 0.144932 1.07E+07
6.51E+07 0.155709 1.01E+07
6.18E+07 0.157151 9.72E+06
5.42E+07 0.167499 9.08E+06
5.10E+07 0.170216 8.69E+06
4.55E+07 0.178016 8.10E+06
4.24E+07 0.181131 7.69E+06
3.75E+07 0.187205 7.03E+06
3.22E+07 0.196633 6.34E+06
2.98E+07 0.20152 6.00E+06
2.55E+07 0.210239 5.36E+06
2.35E+07 0.215727 5.07E+06
1.99E+07 0.225836 4.49E+06
1.84E+07 0.230512 4.25E+06
1.57E+07 0.245758 3.85E+06
1.46E+07 0.248275 3.62E+06
1.22E+07 0.272026 3.31E+06
1.08E+07 0.285264 3.07E+06
8.72E+06 0.313798 2.74E+06
7.22E+06 0.343927 2.48E+06
6.36E+06 0.365419 2.32E+06
5.10E+06 0.406055 2.07E+06
4.62E+06 0.434278 2.01E+06
3.53E+06 0.513077 1.81E+06
3.07E+06 0.552853 1.70E+06
2.46E+06 0.62565 1.54E+06
2.12E+06 0.693305 1.47E+06
1.52E+06 0.855569 1.30E+06
1.04E+06 1.12825 1.18E+06
785170 1.40852 1.11E+06
166769 5.50065 917338
-153933 6000 828545
-282884 6000 769132
-317081 6000 749092
-285210 6000 756283
-266942 6000 754839
-241931 6000 757228
-201231 6000 766530
-160478 6000 765397
-94485.2 6000 784557
-33958.4 6000 801402
49180.2 16.6216 817454
74959.6 10.9744 822639
159117 5.25392 835991
208290 4.11252 856597
246761 3.4517 851745
287162 3.01908 866964
339769 2.59301 881025
369931 2.4041 889350
407508 2.19803 895716
421560 2.11832 892997
429409 2.09856 901142
474316 1.92796 914460
494979 1.81899 900363
495002 1.84403 912797
490714 1.86746 916387
525238 1.75782 923274
519247 1.76821 918134
503894 1.81057 912338
533386 1.72772 921541
506229 1.8286 925689
522828 1.76036 920367
521643 1.77707 926996
529726 1.74342 923533
552280 1.67848 926994
547630 1.67702 918386
530974 1.72895 918029
546973 1.6692 913005
564763 1.63271 922095
563762 1.64795 929053
544836 1.69645 924290
577417 1.59399 920394
558628 1.65201 922857
556028 1.64684 915689
548425 1.66921 915434
562703 1.62332 913445
554262 1.65658 918176
584158 1.58279 924597
573856 1.60672 922025
585890 1.56484 916825
565224 1.63382 923477
557640 1.64614 917951
552974 1.66481 920597
560946 1.59789 896330
555181 1.63851 909668
563874 1.6308 919568
554571 1.65792 919435
565953 1.60559 908688
567089 1.59862 906559
568596 1.60789 914239
 44.95 47.5 48.8 51.55 52.9 55.4
1.25E+09 1.18E+09 1.14E+09 1.07E+09 1.04E+09 9.75E+08

44.95 47.5 48.8 51.55 52.9 55.4

1.15E+08 1.18E+08 1.18E+08 1.20E+08 1.20E+08 1.20E+08

44.95 47.5 48.8 51.55 52.9 55.4

0.0924355 0.100171 0.103545 0.111366 0.115055 0.122822

us variation with temperature for basic polypropylene as well

as the 5%WF/PP, 10%WF/PP and 20%WF/PP
20E+08

00E+08

00E+07
E''1(Pa)
00E+07 E''2(Pa)
E''3(Pa)
00E+07 E''4(Pa)

00E+07

00E+00
20 30 40 50 60 70 80 90 100 110 120
Température (°C)
00E+00
20 30 40 50 60 70 80 90 100 110 120
Température (°C)

1.25E+09 1.18E+09 1.14E+09 1.07E+09 1.04E+09 9.75E+08

1.15E+08 1.18E+08 1.18E+08 1.20E+08 1.20E+08 1.20E+08
 56.65 59.45 60.7 63.4 64.7 67.4 68.75 71.4
9.43E+08 8.77E+08 8.47E+08 7.80E+08 7.59E+08 6.99E+08 6.71E+08 6.20E+08

56.65 59.45 60.7 63.4 64.7 67.4 68.75 71.4

1.19E+08 1.17E+08 1.16E+08 1.13E+08 1.11E+08 1.08E+08 1.06E+08 1.02E+08

56.65 59.45 60.7 63.4 64.7 67.4 68.75 71.4

0.126128 0.133989 0.137019 0.144869 0.146567 0.154032 0.157998 0.163894
9.43E+08 8.77E+08 8.47E+08 7.80E+08 7.59E+08 6.99E+08 6.71E+08 6.20E+08
1.19E+08 1.17E+08 1.16E+08 1.13E+08 1.11E+08 1.08E+08 1.06E+08 1.02E+08
 72.7 75.3 78 79.3 81.85 83.15 85.95 87.2
5.98E+08 5.50E+08 5.02E+08 4.82E+08 4.40E+08 4.16E+08 3.61E+08 3.25E+08

72.7 75.3 78 79.3 81.85 83.15 85.95 87.2

9.90E+07 9.54E+07 8.95E+07 8.70E+07 8.26E+07 7.99E+07 7.26E+07 6.75E+07

72.7 75.3 78 79.3 81.85 83.15 85.95 87.2

0.165527 0.173389 0.178203 0.180473 0.187638 0.191934 0.201223 0.207645
5.98E+08 5.50E+08 5.02E+08 4.82E+08 4.40E+08 4.16E+08 3.61E+08 3.25E+08
9.90E+07 9.54E+07 8.95E+07 8.70E+07 8.26E+07 7.99E+07 7.26E+07 6.75E+07
 89.9 92.65 93.85 95 97.8 99.15 101.7 104.3
1.95E+08 5.54E+07 3.92E+07 3.00E+07 1.89E+07 1.57E+07 1.11E+07 8.31E+06

