Meas. Pts.

Storage Modulus Loss ModulusShear Rate Shear Stress Viscosity Model HB

[Pa] [Pa] [1/s] [Pa] [Pa·s]
1 ****** ****** 200 377.6 1.887 381.328135
2 ****** ****** 136.5 339.5 2.487 350.291093
3 ****** ****** 93.16 311.7 3.346 321.824534
4 ****** ****** 63.55 290.2 4.566 295.684776
5 ****** ****** 43.39 269.9 6.221 271.767031
6 ****** ****** 29.59 252.3 8.528 249.763185
7 ****** ****** 20.18 234.8 11.63 229.588453
8 ****** ****** 13.79 221.7 16.08 211.180744
9 ****** ****** 9.405 208.3 22.15 194.210406
10 ****** ****** 6.419 196.8 30.66 178.676723
11 ****** ****** 4.383 185.6 42.35 164.446048
12 ****** ****** 2.987 174.7 58.48 151.329655
13 ****** ****** 2.042 161.3 79.02 139.397785
14 ****** ****** 1.41 142.3 100.9 128.726306
15 ****** ****** 0.9768 121.6 124.5 118.996384
16 ****** ****** 0.6763 103.8 153.5 110.028761
17 ****** ****** 0.4682 89.29 190.7 101.775285
18 ****** ****** 0.3242 77.84 240.1 94.1852347
19 ****** ****** 0.2252 69.02 306.5 87.2588653
20 ****** ****** 0.1575 62.1 394.3 80.9953676
21 ****** ****** 0.112 56.3 502.6 75.4774662
22 ****** ****** 0.07865 51.6 656.1 70.1886309
23 ****** ****** 0.05509 47.97 870.8 65.2727838
24 ****** ****** 0.03872 45.21 1,168 60.7795862
25 ****** ****** 0.02725 43.1 1,582 56.6459475
26 ****** ****** 0.01928 41.47 2,151 52.8839006
27 ****** ****** 0.01394 40.2 2,885 49.6153564
28 ****** ****** 0.009832 39.23 3,990 46.3548725
29 ****** ****** 0.007379 38.44 5,209 43.8609377
30 ****** ****** 0.005368 37.8 7,041 41.2790464
31 ****** ****** 0.004057 37.29 9,192 39.1557672
32 ****** ****** 0.002876 36.89 12,830 36.7246788
33 ****** ****** 0.002432 36.55 15,030 35.6066739
34 ****** ****** 0.001664 36.26 21,790 33.2279057
35 ****** ****** 0.001434 36.02 25,120 32.3498033
36 ****** ****** 0.001049 35.82 34,160 30.5979932
37 ****** ****** 0.0009276 35.64 38,430 29.9420904
38 ****** ****** 0.0007443 35.49 47,680 28.8126725
39 ****** ****** 0.0005906 35.36 59,880 27.6851686
40 ****** ****** 0.0004813 35.25 73,250 26.7356643
41 ****** ****** 0.0003912 35.17 89,900 25.8177988
42 ****** ****** 0.0003191 35.09 110,000 24.9566984
43 ****** ****** 0.0002819 35.03 124,200 24.4518597
44 ****** ****** 0.000254 34.97 137,700 24.038222
45 ****** ****** 0.000221 34.92 158,000 23.5008568
Parametre HB Erreur HB Modele WD Paramatre WD Erreur WD
Ty0 6.71384445
K 112.880851 13.8989913 19302.1212 Ty0 34 358137503.22
n 0.22640473 116.447697 13233.0306 n 98 166243131.1
102.506186 9059.85592 Ty1 160 76530231.927
30.0827697 6198.04096 Y 155 34902584.798
3.48580569 4245.5164 15805525.753
6.43542795 2907.31687 7049114.57
27.1602226 1994.11985 3095206.3286
110.654756 1373.69628 1327095.4293
198.51666 947.807932 546871.98081
328.453184 657.73442 212460.53983
447.489704 459.920191 75251.567394
546.17303 324.274311 22372.474429
479.707039 232.445069 5061.6208711
184.245177 171.028577 825.33115227
6.7788163 128.929849 53.726684285
38.7974661 99.7264324 16.593952792
155.88233 79.5024233 95.796657664
267.166698 65.507781 152.08362628
332.656209 55.8864011 172.491419
357.034917 49.3069027 163.66333926
367.77521 44.8849219 130.30400718
345.5372 41.6437489 99.126935216
299.386326 39.3540292 74.234952792
242.412013 37.7630805 55.456610704
183.492695 36.6483464 41.623833661
130.277127 35.8737663 31.317832173
88.6489355 35.3547876 23.476083013
50.7638076 34.9555433 18.270980234
29.386566 34.7171434 13.859660934
12.1037639 34.5217003 10.747249186
3.48108734 34.394288 8.385147938
0.02733111 34.2795101 6.8146576818
0.88986406 34.236359 5.3529346591
9.19359578 34.1617193 4.4027818046
13.4703438 34.1393663 3.536783146
27.2693553 34.1019493 2.9516983396
32.4661741 34.0901507 2.4020327017
44.5867019 34.0723364 2.0097702113
58.9030373 34.0573987 1.6967701508
72.4939132 34.0467761 1.4477476354
87.4636681 34.0380196 1.2813796444
102.6838 34.0310124 1.1214547321
111.897052 34.027397 1.0052126906
119.503771 34.0246855 0.8936194615
130.396831 34.0214783 0.8073411586
6318.08326 663954433.52
Modele MA Parametre MA Erreur MA