89.9 92.65 93.85 95 97.8 99.15 101.7 104.3

4.79E+07 1.69E+07 1.12E+07 8.77E+06 6.33E+06 5.56E+06 4.58E+06 3.98E+06

89.9 92.65 93.85 95 97.8 99.15 101.7 104.3

0.245752 0.304869 0.286517 0.292211 0.335769 0.35338 0.41191 0.478096
1.95E+08 5.54E+07 3.92E+07 3.00E+07 1.89E+07 1.57E+07 1.11E+07 8.31E+06
4.79E+07 1.69E+07 1.12E+07 8.77E+06 6.33E+06 5.56E+06 4.58E+06 3.98E+06
 105.7 108.2 109.6 112.1 113.35 116.15 119.25 120.2
7.07E+06 5.13E+06 4.25E+06 2.96E+06 1.85E+06 1.30E+06 1714.98 -410056

105.7 108.2 109.6 112.1 113.35 116.15 119.25 120.2

3.69E+06 3.24E+06 3.00E+06 2.63E+06 2.41E+06 2.17E+06 1.78E+06 1.69E+06

105.7 108.2 109.6 112.1 113.35 116.15

0.521764 0.630899 0.706436 0.886338 1.3063 1.67891
7.07E+06 5.13E+06 4.25E+06 2.96E+06 1.85E+06 1.30E+06 1714.98 -410056
3.69E+06 3.24E+06 3.00E+06 2.63E+06 2.41E+06 2.17E+06 1.78E+06 1.69E+06
 120.8 121.1 121.1 120.95 120.9 120.85 120.7 120.65
-747929 -884520 -884089 -808152 -810434 -782807 -737929 -715386

120.8 121.1 121.1 120.95 120.9 120.85 120.7 120.65

1.60E+06 1.56E+06 1.55E+06 1.57E+06 1.56E+06 1.57E+06 1.57E+06 1.57E+06
-747929 -884520 -884089 -808152 -810434 -782807 -737929 -715386
1.60E+06 1.56E+06 1.55E+06 1.57E+06 1.56E+06 1.57E+06 1.57E+06 1.57E+06
 120.55 120.6 120.5 120.45 120.35 120.5 120.35 120.35
-672788 -658289 -627925 -668331 -582170 -569405 -550998 -504749

120.55 120.6 120.5 120.45 120.35 120.5 120.35 120.35

1.58E+06 1.61E+06 1.60E+06 1.58E+06 1.57E+06 1.58E+06 1.59E+06 1.60E+06
-672788 -658289 -627925 -668331 -582170 -569405 -550998 -504749
1.58E+06 1.61E+06 1.60E+06 1.58E+06 1.57E+06 1.58E+06 1.59E+06 1.60E+06
 120.3 120.25 120.2 120.25 120.25 120.25 120.2 120.25
-519461 -486615 -458054 -433742 -444046 -442110 -426409 -422615

120.3 120.25 120.2 120.25 120.25 120.25 120.2 120.25

1.60E+06 1.61E+06 1.60E+06 1.59E+06 1.60E+06 1.58E+06 1.61E+06 1.60E+06
-519461 -486615 -458054 -433742 -444046 -442110 -426409 -422615
1.60E+06 1.61E+06 1.60E+06 1.59E+06 1.60E+06 1.58E+06 1.61E+06 1.60E+06
 120.15 120.05 120 120.15 120.05 120.15 120.1 120.05
-401768 -384123 -327942 -404548 -378098 -338581 -342939 -325463

120.15 120.05 120 120.15 120.05 120.15 120.1 120.05

1.60E+06 1.60E+06 1.60E+06 1.60E+06 1.58E+06 1.60E+06 1.60E+06 1.59E+06
-401768 -384123 -327942 -404548 -378098 -338581 -342939 -325463
1.60E+06 1.60E+06 1.60E+06 1.60E+06 1.58E+06 1.60E+06 1.60E+06 1.59E+06
 120.05 120.15 120.1 120.15 120.05 120.05 120.1 120.05
-322255 -330310 -320019 -309005 -273064 -255303 -269312 -238822

120.05 120.15 120.1 120.15 120.05 120.05 120.1 120.05

1.58E+06 1.57E+06 1.59E+06 1.58E+06 1.59E+06 1.59E+06 1.59E+06 1.57E+06
-322255 -330310 -320019 -309005 -273064 -255303 -269312 -238822
1.58E+06 1.57E+06 1.59E+06 1.58E+06 1.59E+06 1.59E+06 1.59E+06 1.57E+06
 120 120 120.15 120.1 120 120.05 120 120
-257347 -224878 -203177 -210683 -200608 -212083 -195760 -200742

120 120 120.15 120.1 120 120.05 120 120

1.59E+06 1.59E+06 1.57E+06 1.58E+06 1.57E+06 1.57E+06 1.58E+06 1.57E+06
-257347 -224878 -203177 -210683 -200608 -212083 -195760 -200742
1.59E+06 1.59E+06 1.57E+06 1.58E+06 1.57E+06 1.57E+06 1.58E+06 1.57E+06
 119.95 120.05 120.05 120.1 120 120 120.05 120.05
-198130 -203764 -200735 -233709 -210161 -186893 -216549 -222177

119.95 120.05 120.05 120.1 120 120 120.05 120.05

1.57E+06 1.58E+06 1.57E+06 1.56E+06 1.56E+06 1.58E+06 1.57E+06 1.58E+06
-198130 -203764 -200735 -233709 -210161 -186893 -216549 -222177
1.57E+06 1.58E+06 1.57E+06 1.56E+06 1.56E+06 1.58E+06 1.57E+06 1.58E+06
 120 120 120.05 119.9 120 119.95 120 120
-236371 -220739 -256440 -233844 -249677 -247169 -244000 -243564

120 120 120.05 119.9 120 119.95 120 120

1.56E+06 1.56E+06 1.56E+06 1.57E+06 1.58E+06 1.57E+06 1.57E+06 1.56E+06
-236371 -220739 -256440 -233844 -249677 -247169 -244000 -243564
1.56E+06 1.56E+06 1.56E+06 1.57E+06 1.58E+06 1.57E+06 1.57E+06 1.56E+06
 120 120.05 21.15 21.3 22.55 23.4 25.35 26.45
-257724 -257662
7.70E+08 7.71E+08 7.57E+08 7.48E+08 7.28E+08 7.15E+08

120 120.05 21.15 21.3 22.55 23.4 25.35 26.45

1.56E+06 1.55E+06
3.49E+07 3.49E+07 3.58E+07 3.61E+07 3.73E+07 3.80E+07

21.15 21.3 22.55 23.4 25.35 26.45

0.0453129 0.045304 0.0472602 0.0482488 0.0511848 0.0531604

-257724 -257662 7.70E+08 7.71E+08 7.57E+08 7.48E+08 7.28E+08 7.15E+08
1.56E+06 1.55E+06
3.49E+07 3.49E+07 3.58E+07 3.61E+07 3.73E+07 3.80E+07
 28.7 29.9 32.35 33.6 36.1 37.4 40.05 41.35