558.22058 Ty0 36.991129 0.22880762 1000

464.513909 K 39.3346476 0.13559295
389.03616 Ty1 0 0.06155901

Contrainte de cissaillement Pa
328.077176 Y 67.8980693 0.01703572
278.625352 0.00104511
237.891364 0.00326145
100
204.179973 0.0170065
176.260856 0.0420077
152.836102 0.07089935
133.311512 0.10407341
117.0282 0.13650079
103.38091 0.16665785 10
0.0001 0.001 0.01 0.1 1
92.1038491 0.18403276
Vitesse d'ecoulement,s-1
82.938183 0.17402217
75.3384624 0.1447348
68.9723226 0.1125782
63.6517176 0.0824465
59.2115079 0.05727298
100000
55.5349947 0.03817265
52.5158762 0.0238189
Contrainte de cisaillement,Pa

50.0940522 0.01215065 10000

47.9795525 0.00492295
46.193465 0.00137154 1000
44.7100755 0.00012228
43.4694822 7.34907E-05
100
42.4423385 0.00054975
41.6276897 0.00126129
40.8860566 0.00178202 10
0.0001 0.001 0.01 0.1 1
40.3659989 0.00251041 Vitesse d'ecoulement,s¯¹
39.870122 0.00299922
39.4943228 0.00349434
39.0990145 0.00358575
38.9296045 0.00423872
38.5947676 0.00414602
38.4798798 0.0046638
1000
38.2645387 0.00465739
Contrainte de cisaillement,Pa

38.1886204 0.0051137
38.063846 0.0052596
37.9467282 0.00535152
37.853812 0.00545633 100
37.7689071 0.00546055
37.6936046 0.00550533
37.6513994 0.00559998

10
0.0001 0.001 0.01 0.1 1
Vitesse de cisaillement,s¯¹
 100

Contrainte d
37.6178818 0.00573332
10
37.5757602 0.00578401 0.0001 0.001 0.01 0.1 1
1.90332038 Vitesse de cisaillement,s¯¹

1000000

100000

10000

Viscosite
1000

100

10

1
0.0001 0.001 0.01 0.1 1 1
Vitesse de cisaillment,s¯¹
 Modele
HB

Courbe
d'ecoule
ment

0.1 1 10 100 1000

Vitesse d'ecoulement,s-1

Modele
WD

Courbe
d'ecoule
ment

0.01 0.1 1 10 100 1000

Vitesse d'ecoulement,s¯¹

Mod
ele

ecoule
ment

01 0.1 1 10 100 1000

Vitesse de cisaillement,s¯¹
 ele

ecoule
ment

01 0.1 1 10 100 1000

Vitesse de cisaillement,s¯¹

Viscosite

0.01 0.1 1 10 100 1000

Vitesse de cisaillment,s¯¹
Meas. Pts. Storage Modulus Loss Modulus Shear Rate Shear Stress Viscosity
[Pa] [Pa] [1/s] [Pa] [Pa·s]
1 1,115 12.16 0.0009875 0.1101 ******
2 1,118 13.18 0.001376 0.1538 ******
3 1,120 12.79 0.00192 0.215 ******
4 1,122 12.32 0.00267 0.2995 ******
5 1,123 11.71 0.003712 0.4169 ******
6 1,129 12.6 0.005156 0.5821 ******
7 1,129 13.49 0.007169 0.8091 ******
8 1,126 13.73 0.009964 1.122 ******
9 1,124 14.94 0.01385 1.557 ******
10 1,122 16.02 0.01924 2.158 ******
11 1,119 17.18 0.02672 2.991 ******
12 1,117 18.6 0.03712 4.149 ******
13 1,118 20.13 0.05158 5.77 ******
14 1,121 21.97 0.0717 8.037 ******
15 1,120 24.02 0.09963 11.16 ******
16 1,111 26.44 0.1385 15.39 ******
17 1,085 54.67 0.1922 20.89 ******
18 1,028 219.1 0.2676 28.12 ******
19 931.8 322.6 0.3722 36.7 ******
20 834.3 401.3 0.5173 47.89 ******
21 734.7 448.9 0.7189 61.9 ******
22 640.9 471.2 0.9988 79.45 ******
23 552.7 472.6 1.388 100.9 ******
24 467.1 454.4 1.928 125.7 ******
25 381.5 419.5 2.68 152 ******
26 291.9 364.3 3.726 173.9 ******
27 203.6 301.1 5.179 188.3 ******
28 140.9 245.3 7.196 203.6 ******
29 97.62 197.4 9.998 220.2 ******
30 66.73 159.2 13.89 239.8 ******
31 45.15 127.6 19.3 261.2 ******
32 30.13 101.3 26.83 283.6 ******
33 19.82 80.01 37.27 307.3 ******
34 12.84 62.82 51.79 332.1 ******
35 8.194 49.15 71.97 358.6 ******
36 5.17 38.6 100 389.4 ******
 10,000