6.89E+08 6.75E+08 6.43E+08 6.27E+08 5.93E+08 5.75E+08 5.38E+08 5.21E+08

28.7 29.9 32.35 33.6 36.1 37.4 40.05 41.35

3.95E+07 4.04E+07 4.16E+07 4.25E+07 4.37E+07 4.42E+07 4.50E+07 4.57E+07

28.7 29.9 32.35 33.6 36.1 37.4 40.05 41.35

0.0572631 0.0598293 0.0646907 0.0676904 0.0737436 0.0768373 0.0836402 0.0878234

6.89E+08 6.75E+08 6.43E+08 6.27E+08 5.93E+08 5.75E+08 5.38E+08 5.21E+08

3.95E+07 4.04E+07 4.16E+07 4.25E+07 4.37E+07 4.42E+07 4.50E+07 4.57E+07

 43.9 45.3 47.85 49.25 51.85 53.2 55.8 57.15

4.83E+08 4.66E+08 4.29E+08 4.13E+08 3.80E+08 3.62E+08 3.28E+08 3.11E+08

43.9 45.3 47.85 49.25 51.85 53.2 55.8 57.15

4.61E+07 4.58E+07 4.56E+07 4.54E+07 4.48E+07 4.40E+07 4.23E+07 4.13E+07

43.9 45.3 47.85 49.25 51.85 53.2 55.8 57.15

0.0954331 0.098437 0.106225 0.109776 0.118053 0.121518 0.128914 0.132925

4.83E+08 4.66E+08 4.29E+08 4.13E+08 3.80E+08 3.62E+08 3.28E+08 3.11E+08

4.61E+07 4.58E+07 4.56E+07 4.54E+07 4.48E+07 4.40E+07 4.23E+07 4.13E+07

 59.75 61.15 63.75 65.1 67.75 70.4 71.7 74.2

2.79E+08 2.63E+08 2.30E+08 2.14E+08 1.79E+08 1.49E+08 1.36E+08 1.08E+08

59.75 61.15 63.75 65.1 67.75 70.4 71.7 74.2

3.92E+07 3.79E+07 3.50E+07 3.35E+07 2.96E+07 2.58E+07 2.41E+07 2.01E+07

59.75 61.15 63.75 65.1 67.75 70.4 71.7 74.2

0.140517 0.144172 0.152203 0.15674 0.16488 0.172756 0.177199 0.186311

2.79E+08 2.63E+08 2.30E+08 2.14E+08 1.79E+08 1.49E+08 1.36E+08 1.08E+08

3.92E+07 3.79E+07 3.50E+07 3.35E+07 2.96E+07 2.58E+07 2.41E+07 2.01E+07

 75.6 78.25 79.6 82.15 83.5 86.1 87.4 90.1

9.45E+07 7.33E+07 6.51E+07 4.96E+07 4.30E+07 3.42E+07 3.01E+07 2.34E+07

75.6 78.25 79.6 82.15 83.5 86.1 87.4 90.1

1.81E+07 1.47E+07 1.33E+07 1.07E+07 9.49E+06 7.81E+06 7.12E+06 5.81E+06

75.6 78.25 79.6 82.15 83.5 86.1 87.4 90.1

0.191723 0.200212 0.203657 0.215258 0.220748 0.228424 0.236857 0.247944

9.45E+07 7.33E+07 6.51E+07 4.96E+07 4.30E+07 3.42E+07 3.01E+07 2.34E+07

1.81E+07 1.47E+07 1.33E+07 1.07E+07 9.49E+06 7.81E+06 7.12E+06 5.81E+06

 91.4 94.1 95.45 97.95 99.35 101.95 103.25 105.9

2.08E+07 1.68E+07 1.51E+07 1.19E+07 1.06E+07 8.59E+06 7.87E+06 6.42E+06

91.4 94.1 95.45 97.95 99.35 101.95 103.25 105.9

5.29E+06 4.53E+06 4.23E+06 3.62E+06 3.36E+06 2.97E+06 2.84E+06 2.53E+06

91.4 94.1 95.45 97.95 99.35 101.95 103.25 105.9

0.254073 0.270424 0.280534 0.305308 0.316923 0.345943 0.360384 0.393858

2.08E+07 1.68E+07 1.51E+07 1.19E+07 1.06E+07 8.59E+06 7.87E+06 6.42E+06

5.29E+06 4.53E+06 4.23E+06 3.62E+06 3.36E+06 2.97E+06 2.84E+06 2.53E+06

 107.15 109.9 111.15 113.65 115 118.9 120.3 120.75

5.72E+06 4.43E+06 3.91E+06 2.88E+06 2.42E+06 1.37E+06 835485 649366

107.15 109.9 111.15 113.65 115 118.9 120.3 120.75

2.36E+06 2.07E+06 1.95E+06 1.68E+06 1.55E+06 1.24E+06 1.07E+06 1.01E+06

107.15 109.9 111.15 113.65 115 118.9 120.3 120.75

0.412474 0.467627 0.499218 0.582669 0.640219 0.906745 1.27549 1.56074

5.72E+06 4.43E+06 3.91E+06 2.88E+06 2.42E+06 1.37E+06 835485 649366

2.36E+06 2.07E+06 1.95E+06 1.68E+06 1.55E+06 1.24E+06 1.07E+06 1.01E+06

 120.95 121.1 121.1 121.05 120.85 120.6 120.65 120.8

531695 523307 572464 641578 701372 790184 860352 964694

120.95 121.1 121.1 121.05 120.85 120.6 120.65 120.8

977001 974572 980138 992705 996746 1.01E+06 1.03E+06 1.04E+06

120.95 121.1 121.1 121.05 120.85 120.6 120.65 120.8

1.83752 1.86233 1.71214 1.54729 1.42114 1.2828 1.19911 1.08094

531695 523307 572464 641578 701372 790184 860352 964694

977001 974572 980138 992705 996746 1.01E+06 1.03E+06 1.04E+06

 120.5 120.45 120.6 120.4 120.45 120.45 120.35 120.35

1.03E+06 1.11E+06 1.15E+06 1.19E+06 1.27E+06 1.32E+06 1.35E+06 1.40E+06

120.5 120.45 120.6 120.4 120.45 120.45 120.35 120.35

1.05E+06 1.07E+06 1.08E+06 1.07E+06 1.09E+06 1.10E+06 1.10E+06 1.11E+06

120.5 120.45 120.6 120.4 120.45 120.45 120.35 120.35

1.0167 0.96411 0.937916 0.900686 0.858871 0.833192 0.812552 0.791552

1.03E+06 1.11E+06 1.15E+06 1.19E+06 1.27E+06 1.32E+06 1.35E+06 1.40E+06

1.05E+06 1.07E+06 1.08E+06 1.07E+06 1.09E+06 1.10E+06 1.10E+06 1.11E+06

 120.2 120.25 120.25 120.15 120.25 120.25 120.2 120.2

1.46E+06 1.48E+06 1.51E+06 1.56E+06 1.58E+06 1.60E+06 1.60E+06 1.61E+06

120.2 120.25 120.25 120.15 120.25 120.25 120.2 120.2

1.11E+06 1.12E+06 1.12E+06 1.13E+06 1.12E+06 1.13E+06 1.13E+06 1.13E+06

120.2 120.25 120.25 120.15 120.25 120.25 120.2 120.2

0.763346 0.760239 0.742577 0.72535 0.709498 0.70764 0.70635 0.699032

1.46E+06 1.48E+06 1.51E+06 1.56E+06 1.58E+06 1.60E+06 1.60E+06 1.61E+06

1.11E+06 1.12E+06 1.12E+06 1.13E+06 1.12E+06 1.13E+06 1.13E+06 1.13E+06

 120.2 120.15 120 120.1 120 120.1 120.15 120.1

1.63E+06 1.67E+06 1.71E+06 1.73E+06 1.75E+06 1.74E+06 1.76E+06 1.79E+06

120.2 120.15 120 120.1 120 120.1 120.15 120.1

1.13E+06 1.13E+06 1.12E+06 1.14E+06 1.13E+06 1.13E+06 1.13E+06 1.13E+06

120.2 120.15 120 120.1 120 120.1 120.15 120.1

0.692105 0.67772 0.657729 0.656917 0.649019 0.650732 0.646434 0.631091

1.63E+06 1.67E+06 1.71E+06 1.73E+06 1.75E+06 1.74E+06 1.76E+06 1.79E+06

1.13E+06 1.13E+06 1.12E+06 1.14E+06 1.13E+06 1.13E+06 1.13E+06 1.13E+06

 120.1 120 120.1 120.05 120.15 120.1 120.05 120.1

1.81E+06 1.84E+06 1.87E+06 1.89E+06 1.90E+06 1.91E+06 1.94E+06 1.93E+06

120.1 120 120.1 120.05 120.15 120.1 120.05 120.1

1.13E+06 1.15E+06 1.14E+06 1.15E+06 1.15E+06 1.15E+06 1.15E+06 1.14E+06

120.1 120 120.1 120.05 120.15 120.1 120.05 120.1

0.626583 0.624884 0.607544 0.607059 0.604223 0.598417 0.591668 0.590345

1.81E+06 1.84E+06 1.87E+06 1.89E+06 1.90E+06 1.91E+06 1.94E+06 1.93E+06

1.13E+06 1.15E+06 1.14E+06 1.15E+06 1.15E+06 1.15E+06 1.15E+06 1.14E+06

 120.1 120 120.1 120 119.95 120 120.05 120.05

1.94E+06 1.96E+06 1.98E+06 1.99E+06 2.00E+06 1.99E+06 2.04E+06 2.06E+06

120.1 120 120.1 120 119.95 120 120.05 120.05

1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.14E+06 1.14E+06 1.15E+06

120.1 120 120.1 120 119.95 120 120.05 120.05

0.588503 0.583398 0.578124 0.575133 0.565061 0.571209 0.558912 0.557614

1.94E+06 1.96E+06 1.98E+06 1.99E+06 2.00E+06 1.99E+06 2.04E+06 2.06E+06

1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.14E+06 1.14E+06 1.15E+06

 120.05 120 120 119.95 120 120 120.05 120

2.06E+06 2.04E+06 2.07E+06 2.10E+06 2.09E+06 2.09E+06 2.12E+06 2.13E+06

120.05 120 120 119.95 120 120 120.05 120

1.14E+06 1.13E+06 1.14E+06 1.15E+06 1.14E+06 1.13E+06 1.14E+06 1.13E+06

120.05 120 120 119.95 120 120 120.05 120

0.553025 0.55721 0.552698 0.544909 0.545048 0.543867 0.536361 0.529331

2.06E+06 2.04E+06 2.07E+06 2.10E+06 2.09E+06 2.09E+06 2.12E+06 2.13E+06

1.14E+06 1.13E+06 1.14E+06 1.15E+06 1.14E+06 1.13E+06 1.14E+06 1.13E+06

 120.05 120.05 120.05 119.95 120 120.05 119.95 120.05

2.15E+06 2.15E+06 2.17E+06 2.19E+06 2.19E+06 2.19E+06 2.20E+06 2.22E+06

120.05 120.05 120.05 119.95 120 120.05 119.95 120.05

1.13E+06 1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.13E+06 1.14E+06

120.05 120.05 120.05 119.95 120 120.05 119.95 120.05

0.527685 0.531159 0.524672 0.519814 0.520394 0.516084 0.512916 0.51103

2.15E+06 2.15E+06 2.17E+06 2.19E+06 2.19E+06 2.19E+06 2.20E+06 2.22E+06

1.13E+06 1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.13E+06 1.14E+06

 120 119.95 120.05 119.95 120.05 120 119.95 120.05

2.24E+06 2.27E+06 2.26E+06 2.27E+06 2.28E+06 2.30E+06 2.30E+06 2.33E+06

120 119.95 120.05 119.95 120.05 120 119.95 120.05

1.14E+06 1.14E+06 1.15E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.14E+06

120 119.95 120.05 119.95 120.05 120 119.95 120.05

0.509691 0.501677 0.50621 0.502435 0.501709 0.495622 0.492641 0.488299

2.24E+06 2.27E+06 2.26E+06 2.27E+06 2.28E+06 2.30E+06 2.30E+06 2.33E+06

1.14E+06 1.14E+06 1.15E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.14E+06

 120.05 120 120.05 119.95 120.05 120.05 120 119.95

2.34E+06 2.36E+06 2.35E+06 2.36E+06 2.37E+06 2.39E+06 2.38E+06 2.41E+06

120.05 120 120.05 119.95 120.05 120.05 120 119.95

1.14E+06 1.14E+06 1.13E+06 1.13E+06 1.13E+06 1.13E+06 1.14E+06 1.13E+06

120.05 120 120.05 119.95 120.05 120.05 120 119.95

0.488565 0.483763 0.481264 0.480486 0.477325 0.474271 0.478013 0.469942

2.34E+06 2.36E+06 2.35E+06 2.36E+06 2.37E+06 2.39E+06 2.38E+06 2.41E+06

1.14E+06 1.14E+06 1.13E+06 1.13E+06 1.13E+06 1.13E+06 1.14E+06 1.13E+06

 119.95 119.95 120 120 119.9 119.95 120 119.95

2.42E+06 2.43E+06 2.44E+06 2.45E+06 2.46E+06 2.46E+06 2.46E+06 2.50E+06

119.95 119.95 120 120 119.9 119.95 120 119.95

1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.13E+06 1.13E+06

119.95 119.95 120 120 119.9 119.95 120 119.95

0.470139 0.469192 0.465539 0.463565 0.462315 0.458464 0.457381 0.453475

2.42E+06 2.43E+06 2.44E+06 2.45E+06 2.46E+06 2.46E+06 2.46E+06 2.50E+06

1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.14E+06 1.13E+06 1.13E+06 1.13E+06