1,000
Storage Modu-
lus G'
Modules,Pa

Loss Modulus G
100

10

1
0.0001 0.001 0.01 0.1 1 10 100
Vitesse de cisaillment,s¯¹
Angular Frequency Complex Viscosity Damping Factor Storage Modulus Loss Modulus
[rad/s] [Pa·s] [1] [Pa] [Pa]
0.1 112000 0.0687 1,115 12.16
1.11 11200 0.0592 1,118 13.18
2.12 6030 0.0614 1,120 12.79
3.13 4160 0.0634 1,122 12.32
4.14 3190 0.0647 1,123 11.71
5.15 2590 0.066 1,129 12.6
6.15 2190 0.067 1,129 13.49
7.16 1890 0.0677 1,126 13.73
8.17 1670 0.0683 1,124 14.94
9.18 1500 0.0692 1,122 16.02
10.2 1360 0.0697 1,119 17.18
11.2 1240 0.0703 1,117 18.6
12.2 1140 0.0707 1,118 20.13
13.2 1060 0.0711 1,121 21.97
14.2 990 0.0716 1,120 24.02
15.2 928 0.0718 1,111 26.44
16.2 874 0.0722 1,085 54.67
17.3 826 0.0725 1,028 219.1
18.3 782 0.0728 931.8 322.6
19.3 744 0.073 834.3 401.3
20.3 709 0.0734 734.7 448.9
21.3 677 0.0735 640.9 471.2
22.3 648 0.0738 552.7 472.6
23.3 622 0.074 467.1 454.4
24.3 598 0.0742 381.5 419.5
25.3 575 0.0744 291.9 364.3
26.3 555 0.0746 203.6 301.1
27.3 535 0.0748 140.9 245.3
28.4 517 0.075 97.62 197.4
29.4 501 0.0751 66.73 159.2
30.4 485 0.0753 45.15 127.6
31.4 470 0.0754 30.13 101.3
32.4 457 0.0756 19.82 80.01
33.4 444 0.0757 12.84 62.82
34.4 431 0.0759 8.194 49.15
35.4 420 0.076 5.17 38.6
36.4 409 0.0761
37.4 399 0.0762
38.4 389 0.0764
39.5 380 0.0765
40.5 371 0.0766
41.5 362 0.0767
42.5 354 0.0768
43.5 346 0.0769
44.5 339 0.077
45.5 332 0.0771
46.5 325 0.0772
47.5 319 0.0773
48.5 313 0.0774
49.5 307 0.0775
50.6 301 0.0776
51.6 295 0.0777
52.6 290 0.0777
53.6 285 0.0778
54.6 280 0.0779
55.6 275 0.078
56.6 271 0.0781
57.6 266 0.0781
58.6 262 0.0782
59.6 258 0.0783
60.6 254 0.0783
61.7 250 0.0784
62.7 246 0.0785
63.7 243 0.0786
64.7 239 0.0786
65.7 236 0.0787
66.7 232 0.0788
67.7 229 0.0788
68.7 226 0.0789
69.7 223 0.0789
70.7 220 0.079
71.7 217 0.0791
72.8 214 0.0791
73.8 212 0.0792
74.8 209 0.0791
75.8 206 0.0794
76.8 204 0.0793
77.8 201 0.0795
78.8 199 0.0794
79.8 197 0.0795
80.8 194 0.0795
81.8 192 0.0796
82.8 190 0.0797
83.9 188 0.0797
84.9 186 0.0798
85.9 184 0.0798
86.9 182 0.0799
87.9 180 0.0799
88.9 178 0.08
89.9 176 0.08
90.9 174 0.0801
91.9 173 0.0801
92.9 171 0.0801
93.9 169 0.0802
95 167 0.0802
96 166 0.0803
97 164 0.0803
98 163 0.0803
99 161 0.0804
100 160 0.0804
 1000000
G'(Pa),G"(Pa),C Viscosite(Pa•s),Damping Factor
100000

10000
Damping factor
1000

100

10
Complexe de
1 viscosite

0.1

0.01
0.1 1 10 100
Angular Frequency
 Damping factor

Complexe de
viscosite

100
Nom
Sangwa Mvumvu Eliel
Kongolo Kapinga Merdie
Mutshail a Nawej Daniel

Modele Ty Observations
HB 6.71384445 Moyen fit
WD 34 Mauvais fit
MA 36.991129 Bon fit
Pas de fit 34.92 Pas important de fiter a cause du palier
Par rapport a la courbe de viscosite apparente,le materiaux est rheoflofluidisant.
Par rapport a amplitude sweep de 1115 a 641,le materiau a un comportement solide(solid like) parceque G'>G",d
Par rapport a frequency sweep,selon la courbe de tangente le materiau est solide(solid like),selon la courbe de vi
lide(solid like) parceque G'>G",de 419,5 a 38,6 , le materiau a comportement liquide(liquid like) parceque G">G'.
(solid like),selon la courbe de viscosite complexe le materiau est rheofluidisant.