 120.1 120 119.95 62.6 66.75 68.55 69 69.85

2.50E+06 2.50E+06 2.52E+06

7.37E+07 6.54E+07 6.18E+07 6.10E+07 5.92E+07

120.1 120 119.95 62.6 66.75 68.55 69 69.85

1.12E+06 1.13E+06 1.14E+06

1.34E+07 1.20E+07 1.14E+07 1.12E+07 1.09E+07

120.1 120 119.95 62.6 66.75 68.55 69 69.85

0.450078 0.452494 0.454254

0.182232 0.183032 0.1842 0.183257 0.184169
2.50E+06 2.50E+06 2.52E+06 7.37E+07 6.54E+07 6.18E+07 6.10E+07 5.92E+07

1.12E+06 1.13E+06 1.14E+06

1.34E+07 1.20E+07 1.14E+07 1.12E+07 1.09E+07
 70.6 72.3 74.35 75.55 77.75 78.95 81.5 82.8

5.74E+07 5.37E+07 4.92E+07 4.69E+07 4.29E+07 4.06E+07 3.61E+07 3.38E+07

70.6 72.3 74.35 75.55 77.75 78.95 81.5 82.8

1.08E+07 1.02E+07 9.68E+06 9.38E+06 8.84E+06 8.51E+06 7.88E+06 7.52E+06

70.6 72.3 74.35 75.55 77.75 78.95 81.5 82.8

0.187546 0.190681 0.196743 0.200266 0.20594 0.209543 0.218201 0.222615

5.74E+07 5.37E+07 4.92E+07 4.69E+07 4.29E+07 4.06E+07 3.61E+07 3.38E+07

1.08E+07 1.02E+07 9.68E+06 9.38E+06 8.84E+06 8.51E+06 7.88E+06 7.52E+06

 85.35 88 89.3 91.85 93.25 96 98.55 101.3

3.00E+07 2.55E+07 2.35E+07 1.97E+07 1.75E+07 1.39E+07 1.06E+07 7.95E+06

85.35 88 89.3 91.85 93.25 96 98.55 101.3

6.89E+06 6.14E+06 5.81E+06 5.12E+06 4.72E+06 4.08E+06 3.48E+06 2.92E+06

85.35 88 89.3 91.85 93.25 96 98.55 101.3

0.229503 0.241021 0.246813 0.260063 0.269193 0.294587 0.327991 0.366816

3.00E+07 2.55E+07 2.35E+07 1.97E+07 1.75E+07 1.39E+07 1.06E+07 7.95E+06

6.89E+06 6.14E+06 5.81E+06 5.12E+06 4.72E+06 4.08E+06 3.48E+06 2.92E+06

 102.65 103.95 106.7 109.35 110.65 113.3 114.55 118.25

6.89E+06 5.94E+06 4.29E+06 3.06E+06 2.59E+06 1.80E+06 1.46E+06 605548

102.65 103.95 106.7 109.35 110.65 113.3 114.55 118.25

2.71E+06 2.53E+06 2.17E+06 1.89E+06 1.76E+06 1.52E+06 1.41E+06 1.14E+06

102.65 103.95 106.7 109.35 110.65 113.3 114.55 118.25

0.393041 0.425674 0.506724 0.61953 0.678311 0.844262 0.963214 1.88836

6.89E+06 5.94E+06 4.29E+06 3.06E+06 2.59E+06 1.80E+06 1.46E+06 605548

2.71E+06 2.53E+06 2.17E+06 1.89E+06 1.76E+06 1.52E+06 1.41E+06 1.14E+06

 119.65 120.3 120.55 120.75 120.6 120.5 120.55 120.5

283458 166915 125944 106124 102235 126233 149065 173452

119.65 120.3 120.55 120.75 120.6 120.5 120.55 120.5

1.03E+06 997444 963164 943267 948576 944917 939488 954545

119.65 120.3 120.55 120.75 120.6 120.5 120.55 120.5

3.63151 5.97576 7.64757 8.88838 9.2784 7.48551 6.30256 5.50321

 283458 166915 125944 106124 102235 126233 149065 173452

1.03E+06 997444 963164 943267 948576 944917 939488 954545

 120.55 120.4 120.35 120.4 120.35 120.2 120.25 120.25

206997 213385 208016 201614 225367 240428 255007 244095

120.55 120.4 120.35 120.4 120.35 120.2 120.25 120.25

954531 962221 957760 951049 951549 956051 961305 949583

120.55 120.4 120.35 120.4 120.35 120.2 120.25 120.25

4.61133 4.50933 4.60425 4.71717 4.22223 3.97645 3.76972 3.89021

206997 213385 208016 201614 225367 240428 255007 244095

954531 962221 957760 951049 951549 956051 961305 949583

 120.2 120.15 120.2 120.2 120.1 120.1 120.15 120.05

266937 240461 272076 295474 276492 291586 302080 284888

120.2 120.15 120.2 120.2 120.1 120.1 120.15 120.05

957344 951542 944817 967854 957916 957527 956683 950938

120.2 120.15 120.2 120.2 120.1 120.1 120.15 120.05

3.58641 3.95715 3.47262 3.2756 3.46453 3.28386 3.16699 3.33793

266937 240461 272076 295474 276492 291586 302080 284888

957344 951542 944817 967854 957916 957527 956683 950938

 120.05 120 120.1 120.1 120 120.1 120.1 120

327385 333416 332529 328589 340807 334832 339966 359889

120.05 120 120.1 120.1 120 120.1 120.1 120

960355 959766 956619 947843 963856 955421 953937 949519

120.05 120 120.1 120.1 120 120.1 120.1 120

2.93341 2.87858 2.8768 2.88458 2.82816 2.85344 2.80598 2.63837

327385 333416 332529 328589 340807 334832 339966 359889

960355 959766 956619 947843 963856 955421 953937 949519

 119.95 120.05 120 120.1 120 120.1 120.05 120

375818 380085 388115 397812 398837 383114 400268 408748

119.95 120.05 120 120.1 120 120.1 120.05 120

959517 962456 963896 968500 960929 962328 959749 959712

119.95 120.05 120 120.1 120 120.1 120.05 120

2.55314 2.53221 2.48353 2.43457 2.40933 2.51185 2.39776 2.34793

375818 380085 388115 397812 398837 383114 400268 408748

959517 962456 963896 968500 960929 962328 959749 959712

 120 119.95 119.95 120.05 119.95 120.1 119.95 120

422283 431097 438685 437483 440578 436824 448112 471945

120 119.95 119.95 120.05 119.95 120.1 119.95 120

965189 967167 961940 965322 963041 961123 961662 963035

120 119.95 119.95 120.05 119.95 120.1 119.95 120

2.28564 2.2435 2.19278 2.20654 2.18586 2.20025 2.14603 2.04057

422283 431097 438685 437483 440578 436824 448112 471945

965189 967167 961940 965322 963041 961123 961662 963035

 120 119.9 120.05 120.1 119.95 120 120 120.05

484095 489778 473437 478763 494149 484991 506182 503764

120 119.9 120.05 120.1 119.95 120 120 120.05

968809 966697 966413 963906 963758 969546 971181 970101

120 119.9 120.05 120.1 119.95 120 120 120.05

2.00128 1.97375 2.04127 2.01333 1.95034 1.9991 1.91864 1.92571

484095 489778 473437 478763 494149 484991 506182 503764

968809 966697 966413 963906 963758 969546 971181 970101

 120.05 120.05 120.05 119.95 119.95 120 120.1 120

488250 504949 521222 529943 525544 525367 523434 539327

120.05 120.05 120.05 119.95 119.95 120 120.1 120

973821 956623 977179 973142 979025 967487 974851 969132

120.05 120.05 120.05 119.95 119.95 120 120.1 120

1.99451 1.89449 1.87478 1.83632 1.86288 1.84154 1.86242 1.79693

488250 504949 521222 529943 525544 525367 523434 539327

973821 956623 977179 973142 979025 967487 974851 969132

 120.05 120 119.95 120.05 119.95 120 120.05 119.95

537423 552686 560329 560169 558797 560341 553169 561141

120.05 120 119.95 120.05 119.95 120 120.05 119.95

973226 984506 977293 970388 967892 979394 973533 969278

120.05 120 119.95 120.05 119.95 120 120.05 119.95

1.81091 1.78131 1.74414 1.73231 1.7321 1.74785 1.75992 1.72733

537423 552686 560329 560169 558797 560341 553169 561141

973226 984506 977293 970388 967892 979394 973533 969278

 120.1 120.05 120 119.9 119.95 119.95 120 21.95

551384 573681 582854 610436 577933 587566 601867

1.98E+08

120.1 120.05 120 119.9 119.95 119.95 120 21.95

975702 976225 976688 983721 977169 978412 980144

1.10E+07

120.1 120.05 120 119.9 119.95 119.95 120 21.95

1.76955 1.70169 1.6757 1.61151 1.6908 1.6652 1.62851

0.0555835
551384 573681 582854 610436 577933 587566 601867 1.98E+08

975702 976225 976688 983721 977169 978412 980144

1.10E+07
 22.15 23.5 24.3 26.2 27.3 29.6 30.8 33.2

1.97E+08 1.92E+08 1.90E+08 1.84E+08 1.80E+08 1.72E+08 1.68E+08 1.59E+08

22.15 23.5 24.3 26.2 27.3 29.6 30.8 33.2

1.11E+07 1.13E+07 1.14E+07 1.15E+07 1.16E+07 1.20E+07 1.21E+07 1.23E+07

22.15 23.5 24.3 26.2 27.3 29.6 30.8 33.2

0.0561934 0.0585354 0.0598728 0.0627869 0.0646087 0.0696074 0.0717613 0.0778073

1.97E+08 1.92E+08 1.90E+08 1.84E+08 1.80E+08 1.72E+08 1.68E+08 1.59E+08

1.11E+07 1.13E+07 1.14E+07 1.15E+07 1.16E+07 1.20E+07 1.21E+07 1.23E+07

 34.45 37 38.25 40.95 42.2 44.8 47.45 48.75

1.54E+08 1.44E+08 1.38E+08 1.28E+08 1.23E+08 1.14E+08 1.04E+08 9.88E+07

34.45 37 38.25 40.95 42.2 44.8 47.45 48.75

1.24E+07 1.26E+07 1.27E+07 1.26E+07 1.26E+07 1.24E+07 1.23E+07 1.21E+07

34.45 37 38.25 40.95 42.2 44.8 47.45 48.75

0.0808401 0.0872356 0.0913902 0.098459 0.102415 0.109047 0.117931 0.122118

1.54E+08 1.44E+08 1.38E+08 1.28E+08 1.23E+08 1.14E+08 1.04E+08 9.88E+07

1.24E+07 1.26E+07 1.27E+07 1.26E+07 1.26E+07 1.24E+07 1.23E+07 1.21E+07

 51.4 52.75 55.5 56.7 59.45 60.75 63.35 64.75

9.00E+07 8.54E+07 7.71E+07 7.39E+07 6.51E+07 6.18E+07 5.42E+07 5.10E+07

51.4 52.75 55.5 56.7 59.45 60.75 63.35 64.75

1.17E+07 1.15E+07 1.10E+07 1.07E+07 1.01E+07 9.72E+06 9.08E+06 8.69E+06

51.4 52.75 55.5 56.7 59.45 60.75 63.35 64.75

0.129819 0.134462 0.142942 0.144932 0.155709 0.157151 0.167499 0.170216

9.00E+07 8.54E+07 7.71E+07 7.39E+07 6.51E+07 6.18E+07 5.42E+07 5.10E+07

1.17E+07 1.15E+07 1.10E+07 1.07E+07 1.01E+07 9.72E+06 9.08E+06 8.69E+06

 67.25 68.7 71.2 73.8 75.15 77.7 79.1 81.75

4.55E+07 4.24E+07 3.75E+07 3.22E+07 2.98E+07 2.55E+07 2.35E+07 1.99E+07

67.25 68.7 71.2 73.8 75.15 77.7 79.1 81.75

8.10E+06 7.69E+06 7.03E+06 6.34E+06 6.00E+06 5.36E+06 5.07E+06 4.49E+06

67.25 68.7 71.2 73.8 75.15 77.7 79.1 81.75

0.178016 0.181131 0.187205 0.196633 0.20152 0.210239 0.215727 0.225836

4.55E+07 4.24E+07 3.75E+07 3.22E+07 2.98E+07 2.55E+07 2.35E+07 1.99E+07

8.10E+06 7.69E+06 7.03E+06 6.34E+06 6.00E+06 5.36E+06 5.07E+06 4.49E+06

 83.1 85.65 86.95 89.45 90.75 93.75 95.9 97.3

1.84E+07 1.57E+07 1.46E+07 1.22E+07 1.08E+07 8.72E+06 7.22E+06 6.36E+06

83.1 85.65 86.95 89.45 90.75 93.75 95.9 97.3

4.25E+06 3.85E+06 3.62E+06 3.31E+06 3.07E+06 2.74E+06 2.48E+06 2.32E+06

83.1 85.65 86.95 89.45 90.75 93.75 95.9 97.3

0.230512 0.245758 0.248275 0.272026 0.285264 0.313798 0.343927 0.365419

1.84E+07 1.57E+07 1.46E+07 1.22E+07 1.08E+07 8.72E+06 7.22E+06 6.36E+06

4.25E+06 3.85E+06 3.62E+06 3.31E+06 3.07E+06 2.74E+06 2.48E+06 2.32E+06

 100.1 101.4 103.75 105.25 107.85 108.9 112 114.25

5.10E+06 4.62E+06 3.53E+06 3.07E+06 2.46E+06 2.12E+06 1.52E+06 1.04E+06

100.1 101.4 103.75 105.25 107.85 108.9 112 114.25

2.07E+06 2.01E+06 1.81E+06 1.70E+06 1.54E+06 1.47E+06 1.30E+06 1.18E+06

100.1 101.4 103.75 105.25 107.85 108.9 112 114.25

0.406055 0.434278 0.513077 0.552853 0.62565 0.693305 0.855569 1.12825

5.10E+06 4.62E+06 3.53E+06 3.07E+06 2.46E+06 2.12E+06 1.52E+06 1.04E+06

2.07E+06 2.01E+06 1.81E+06 1.70E+06 1.54E+06 1.47E+06 1.30E+06 1.18E+06

 115.55 118.95 120.3 120.75 121.15 121 120.9 120.9

785170 166769 -153933 -282884 -317081 -285210 -266942 -241931

115.55 118.95 120.3 120.75 121.15 121 120.9 120.9

1.11E+06 917338 828545 769132 749092 756283 754839 757228

115.55 118.95 120.3 120.75 121.15 121 120.9 120.9

1.40852 5.50065 6000 6000 6000 6000 6000 6000

 785170 166769 -153933 -282884 -317081 -285210 -266942 -241931

1.11E+06 917338 828545 769132 749092 756283 754839 757228

 121 120.9 120.75 120.65 120.5 120.7 120.3 120.5

-201231 -160478 -94485.2 -33958.4 49180.2 74959.6 159117 208290

121 120.9 120.75 120.65 120.5 120.7 120.3 120.5

766530 765397 784557 801402 817454 822639 835991 856597

121 120.9 120.75 120.65 120.5 120.7 120.3 120.5

6000 6000 6000 6000 16.6216 10.9744 5.25392 4.11252

-201231 -160478 -94485.2 -33958.4 49180.2 74959.6 159117 208290

766530 765397 784557 801402 817454 822639 835991 856597

 120.5 120.45 120.5 120.45 120.4 120.25 120.3 120.25

246761 287162 339769 369931 407508 421560 429409 474316

120.5 120.45 120.5 120.45 120.4 120.25 120.3 120.25

851745 866964 881025 889350 895716 892997 901142 914460

120.5 120.45 120.5 120.45 120.4 120.25 120.3 120.25

3.4517 3.01908 2.59301 2.4041 2.19803 2.11832 2.09856 1.92796

246761 287162 339769 369931 407508 421560 429409 474316

851745 866964 881025 889350 895716 892997 901142 914460

 120.1 120.25 120.3 120.25 120.15 120.15 120.2 120.1

494979 495002 490714 525238 519247 503894 533386 506229

120.1 120.25 120.3 120.25 120.15 120.15 120.2 120.1

900363 912797 916387 923274 918134 912338 921541 925689

120.1 120.25 120.3 120.25 120.15 120.15 120.2 120.1

1.81899 1.84403 1.86746 1.75782 1.76821 1.81057 1.72772 1.8286

494979 495002 490714 525238 519247 503894 533386 506229

900363 912797 916387 923274 918134 912338 921541 925689

 120.1 120.1 120.2 120.1 120.1 120.05 120.05 120

522828 521643 529726 552280 547630 530974 546973 564763

120.1 120.1 120.2 120.1 120.1 120.05 120.05 120

920367 926996 923533 926994 918386 918029 913005 922095

120.1 120.1 120.2 120.1 120.1 120.05 120.05 120

1.76036 1.77707 1.74342 1.67848 1.67702 1.72895 1.6692 1.63271

522828 521643 529726 552280 547630 530974 546973 564763

920367 926996 923533 926994 918386 918029 913005 922095

 120.05 120.1 120 120.1 120.05 120 120.05 120

563762 544836 577417 558628 556028 548425 562703 554262

120.05 120.1 120 120.1 120.05 120 120.05 120

929053 924290 920394 922857 915689 915434 913445 918176

120.05 120.1 120 120.1 120.05 120 120.05 120

1.64795 1.69645 1.59399 1.65201 1.64684 1.66921 1.62332 1.65658

563762 544836 577417 558628 556028 548425 562703 554262

1.40E+
929053 924290 920394 922857 915689 915434 913445 918176
1.20E+

1.00E+

Loss Modulus (MPa)

8.00E+

6.00E+

4.00E+

2.00E+

0.00E+
-5.00E+08
 119.95 120.05 120.05 120.05 120 120 119.9 120.05

584158 573856 585890 565224 557640 552974 560946 555181

119.95 120.05 120.05 120.05 120 120 119.9 120.05

924597 922025 916825 923477 917951 920597 896330 909668

119.95 120.05 120.05 120.05 120 120 119.9 120.05

1.58279 1.60672 1.56484 1.63382 1.64614 1.66481 1.59789 1.63851

 584158 573856 585890 565224 557640 552974 560946 555181

1.40E+08
924597 922025 916825 923477 917951 920597 896330 909668
1.20E+08

1.00E+08
Loss Modulus (MPa)

8.00E+07
E''1(Pa)
6.00E+07 E''2(Pa)
E''3(Pa)
E''4(Pa)
4.00E+07

2.00E+07

0.00E+00
-5.00E+08 0.00E+00 5.00E+08 1.00E+09 1.50E+09 2.00E+09
Storage Modulus (MPa)
 120 120.05 119.9 119.95 119.95

563874 554571 565953 567089 568596

120 120.05 119.9 119.95 119.95

919568 919435 908688 906559 914239

120 120.05 119.9 119.95 119.95

1.6308 1.65792 1.60559 1.59862 1.60789

 563874 554571 565953 567089 568596

919568 919435 908688 906559 914239

E''1(Pa)
E''2(Pa)
E''3(Pa)
E''4(Pa)

2.00E+09
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